Laboratory Manual material science and testing
Laboratory Manual material science and testing
1 Construction
Material and Testing Laboratory
Experiment
__________________________
Student
_________________________________________________
Instructor
Name : _______________________ Course & Year: _______________
Instructor : ____________________ Offer # : ________________
TABLE OF CONTENTS
9 Blending of Aggregates
11 Fineness of Cement
15 Testing of Concrete
20 Testing of Wood
AVERAGE
St. Peter’s College
Iligan City
I. Experiment # 1
III. Objective :
IV. Theory:
V. Apparatus:
A hydraulic testing machine and its accessories
VI. Procedure:
1. The main parts of the testing machine will be indicated to the class, then the
operation of the machine will be explained.
2. Compression and tension tests will be demonstrated. The dimensions of the
specimens shall be measured prior to testing.
3. The force at the breaking point of the specimens shall be measured.
Load is applied by pumping oil from the reservoir to the cylinder, with
the loading valve open and the unloading valve closed. The ram on top of the
cylinder is driven upwards.Attached to the ram is the worktable which carries the
two compression columns and the top platen. Between the worktable and the top
platen is the sensitive platen. Therefore when a force is applied to the cylinder, a
sample is placed below the sensitive platen will be compressed by the upward
movement of the top platen. In either case, the force on the sensitive
platen is in upward direction.
1
The screw columns and the bottom platen in the base of the machine
transmit the force to the capsule. Mounted between the bottom platen and the
cylinder.
The copper tube from the capsule loads to the sensitive elements of the
indicator - three bourdon tubes in the upper half of the cabinet. Any
movement of these tubes is opposed by an independent force which derives its
power from air line. The instant, the two forces are not exactly balanced
the independent force automatically operates to produce balance.The magnitude
of the independent force determines the indication of the dial.
A decrease in load causes the free end of the Bourdon tube and the baffle
to fall, which restricts the flow of air from the pipe line.the air pressure in
the system is increased., the bellows inflate and move upward.Tension on the
isosclastic spring is reduced and consequently, the free end of the Bourdon
tube and baffle rise to the original position.
Forming the top of the bellows is an L- shaped unit with gear teeth
engaged to a pinion. Thus movement of the bellows causes the pointer to rotate on
the scale. The angular displacement of the pointer on the scale is directly
proportional to the stretch of the isosclastic spring.
Air enter through the supply valve after passing through the filter. If then
passes an air pressure regulator so that the pressure of the air delivered
as 25 psi as indicated by the gage on the panel. The air then passes through an
orifice union which regulates the flow to the jets and bellows.
The unit consists of a radial piston pump and differential device which by
varying the displacement of the pump, maintain an instant speed of the ram, any
leakage past the main cylinder packing and any internal pump leakage. The
differential device is essentially a two chamber unit separated by a flexural
diaphragm. One chamber is connected to the pump oil pressure and the other side
to the cylinder oil pressure. Any change in pressure in the cylinder or in the
pump will result in movement of the diaphragm. Since the diaphragm is
connected to the pump plunger, this movement will vary the eccentricity of the
pump and hence its displacement, thereby tending to equalize the forces against
the diaphragm.
2
VII. Operation
A. Compression
B. Tension
1. Set sensitive platen to position which will give desired tension space. If
necessary the top platen may also be moved.
2. Insert pinion shaft which operate s the grips in top platen.Screw the L-
shaped steps in top of grips, lower grips, lower grips in top platen. Level grips by
pushing in or pulling out the pinion shaft and tighten set- screw to hold
adjustment.Depending on size of specimen, introduce liner plates in pairs of same
thickness so that at start of test, lower ends of wedge grips are about 12 inch above
the lower surface of the top platen.
3. Arrange grips and liners in the sensitive platen in same way as in top platen so
that top ends grips are about 1/2 inch below the top surface.
4. Insert specimen in top platen, using care that a full bite on the
specimen is obtained.
