ISO-21809-1-2018
ISO-21809-1-2018
ISO-21809-1-2018
STANDARD 21809-1
Second edition
2018-10
Reference number
ISO 21809-1:2018(E)
© ISO 2018
ISO 21809-1:2018(E)
Contents Page
Foreword...........................................................................................................................................................................................................................................v
Introduction................................................................................................................................................................................................................................. vi
1 Scope.................................................................................................................................................................................................................................. 1
2 Normative references....................................................................................................................................................................................... 1
3 Terms and definitions...................................................................................................................................................................................... 3
4 Conformance.............................................................................................................................................................................................................. 6
4.1 Rounding....................................................................................................................................................................................................... 6
4.2 Compliance with this document............................................................................................................................................... 6
5 Symbols and abbreviated terms............................................................................................................................................................ 6
5.1 Symbols.......................................................................................................................................................................................................... 6
5.2 Abbreviations............................................................................................................................................................................................ 7
6 Information supplied by the purchaser........................................................................................................................................ 7
6.1 General information............................................................................................................................................................................ 7
6.2 Additional information..................................................................................................................................................................... 8
7 Coating classification........................................................................................................................................................................................ 9
7.1 General............................................................................................................................................................................................................ 9
7.2 Coating classes......................................................................................................................................................................................... 9
7.3 Coating thickness classes................................................................................................................................................................ 9
8
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Qualification processes...............................................................................................................................................................................10
8.1 (standards.iteh.ai)
General — Qualification scheme........................................................................................................................................... 10
8.2 Application procedure specification.................................................................................................................................. 11
8.3 Pre-production trial (PPT)ISO ..........................................................................................................................................................
21809-1:2018 12
8.4 Inspection and testing plan (ITP) .........................................................................................................................................
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8.5 Procedure qualification trial (PQT)
b33759eab454/iso-21809-1-2018 . . ................................................................................................................................... 13
9 Coating material qualification..............................................................................................................................................................13
9.1 Composition of the coating system..................................................................................................................................... 13
9.2 Qualification of the coating materials............................................................................................................................... 14
9.2.1 General requirements................................................................................................................................................ 14
9.2.2 Epoxy material................................................................................................................................................................. 14
9.2.3 Adhesive material......................................................................................................................................................... 15
9.2.4 PE/PP top layer material........................................................................................................................................ 15
9.3 Batch certificate................................................................................................................................................................................... 17
9.4 Storage and handling of coating materials................................................................................................................... 18
10 Coating system qualification..................................................................................................................................................................18
11 Application of the coating system.....................................................................................................................................................19
11.1 General......................................................................................................................................................................................................... 19
11.2 Surface preparation.......................................................................................................................................................................... 20
11.2.1 Initial preparation........................................................................................................................................................ 20
11.2.2 Abrasive blast cleaning — Cleanliness and surface roughness............................................. 20
11.2.3 Surface dust contamination................................................................................................................................. 20
11.2.4 Surface pre-treatment and salt contamination................................................................................... 21
11.3 Coating application........................................................................................................................................................................... 21
11.3.1 General................................................................................................................................................................................... 21
11.3.2 Epoxy application.......................................................................................................................................................... 21
11.3.3 Adhesive application.................................................................................................................................................. 21
11.3.4 PE/PP application......................................................................................................................................................... 22
11.3.5 Rough coat application............................................................................................................................................. 22
11.4 Cutback........................................................................................................................................................................................................ 22
12 Inspection and testing..................................................................................................................................................................................22
12.1 General......................................................................................................................................................................................................... 22
12.2 Re-testing................................................................................................................................................................................................... 25
13 Coating repairs.....................................................................................................................................................................................................25
14 Marking........................................................................................................................................................................................................................ 25
14.1 General......................................................................................................................................................................................................... 25
14.2 Required markings............................................................................................................................................................................ 26
15 Handling and storage in the applicator’s facilities.........................................................................................................26
15.1 Handling..................................................................................................................................................................................................... 26
15.2 Storage......................................................................................................................................................................................................... 26
16 Test reports and certificate of compliance..............................................................................................................................26
Annex A (normative) Inspection of thickness...........................................................................................................................................27
Annex B (normative) Holiday detection test..............................................................................................................................................29
Annex C (normative) Peel strength test...........................................................................................................................................................31
Annex D (normative) Thermal analysis of epoxy and cured epoxy coating film with Tg ≤ 115°C.......34
Annex E (normative) Impact test............................................................................................................................................................................39
Annex F (normative) Indentation test..............................................................................................................................................................41
Annex G (normative) UV ageing test and thermal ageing test.................................................................................................43
Annex H (normative) Cathodic disbondment test................................................................................................................................47
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Annex I (normative) Flexibility test....................................................................................................................................................................52
Annex J (normative) Gel time of the epoxy powder............................................................................................................................54
(standards.iteh.ai)
Annex K (normative) Total volatile/moisture content of the epoxy powder — Mass loss.........................56
Annex L (normative) Hot water immersion test ISO 21809-1:2018
.................................................................................................................................... 58
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Annex M (normative) Density of epoxy powder ..................................................................................................................................... 60
b33759eab454/iso-21809-1-2018
Bibliography.............................................................................................................................................................................................................................. 62
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www.iso.org/patents).
