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    Experiment Chemical Kinetics

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    akshanprakash12

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    © All Rights Reserved
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    Experiment Chemical Kinetics

    Uploaded by

    akshanprakash12
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    2 views2 pages

    Experiment Chemical Kinetics

    Uploaded by

    akshanprakash12

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
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    VISHWA BHARATI PUBLIC SCHOOL, NOIDA

    CHEMISTRY PRACTICAL

    TOPIC: CHEMICAL KINETICS

    Aim: To study the effect of concentration on the rate of reaction between sodium thiosulphate and
    hydrochloric acid.

    Apparatus: Beaker (100 mL), measuring cylinder, Pipette (10 mL), Stop watch

    Theory: Sodium thiosulphate reacts with hydrochloric acid and produces a colloidal solution of
    sulphur, which makes the solution translucent. The reaction occurs as follows:

    Na2 S2O3 (aq) + 2HCl (aq) → 2NaCl (aq) + H2O(l) + SO2 (g) + S(s)

    The property of the colloidal solution of sulphur to make the system translucent is used to study the
    rate of precipitation of sulphur. The rate of precipitation of sulphur increases with an increase in the
    concentration of the reacting species. With an increase in the concentration, the number of
    molecular collisions per unit time between the reacting species increase and consequently chances
    of product formation increase.

    Procedure:

    (i) Take a trough and fill half of it with water. This will serve as constant temperature bath,
    maintained at room temperature.
    (ii) Rinse and fill the burette with 1.0 M HCl solution.
    (iii) Take a 100 mL beaker and make a mark ‘X’ in the centre of the outer surface of the
    bottom with the help of a glass marker pencil. Fill 50 mL of 0.1M sodium thiosulphate
    solution in it. Place the beaker in the trough. The mark ‘X’ will be visible to the naked eye
    on account of the transparent nature of the system. Allow the beaker to stand in the
    trough for a few minutes so that it attains the temperature of the bath.
    (iv) Add 10 mL of 1.0 M HCl solution. Start the stopwatch when half the HCl solution has
    been transferred. Swirl the beaker while adding HCl.
    (v) Record the time required for the mark ‘X’ on the bottom of the beaker to become
    invisible (This is considered as a stage of completion of the reaction).
    (vi) Repeat the experiment by adding 40 mL, 30 mL, 20 mL and 10 mL of acid solution to
    sodium thiosulphate solution and water making the solution 50 mL. Record the time
    required for the disappearance of the mark ‘X’ in each case separately.

    Precautions:

    (a) Start the stopwatch when half of the hydrochloric acid solution has been transferred to the
    reaction flask and stop the watch when the mark ‘X’ becomes invisible.

    (b) Select suitable scale for plotting the graph.

    Observation Table: (draw on left side)

    S.No. Volume of Volume of Conc. Of Volume of Time taken for the 1/t
    Na2S2O3 water(ml) Na2S2O3 1M HCl(ml) cross to disappear seconds
    1 10 40 0.02 M 10
    2 20 30 0.04 M 10
    3 30 20 0.06 M 10

    Vbpsnoida/ClassXII/Chemistry practical
    4 40 10 0.08 M 10
    5 50 nil 0.1 M 10

    Plat a graph between 1/t and concentration of Na2S2O3 by taking suitable scale (to be pasted on
    left side)

    Result: The rate of reaction is directly proportional to the concentration of the reacting species.

    Vbpsnoida/ClassXII/Chemistry practical

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