Report: Experiment 1

PREPARATION OF SODIUM CHLORIDE FOR

MEDICINAL PURPOSES

Student's name: Group: Class: Course:

Lecturer: Date:

1. Product description sodium chloride

2. Chemical equations

3. Materials used
Material Quantity of substances Mole Notes

4. Diagram of equipment and tools

5. The steps taken

6. Summary of results

7. Comments and conclusions

8. Lecturer's comments:

Signature: Lecturer Lab’s Staff Student

Report: Experiment 2

RUTIN EXTRACT FROM

STYPHNOLOBIUM JAPONICUM L.
Student's name: Group: Class: Course:

Lecturer: Date:

1. Description of rutin finished product

2. Chemical equations

3. Materials used
Material Quantity of substances Mole Notes
Styphnolobium japonicum L.
(buds and flowers)
Ethanol
n-butanol
Acetic acid
NaOH 20%
FeCl3 5%
Activated carbon
4. Diagram of equipment and tools

5. The steps taken

6. Summary of results

7. Comments and conclusions

8. Lecturer's comments:

Signature: Lecturer Lab’s Staff Student

Report: Experiment 3

ANALYSIS OF RUTIN USING THIN LAYER

CHROMATOGRAPHY

Student's name: Group: Class: Course:

Lecturer: Date:

1. Description of rutin finished product

2. Materials used
Material Quantity Mole Notes
Rutin
Ethanol
n-butanol
Acetic acid
NaOH 20%
FeCl3 5%
Activated carbon
4. Diagram of equipment and tools

5. The steps taken

6. Summary of results

7. Comments and conclusions

8. Lecturer's comments:

Signature: Lecturer Lab’s Staff Student

Report: Experiment 4

SYNTHESIS OF METHYL SALICYLATE

Student's name: Group: Class: Course:

Lecturer: Date:

1. Description of methyl salicylate finished product

2. Chemical equations

3. Materials used
Material Property Quantity Mole Notes
Anhydrous salicylic acid
Methanol
Sulphuric acid 98%

4. Diagrams of equipment and tools.

5. The steps taken

6. Summary of results

Results Weight (g) Performance (%)

According to theory
Experimental results

7. Comments and conclusions

8. Lecturer's comments:

Signature: Lecturer Lab’s Staff Student

Report: Experiment 5

PURIFICATION OF METHYL SALICYLATE

Student's name: Group: Class: Course:

Lecturer: Date:

1. Description of methyl salicylate finished product

2. Chemical equations

3. Materials used
Material Property Quantity Mole Notes
NaHCO3 10%
Na2SO4 khan

4. Diagrams of equipment and tools.

5. The steps taken

6. Summary of results

Results Weight (g) Performance (%)

According to theory
Experimental results

7. Comments and conclusions

8. Lecturer's comments:

Signature: Lecturer Lab’s Staff Student

Report: Experiment 6
SYNTHESIS OF DIETHYPHTALATE

Student's name: Group: Class: Course:

Lecturer: Date:

1. Description of diethylphtalate finished product

2. Chemical equations

3. Materials used
Material Property Quantity Mole Notes
Anhidrit phthalic
Ethanol
Sulphuric acid 98%

4. Diagrams of equipment and tools.

5. The steps taken

6. Summary of results

Results table
Result Weight (g) Performance (%)
According to theory
Experimental results

7. Comments and conclusions

8. Lecturer's comments:

Signature: Lecturer Lab’s Staff Student

Report: Experiment 7
PURIFICATION OF DIETHYPHTALATE

Student's name: Group: Class: Course:

Lecturer: Date:

1. Description of diethylphtalate finished product

2. Chemical equations

3. Materials used
Material Property Quantity Mole Notes
Na2CO3 saturated
Na2SO4 anhydrous

4. Diagrams of equipment and tools.

5. The steps taken

6. Summary of results

Results table
Result Weight (g) Performance (%)
According to theory
Experimental results

7. Comments and conclusions

8. Lecturer's comments:

Signature: Lecturer Lab’s Staff Student

Report: Experiment 8
SYNTHESIS OF P-NITROSOPHENOL
Student's name: Group: Class: Course:

Lecturer: Date:

1. Description of finished product p-nitrosophenol

2. Chemical equations

3. Materials used
Material Property Quantity Mole Notes
Phenol
Sodium nitrite
Sulphuric acid 22%

4. Diagrams of equipment and tools.

5. The steps taken

6. Summary of results

Results table
Result Weight (g) Performance (%)
According to theory
Experimental results

7. Comments and conclusions

8. Lecturer's comments:

Signature: Lecturer Lab’s Staff Student

Report: Experiment 9

SYNTHESIS OF P-AMINOPHENOL

Student's name: Group: Class: Course:

Lecturer: Date:

1. Description of the p-aminophenol finished product

2. Chemical equations

3. Materials used
Material Property Quantity Mol Notes
Sulphuric acid 10%
p-nitrosophenol
Sulfur powder
Solid NaOH

4. Diagrams of equipment and tools.

5. The steps taken

6. Summary of results

Results
Results Volume (g) Performance (%)
According to theory
Experimental results

7. Comments and conclusions

8. Lecturer's comments:

Signature: Lecturer Lab’s Staff Student

Report: Experiment 10
SYNTHESIS OF PARACETAMOL

Student's name: Nest: Class: Lock:

Teacher instructed: Date:

1. Description of paracetamol finished products

2. Chemical equations

3. Materials used
Material Property Quantity Mol Notes
p-aminophenol
Anhydrite acetic
Activated carbon

4. Diagrams of equipment and tools.

5. The steps taken

6. Summary of results

Results table
Results Weight (g) Performance (%)
According to theory
Experimental results

7. Comments and conclusions

8. Lecturer's comments:

Signature: Lecturer Lab’s Staff Student