5. Raise sensitive platen until its grips are in a position to bite the
greatest possible area of the specimen.
6. Set grips tight with handles on opinion shafts and start test as
describe under Compression. As soon as load starts to increase, remove
handles. At breakage close control valve and open release valve.
C. Flexure
3
4
Saint Peter’s College
Iligan City
Offer # Rating
I. Experiment # 2
III. Objective :
IV. Theory :
V. Apparatus :
VI. Procedure :
3. Mix the sample by shoveling from the bottom of the pile to the top of the
cone allowing the material to run down equally in all directions.
4. Spread the cone into a flat circular pile by drawing the material from the
center outward with the shovel until it spread to an even thickness.
5. Divide the flat pile into quarters and two diagonally opposite quarters
rejected.
6. Mix the remaining quarters and the process of piling, flattening and
rejecting two quarters repeated until the sample is reduced to the desired size.
VII. Discussion :
1. What would be the criterion in judging whether the quartering process has
5
Saint Peter’s College
Iligan City
Offer # Rating
I. Experiment # 3
III. Objective :
IV. Theory :
V. Apparatus :
Balance
Container
Oven
VI. Procedure :
VII. Calculation:
VIII. Discussion :
6
Saint Peter’s College
Iligan City
Name Date
Performed
Offer # Rating
I. Experiment # 4
III. Objective :
IV. Theory :
V. Apparatus :
VI. Procedure:
1. Determine by wash test the material finer than No. 200 sieve.
2. Made the sieve analysis of the material coarser than the No. 200 sieve.
3. Dry the wash aggregate to constant weight and then separate over the various
sieves.
4. Conduct the sieving operation by means of a lateral and vertical motion of the
sieve, accompanied by jarring action so as to keep the sample moving continuously
over the sieve.
5. Continue sieving till not more than 1% of the residue passes any sieve during
one minute.
6. Determine the weight of material retained on each sieve and from this the
percentage passing shall be based on the weight of the material before
washing.
7. Plot on the graph of Mechanical Analysis the percentage passing each size
and a smooth curve drawn connecting the plotted points.
8. The percentage passing sieve sizes quoted in the specifications but not
available during the test shall be taken from this curve and reported.
VII. Calculation:
7
% Passing = Cumulative Weight Passing x 100
Total Weight of Sample Test
IX. Discussion :
8
Saint Peter’s College
Iligan City
Name Date
Performed
Offer # Rating
I. Experiment # 5
II. Title : Unit Weight Determination for Fine and Coarse Aggregates
III. Objective :
IV. Theory :
V. Apparatus :
VI. Procedure :
1. Fill one third of the measure level and tamp 25 times evenly distributed
over the surface.
2. Fill two thirds of the measure, then to over-flowing. Each time the same
procedure as in step (1) is separated.
3. In tamping the rod should penetrate only the layer being tamped and
should not be forced into the bottom of measure or last layer placed.
4. Strike-off the excess aggregate with tamping rod.
5. Get net weight of aggregate in measure. Compute unit weight by dividing
the net weight by the volume measure.
9
1. Fill volumetric measure to overflowing by means of a shovel or scoop.
Discharge the aggregate from a height of about 2 inches from top of the
measure. Exercise care to prevent aggregation of particles sizes.
2. Level-off carefully surface of aggregate.
3. Get net weight of aggregate and compute unit weight by dividing net
weight by volume of measure
LOOSE COMPACT
1. Container + Sample, Kg Sand Gravel Sand Gravel
2. Container, Kg
3. Sample, Kg (1) - (2)
4. Volume of Container , m3
5. Unit Weight, Kg/m3,(3) / (4)
VIII. Discussion
10
Saint Peter’s College
Iligan City
Name Date
Performed
Offer # Rating
I Experiment # 6
III Objective :
IV Theory :
V Apparatus :
VI Procedure:
1. Pass the dried sample of proper size without washing through available sieves.
2. Determine the weight retained on each sieve.
3. Calculate the percentage passing each size on the basis of the total weight of the
dried samples.