Any trade name used in this document is information given for the convenience of users and does not
constitute an endorsement.
For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and
expressions related to conformity assessment, as well as information about ISO's adherence to the
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World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT) see www.iso
.org/iso/foreword.html. (standards.iteh.ai)
This document was prepared by Technical Committee ISO/TC 67, Materials, equipment and offshore
structures for petroleum, petrochemicalISOand natural gas industries, Subcommittee SC 2, Pipeline
21809-1:2018
transportation systems.
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b33759eab454/iso-21809-1-2018
This second edition cancels and replaces the first edition (ISO 21809-1:2011), which has been technically
revised.
The main changes compared to the previous edition are as follows:
— adoption of qualification processes (Clause 8);
— added prescriptions for coating application on pipes made by corrosion resistant alloys (CRA) or
lined/clad internally with a CRA;
— cathodic disbondment test conditions revised.
A list of all parts in the ISO 21809 series can be found on the ISO website.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www.iso.org/members.html.
Introduction
It is necessary that users of this document be aware that further or differing requirements can be
required for individual applications. This document is not intended to inhibit a vendor from offering,
or the purchaser from accepting, alternative equipment or engineering solutions for the individual
application. This can be particularly applicable where there is innovative or developing technology.
Where an alternative is offered, it is the responsibility of the vendor to identify any variations from this
document and provide details.
1 Scope
This document specifies requirements for plant-applied external three-layer polyethylene and
polypropylene based coatings for corrosion protection of welded and seamless steel pipes for pipeline
transportation systems in the petroleum and natural gas industries in accordance with ISO 13623.
NOTE Pipes coated in accordance with this document are considered suitable for further protection by
means of cathodic protection.
2 Normative references
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The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
(standards.iteh.ai)
undated references, the latest edition of the referenced document (including any amendments) applies.
ISO 179-1, Plastics — Determination of Charpy impact properties — Part 1: Non-instrumented impact test
ISO 21809-1:2018
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ISO 179-2, Plastics — Determination of Charpy impact properties — Part 2: Instrumented impact test
b33759eab454/iso-21809-1-2018
ISO 306, Plastics — Thermoplastic materials — Determination of Vicat softening temperature (VST)
ISO 527-1, Plastics — Determination of tensile properties — Part 1: General principles
ISO 527-2, Plastics — Determination of tensile properties — Part 2: Test conditions for moulding and
extrusion plastics
ISO 868, Plastics and ebonite — Determination of indentation hardness by means of a durometer (Shore
hardness)
ISO 1133-1, Plastics — Determination of the melt mass-flow rate (MFR) and melt volume-flow rate (MVR)
of thermoplastics — Part 1: Standard method
ISO 1183 (all parts), Plastics — Methods for determining the density of non-cellular plastics
ISO 2808, Paints and varnishes — Determination of film thickness
ISO 2811 (all parts), Paint and varnishes — Determination of density
ISO 3183, Petroleum and natural gas industries — Steel pipe for pipeline transportation systems
ISO 3251, Paints, varnishes and plastics — Determination of non-volatile-matter content
ISO 4892-2:2013, Plastics — Methods of exposure to laboratory light sources — Part 2: Xenon-arc lamps
ISO 6964, Polyolefin pipes and fittings — Determination of carbon black content by calcination and
pyrolysis — Test method and basic specification
ISO 8130-2, Coating powders — Part 2: Determination of density by gas comparison pyknometer
(referee method)
ISO 8130-3, Coating powders — Part 3: Determination of density by liquid displacement pyknometer
ISO 8130-7, Coating powders — Part 7: Determination of loss of mass on stoving
