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    Speedwave Entry Vessel Conditioning

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    agansh01

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    Speedwave Entry Vessel Conditioning

    Uploaded by

    agansh01
    5 views2 pages

    Original Title

    Speedwave-Entry-Vessel-Conditioning

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    © © All Rights Reserved

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    Copyright:

    © All Rights Reserved
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    Download as pdf or txt
    5 views2 pages

    Speedwave Entry Vessel Conditioning

    Uploaded by

    agansh01

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    of 2

    APPLICATION NOTE | SPEEDWAVE ENTRY S.

    1/2

    Environment, Geology
    Microwave Vessel Conditioning

    Summary Microwave digestion vessels change their properties during their usage. Accordingly, their
    microwave absorption characteristics may vary. Most important in this context is, that TFM-
    vessels soak up small amounts of acids and nitric oxides (visible as slight yellow discolouring)
    which must be evaporated to get again a uniform heating of all vessels.

    Method
    Equipment
    Type Manufacturer
    speedwave Entry Berghof Products + Instruments GmbH
    DAP-60K Berghof Products + Instruments GmbH
    Procedure
    All microwave vessels are heated at 250°C over night inside a conventional laboratory oven to
    evaporate soaked acids and to re-condition the vessels.

    The effect on DAP-60+ vessels is illustrated in the figures below by heating 25 ml water in the
    microwave oven with the following program.
    Temperature Program Step T [°C] Ta [min] Time [min] Power [%]
    1 200 10 5 90
    2 75 1 10
    3
    4
    5
    Note: To avoid foaming and splashing wait until the vessels have cooled to room temperature (about 20 min). Carefully open the digestion vessel in a
    fume hood wearing hand, eye and body protection since a large amount of gas will be produced during the digestion process.

    Before Conditioning
    APPLICATION NOTE | SPEEDWAVE ENTRY | ENVIRONMENT, GEOLOGY S. 2/2

    After Conditioning

    Results Uniform heating of all vessels


    Note: This application serves only as a guide line and may need to be optimized for your sample.

    Berghof Products + Instruments GmbH | Harretstrasse 1 | 72800 Eningen | www.berghof.com


    53-0202-87-00-01-003 | Speedwave-Entry-Vessel-Conditioning, Änderungen und Irrtümer vorbehalten, Printed in
    Germany

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