4. Plot the percentages passing each size on the “Graph of Mechanical
Analysis” and from the resulting curve the percentages passing sieve sizes quoted
in the specifications but not used in the test shall be obtained.
11
Sieve Size Weight Cum. Percent Spec. % Remarks
Retained Weight Passing Passing
Passing
2”
1 - 1/2”
1”
3/4”
3/8”
No. 4
No. 16
No. 200
Pan
Total
VIII Discussion :
12
Saint Peter’s College
Iligan City
Date
Name Performed
Instructors
Course & Year Signature
Offer # Rating
I. Experiment # 7
III. Objective :
IV. Theory:
V. Apparatus:
VI. Procedure :
1. Filled the 12 oz bottle to the 4 1/2 oz mark with the sand to be tested.
2. Add 3% solution of sodium hydroxide until sand and liquid reaches
the 7 oz mark
3. Stopper, shake, and allow the bottle to stand 24 hours.
4. Compare the color of the clean liquid above the sample after standing 24
hours, with the glass standard with a solution prepared by adding 2.5 ml of a 2%
solution tannic acid in 10% alcohol to 97.5 ml of a 3% sodium hydroxide solution.
5. Report solutions darker in color than this standard as having an organic test
value of more than 500 ppm. In terms of tannic acid.
VII. Discussion :
13
Iligan City
Name Date
Performed
Course & Year Instructors
Signature
Offer # Rating
I. Experiment # 8
III. Objective :
IV. Theory :
The percent passing the No. 200 sieve in an indication cleanliness of the
aggregate. Test determine the silt and clay components which may weaken
concrete if adhering to the aggregate grains. Specifications limit the fines
removed by the No. 200 sieve to 3% in fine aggregate and 1 - 1/2 in coarse
aggregate.
V. Apparatus :
VI. Procedure :
1. Dry the test sample to constant weight at a temperature of about 1050 C ; weight
sample after cooling to room temperature.
2. Place sample in a container large enough to permit vigorous agitation
without spilling when water is added.
3. Add water and agitate.
4. Pour wash water over the nested sieves No.10 over No. 200 sieve,
avoiding decantation of coarse particle. Repeat operation until wash water
is clear.
5. Dry sample to constant weight after cooling to room temperature.
VII. Calculation:
VIII. Discussion:
14
Iligan City
Name Date
Performed
Offer # Rating
I. Experiment # 9
III. Objectives :
IV. Theory :
If the aggregate from one source does not meet grinding specification
blending with other aggregates may be tried in order to meet the grinding
specification.
V. Apparatus :
VI. Procedure :
VII. Discussion :
15
% Passing
Sieve Size
Specs Limit Course Aggregates Fine Aggregates
2”
1 1/2’
1”
3/4”
3/8”
#4
# 40
# 50
# 100
# 200
Table 1
Table 2
Table 3
IX. Conclusion:
16
Iligan City
Name Date
Performed
Offer # Rating
I. Experiment # 10
III. Objectives :
IV. Theory :
Values are used in the design of concrete and bituminous mixtures. A high
value of absorption may indicate a doubtful quality of the material.
V. Apparatus :
VI. Procedure :
1. Hold the mold firmly on a smooth non absorbent surface with the large
diameter down.
2. Place a portion of the partially dried fine aggregate loosely in the mold by
filling it to overflow.
3. Lightly tamp with 25 drops at the height of about 5 mm above the top
surface.
4. Lift the mold vertically if the fine aggregate slumps slightly it indicates
that it reaches its saturated surface dry.
17
Fine Aggregates
1. Prior to test the weight of pycnometer filled with water should be obtained , air
should be expelled by rolling on side or boiling.
2. Soak about 1000g of the sample in water for 24 hours.
3. Spread sample on a flat surface and stir frequently until it approaches a free
flowing condition.
