ASTMD4752
ASTMD4752
ASTMD4752
selected areas in accordance with Test Methods D7091 or 5 No effect on surface; no zinc on cloth after 50 double
rubs
D4138. Mark a 150- by 25-mm (6- by 1-in.) rectangular test 4 Burnished appearance in rubbed area; slight amount of
area on the undamaged cleaned surface using a pencil or other zinc on cloth after 50 double rubs
suitable solvent resistant marker. 3 Some marring and apparent depression of the film after
50 double rubs
6.3 Fold the cloth into a pad of double thickness and 2 Heavy marring; obvious depression in the film after 50
saturate it to a dripping wet condition with the methyl ethyl double rubs
ketone. Do not allow more than 10 s to elapse before 1 Heavy depression in the film but no actual penetration to
the substrate after 50 double rubs
proceeding to the next steps. 0 Penetration to the substrate in 50 double rubs or less
6.4 Place the properly protected index finger into the center
of the pad while holding excess cloth with the thumb and
remaining fingers of the same hand. With the index finger at a
45° angle to the test surface, rub the rectangular test area with 7.1.3 Number of tests conducted.
moderate pressure first away from the operator and then back 7.1.4 Resulting ratings.
towards the operator. Complete each double rub (one forward 7.1.5 In the case of a zero rating, number of double rubs
and back motion) in about 1 s. required to expose the substrate.
6.5 Continue rubbing the surface with the MEK saturated 7.1.6 Field and Fabricating Shop Tests—Identification of
pad, wetting the pad as necessary without lifting it from the the area or piece tested.
surface, until either the metal substrate is exposed or 50 double
rubs have been completed. If the former, record the number of 8. Precision and Bias
rubs when the substrate is exposed. 8.1 Precision—It is not practicable to specify the precision
6.6 Select an adjacent area to be used as a control. Repeat of this procedure since the rating scale is arbitrary and standard
6.1-6.5, except use a dry cloth to establish the effect of methods for conducting round-robin studies and analyzing data
burnishing without the influence of MEK. Use this area as the based on an arbitrary rating scale are not available. See
control to visually show the appearance of No Effect. Appendix X1 “Goodness.”
6.7 Inspect the test areas and the cloths. Rate the results in 8.2 Bias—Since there is no acceptable reference material,
accordance with Table 1. bias cannot be determined.
7. Report 9. Keywords
7.1 Report, as a minimum, the following information: 9.1 curing characteristics; double rub method; drying or
7.1.1 Dry film thickness of the primer. curing; ethyl silicate (inorganic) primer; methyl ethyl ketone;
7.1.2 Elapsed time between the application of the primer MEK (methyl ethyl ketone) resistance; primer; solvent rub
and the running of the tests. method; visual examination; zinc-rich primer
APPENDIX
(Nonmandatory Information)
X1. GOODNESS
X1.1 An intra-lab round-robin evaluation was conducted in operator. The 95 % confidence limits of the overall mean score
order to access the “goodness” of this practice. Using the (combined average score of the eight operators) are represented
procedure outlines in this practice, eight different operators on each of the figures by dashed lines. The following obser-
were asked to rate, in triplicate, the methyl ethyl ketone (MEK) vations were made through this analysis:
rub resistance of a particular inorganic zinc-rich primer. The
X1.2.1 Rub results are cure time dependent, that is, higher
primer was separately applied to multiple test panels at two
rub scores are associated with longer cure periods, lower rub
different dry film thickness ranges; 2.7-4.5 mils and 6.8-8.0
scores are associated with shorter cure periods.
mils. Separate test panels corresponding to each coating
thickness category were scored after a 6-h cure period and a X1.2.2 Rub results are dependent on coating thickness, that
24-h cure period. Performance ratings and general statistical is, higher rub scores are associated with thick coatings films,
information have been in Table X1.1 for each cure period/film lower rub scores are associated with thinner coating films.
thickness combination. X1.2.3 From the plots, the largest number of operators
whose mean score deviated from the 95 % confidence limits of
X1.2 An analysis of the means, (ANOM), was conducted the overall mean score was found to occur when this practice
on the performance data of Table X1.1. Figs. X1.1-X1.4 is applied to thin film, 6-h cured primers. The second largest
illustrate the raw scores and the mean score reported by each number of operators whose mean score deviated from the 95 %
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D4752 – 10
TABLE X1.1 Round Robin Resistance Rating
Case 1: Thin Film, 6-hr cure
Operator ID Rub 1 Rub 2 Rub 3 Range Mean Standard Deviation
A 0 3 3 3 2.0 1.4
B 3 3 3 0 3.0 0.0
C 0 0 1 1 0.3 0.5
D 3 3 3 0 3.0 0.0
E 4 2 3 2 3.0 0.8
F 0 1 0 1 0.3 0.5
G 3 3 3 0 3.0 0.0
H 1 0 1 1 0.7 0.5
limits of the overall score was found to occur in the case of the X1.3 The findings of this practice’s round-robin evaluation
thin film 24-h cured primers. have been offered in this appendix to serve as a reference or
X1.2.4 All operators had mean scores within the 95 % guide for operators wishing to utilize this practice.
confidence limits of the overall mean score when this practice
was applied to either thick, 6-h cured primers or thick, 24-h
cured primers.
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SUMMARY OF CHANGES
Committee D01.46 has identified the location of selected changes to this standard since the last issue
(D4752 - 03) that may impact the use of this standard. (Approved February 1, 2010.)
(1) Changed title from Test Method to Practice. (3) Section 5.2: changed from cheesecloth to 100 % cotton
(2) Section 2.1 and 6.2: replaced Test Methods D1186 and cloth.
D1400 with Test Method D7091.
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