ISO 8501-1:2007, Preparation of steel substrates before application of paints and related products —
Visual assessment of surface cleanliness — Part 1: Rust grades and preparation grades of uncoated steel
substrates and of steel substrates after overall removal of previous coatings
ISO 8502-3, Preparation of steel substrates before application of paints and related products — Tests for
the assessment of surface cleanliness — Part 3: Assessment of dust on steel surfaces prepared for painting
(pressure-sensitive tape method)
ISO 8502-6, Preparation of steel substrates before application of paints and related products — Tests for
the assessment of surface cleanliness — Part 6: Extraction of soluble contaminants for analysis — The
Bresle method
ISO 8502-9, Preparation of steel substrates before application of paints and related products — Tests for
the assessment of surface cleanliness — Part 9: Field method for the conductometric determination of
water-soluble salts
ISO 8503-4, Preparation of steel substrates before application of paints and related products — Surface
roughness characteristics of blast-cleaned steel substrates — Part 4: Method for the calibration of ISO
surface profile comparators and for the determination of surface profile — Stylus instrument procedure
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ISO 8503-5, Preparation of steel substrates before application of paints and related products — Surface
(standards.iteh.ai)
roughness characteristics of blast-cleaned steel substrates — Part 5: Replica tape method for the
determination of the surface profile
ISO 21809-1:2018
ISO 10350-1, Plastics — Acquisition and presentation of comparable single-point data — Part 1: Moulding
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materials b33759eab454/iso-21809-1-2018
ISO 10474:2013, Steel and steel products — Inspection documents
ISO 11124 (all parts), Preparation of steel substrates before application of paints and related products —
Specifications for metallic blast-cleaning abrasives
ISO 11126 (all parts), Preparation of steel substrates before application of paints and related products —
Specifications for non-metallic blast-cleaning abrasives
ISO 11357-2, Plastics — Differential scanning calorimetry (DSC) — Part 2: Determination of glass transition
temperature and glass transition step height
ISO 11357-6, Plastics — Differential scanning calorimetry (DSC) — Part 6: Determination of oxidation
induction time (isothermal OIT) and oxidation induction temperature (dynamic OIT)OIT) and oxidation
induction temperature (dynamic OIT)
ISO 15512, Plastics — Determination of water content
ISO 17855-2, Plastics — Polyethylene (PE) moulding and extrusion materials — Part 2: Preparation of test
specimens and determination of properties
ISO 18553, Method for the assessment of the degree of pigment or carbon black dispersion in polyolefin
pipes, fittings and compounds
ISO 19069-2, Plastics — Polypropylene (PP) moulding and extrusion materials — Part 2: Preparation of
test specimens and determination of properties
ISO 21809-2, Petroleum and natural gas industries — External coatings for buried or submerged pipelines
used in pipeline transportation systems — Part 2: Single layer fusion-bonded epoxy coatings
3.3
application procedure specification
APS
document describing procedures, methods, equipment and tools used for coating application
3.4
batch
quantity of material produced in a continuous manufacturing operation using raw materials of the
same source and grade
3.5
batch certificate
certificate of analysis issued by the manufacturer
1) Society for Protective Coating, 40 24th Street, 6th floor, Pittsburg; PA 15222-4656, USA.
3.6
certificate of compliance
document issued in accordance with ISO 10474 or EN 10204, stating compliance with the purchase
order for coated pipes, but without mention of any test results, issued in accordance with the purchasing
requirements
3.7
coating material qualification
qualification of the coating materials properties carried out by the manufacturer before the coating
system qualification
3.8
coating system qualification
qualification of application method, applied coating system and subsequent inspection/testing of its
properties, to confirm that the APS is adequate to produce a coating with the specified properties
Note 1 to entry: The coating system qualification is not project dependent.