4. Place sample in a conical mold tamp surface 25 times and lift mold
vertically. Sample in the cone will retain its shape in the presence of free
moisture. If this condition exists, continue drying and repeat the test until the
sample slumps upon removal of the mold. This will indicate a surface dry condition.
5. Weigh 500 grams of the surface dry sample and place in the pycnometer.
6. Fill pycnometer with water and roll on a flat surface to remove air bubbles.
Then place in a water bath maintained at 200C for about 1 hour.
7. Fill pycnometer to 500 ml mark and weigh.
8. Remove sample from pycnometer and dry to constant weight.
9. Get oven dry weight.
VII. Calculation :
A. Fine Aggregates
% Absorption = ( W1 - W0 / W0 ) x 100
Where:
W0 = weight in air of oven dry sample
W1 = weight in air of saturated surface dry sample
W2 = weight of pycnometer filled with water
W3 = weight of pycnometer + water + sample in bottle
Coarse Aggregate :
1. Pass about 5 kg. Of the sample through a 3/8” sieve reject portion passing.
2. Wash portion retained to remove dust or other coating and soak in water at
200C for 24 hours.
3. Remove sample from water and wipe all visible films of water with an
absorbent cloth. Sample is now in surface-dry condition.
4. Weigh surface dry sample in air.
5. Place sample in wire basket and determine weight in water.
6. Dry sample to constant weight.
7. Get oven dry weight.
Calculations :
B. Coarse Aggregates
Where:
W0 = weight in air of oven dry sample
W1 = weight in air of saturated surface dry sample
W2 = weight of pycnometer filled with water
W3 = weight of pycnometer + water + sample in bottle
18
Fine Aggregate
1. Sample, O.D. in air, g
2. Sample, SSD in air, g
3. Pyc. + water , g
4. Pyc. + water + sample , g
5. S.G. ( Bulk SSD ) , 2/(2) + (3) - (4)
6. Absorption, % (2) - (1) / (1)
Fine Aggregate
1. Sample, O.D. in air, g
2.Sample, SSD in air, g
3.Weight sample in water
4.Pyc. + water + sample , g
5.S.G. ( Bulk SSD ) , 2/(2) - (3)
6.Absorption, % (2) - (1) / (1)
IX. Discussion :
19
Name Date
Performed
Offer # Rating
I. Experiment # 11
III. Objective :
To determine the fineness of Portland cement by the use of the No. 200
sieve.
IV. Theory :
The coarse particles in cement are inert. The finer the cement the faster it
will undergo hydration, thus resulting in higher early strength and more
rapid generation of heat. The effects of higher fineness is manifested principally
during the early periods of hydration although at later ages finer cement will give
higher strength. Coarse cement tend to give poor concrete workability and cause
excessive bleeding. Bleeding is manifested by water rising to the top of
the concrete due to settlement of solids before initial set. Greater fineness.
Improves not only the strength but also water tightness, workability,
appearance and durability of concrete. The test for fineness by the # 200
sieve consists of passing 50 grams of the cement through this sieve and
weighing the residue. In the turbidimeter test also for fineness determination, light is
made to pass through suspension of cement in water-free kerosene in a glass tank. From
the intensity of the light passing through the suspension the fineness is calculated
in terms of specific surface per gram of cement.
V. Apparatus:
VI. Procedure:
20
1. Place 50 grams sample of cement on # 200 sieve with pan attached.
2. Continue sieving until the residue clean for about 10 minutes
3. Place the cover on the sieve and remove the pan.
4. Brush off the dust adhering to the under side of the sieve.
5. Conduct one minute test to determine the completeness of sieving.
6. Held in an inclined position in one hand the sieve with pan and cover
attached and struck against the other hand gently about 150 times in one
minute.
7. Rotate the sieve about one sixth of a revolution after every 25 strokes.
8. Continue sieving until not more than 0.05 grams passes in one minute of
continuous sieving.