3.9
cutback
length of pipe left uncoated at each end for joining purposes
3.10
design temperature range
temperature range, including maximum and minimum temperatures, likely to be reached during
transport, storage, handling, installation and operation
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Note 1 to entry: The design temperature range of the coating can be narrower than that specified for the steel
pipe material and/or the pipeline system. (standards.iteh.ai)
3.17
manufacturer's specification
document that specifies the characteristics, test requirements and application recommendations for
the coating materials
3.18
operating temperature
temperature that can be endured by a pipeline (component) and/or pipeline system during operation,
within the design temperature range
3.19
peel strength
force required for peeling the coating from the substrate
3.20
pipe diameter length
length along the pipe axis equal to the specified outside diameter of the pipe
3.21
pipeline
components of a pipeline system connected together to convey fluids between stations and/or plants,
including pipe, pig traps, components, appurtenances, isolating valves, and sectionalizing valves
[SOURCE: ISO 13623:2017, 3.1.15, modified]
3.22
pipeline system iTeh STANDARD PREVIEW
pipelines, stations, supervisory control and data acquisition system (SCADA), safety systems, corrosion
(standards.iteh.ai)
protection systems, and any other equipment, facility or building used in the transportation of fluids
[SOURCE: ISO 13623:2017, 3.1.16] ISO 21809-1:2018
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3.23 b33759eab454/iso-21809-1-2018
pre-production trial
PPT
application of a coating and subsequent inspection/testing of its properties, to confirm that the APS is
adequate to produce a coating with the specified properties, carried out in the coating plant immediately
prior to start of production and to verify that the plant's equipment is adequate to consistently adhere
to the APS requirements
3.24
procedure qualification trial
PQT
application of a coating and subsequent inspection/testing of its properties, to confirm that the APS is
adequate to produce a coating with the specified properties, carried out in correlation to a specific project
3.25
purchaser
company responsible for providing the purchase order requirements
3.26
start up
coating application activities re-start in case of modification of production parameters or unplanned
stoppage or production interruption exceeding 12 h
3.27
test report
document that provides the quantitative test results for tests conducted in accordance with the
requirements of this document
3.28
total coating thickness
sum of all three layers, namely epoxy material, adhesive material and top layer, with the exclusion of
rough coat, if applicable
4 Conformance
4.1 Rounding
Unless otherwise stated in this document, to determine conformance with the specified requirements,
observed or calculated values shall be rounded to the nearest unit in the last right-hand place of figures
used in expressing the limiting value, in accordance with ISO 80000-1.
NOTE For the purpose of this provision, the rounding method of ASTM E29 is equivalent to ISO 80000-1.
The applicator shall be responsible for complying with all the applicable requirements of this document.
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The purchaser shall be allowed to make any investigations necessary to ensure compliance by the
applicator and to reject any material and/or coating that does not comply.
(standards.iteh.ai)
5 Symbols and abbreviated terms ISO 21809-1:2018
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5.1 Symbols b33759eab454/iso-21809-1-2018
Pm mass of bare pipe per metre length, expressed in kilograms per metre
ΔTg difference in the glass transition temperature between two successive thermal analysis
scans, expressed in degrees Celsius
5.2 Abbreviations
Cr chromium
IR infrared
LDPE (standards.iteh.ai)
low-density polyethylene
PE polyethylene
PP polypropylene
UV ultraviolet
b) pipe quantity, outside diameter, minimum wall thickness, minimum, maximum and nominal length,
grade of steel;
c) bare pipe standard or specification designation, e.g. ISO 3183;
d) design temperature range in accordance with 7.2;
e) operating temperature;
f) coating class and coating thickness class in accordance with 7.2 and 7.3;
g) qualification scheme as defined in 8.1;
h) minimum number of coated pipes to be used for PPT and PQT (if required);
i) cutback configuration and finish (length, angle, visible epoxy, temporary protection, etc.) (see 11.4);
j) type of certificate of compliance (see 16).
t) coating and cutback preservation and protection against adverse ambient conditions during
storage (e.g. UV protection, additional cutback preparation, end-caps) (see 15.2);
u) identification of pipes to be used for PPT (see 8.3).
If further installation processes (e.g. welding processes and field joint coating application) that
envisage the heating of the coated pipe are needed, further testing (e.g. adhesion) may be considered
by the purchaser in order to assess the compatibility of the line pipe coating against the application
parameters of the chosen field joint coating and vice-versa.
7 Coating classification
7.1 General
The coating class shall be selected based on the design temperature range and expected field duty.
The coating thickness class shall be selected based on transport, handling, laying conditions and the
expected operating and environmental conditions.
Coating classes B or C can be selected because of higher mechanical properties for project or specific
laying purposes rather than maximum operating temperatures listed in Table 1.
The use of coating classes outside these guidelines is acceptable provided that the applied coating shall
be tested against the requirements specified in Table 7 for each relevant class (i.e. class B shall be tested
against requirements for class B in Table 7, class C shall be tested against requirements for class C in
Table 7).
Different requirements for coating materials outside these classification systems shall be agreed upon
by the applicator and purchaser.
Use of coating classes outside these guidelines shall be approved by the purchaser or end user.