9. Weigh the residue in the sieve when the sieving is completed.
10. Brush thoroughly the sieve cloth on both sides to remove all the residue from
the sieve.
VII. Calculation :
VIII. Discussion :
IX. Conclusion :
21
Name Date
Performed
Offer # Rating
I. Experiment # 12
III. Objectives :
IV. Theory :
V. Apparatus :
1. Le Chatelier Flask
2. Water - Free Kerosene
3. Balance and Weights
VI. Procedure :
1. Fill Le Chatelier flask with water free kerosene to a point on the stem
between the zero and 1 - ml mark.
2. Immerse the flask in a constant temperature for a sufficient time interval before
making any reading.
3. Take initial reading.
4. Introduce into the flask the cement sample, about 64 grams.
5. Stopper the flask and roll in an inclined position until no air bubbles rise
into the surface.
6. Immerse in water bath the final reading.
VII. Calculation :
22
S.G = Wc (g)
(Rf - Ri) ml
Where :
Wc = Weight of Cement (grams)
Rf = Final Reading ( ml )
Ri = Initial Reading ( ml )
VIII. Discussion :
23
Name Date
Performed
Offer # Rating
I. Experiment # 13
III. Objective :
IV. Apparatus :
1. Vicat Needle
2. Glass Plate
3. Graduated Cylinder
4. Balance
V. Procedure :
1. Place a 500 grams sample of cement in a mound and form in the center a crater.
2. Poured into the crater a measure quantity of water.
3. Turn into the crater the cement on the outer edge within 30 seconds with a trowel.
4. Allow another 30 seconds for absorption of water.
5. Mix the material with gloved hands for 1 1/2 minutes in a continuous
mixing, kneading and squeezing operation.
6. Formed the cement paste into a ball and tossed from one hand to the other 6 times
the hand being kept 6” apart.
7. Pressed the ball into the larger end of the conical ring of the Vicat Apparatus.
8. Cut off the excess paste at the larger end with the palm of the hand and place
the ring on its larger end on a glass plate
9. Cut off the excess paste at the smaller end of the ring with one stroke of the
trowel.
10. Place the mold under the plunger end of the Vicat apparatus and the
penetration 30 sec after release of the plunger determined.
11. The paste shall be of normal consistency when the rod penetrates 10 mm below
the surface in 30 sec.
12. Paste of different percentages of water shall be fried until the normal
consistency is obtained.
VI. Calculation :
24
500
VII. Tabulated :
Final Reading ,
Weight of Cement Volume of Water Vicat Needle
Penetration
VIII. Discussion :
IX. Conclusion :
25
Name Date
Performed
Offer # Rating
I. Experiment # 14
III. Objective :
IV. Given :
V. Required :
VI. Computation:
26
Saint Peter’s College
Iligan City
27
Name Date
Performed
Offer # Rating
I. Experiment # 15
III. Objective :
IV. Theory :
V. Apparatus :
A. Slump Test
1. Slump mold galvanized metal # 16 gage in the form of the lateral surface of the
frustrum of a cone with the base 8 inches dia. Top 4 inches dia. And height 12
inches.
2. Tamping rod, steel 5/8” dia. 24 inches long and tapered to a distance of
one inch to spherically shaped end.
3. Container for mixing concrete sample
4. Scoop or shovel
5. Steel ruler
B. Strength Tests
28
1. Compression cylindrical molds 6 inches in diameter and 12 inches in
height.
2. Flexure beam molds, 6 inches by 6 inches in cross section and 21 inches
length
3. Standard tamping rod
4. Container for mixing sample
5. Scoop or shovel
6. Mason’s trowel
7. Capping material and facilities
8. Curing facilities
9. Universal testing machine
VI. Procedure :
A. Slump Test
1. Obtain a representative sample from entire batch. If from a mixer pass a scoop
or pail repeatedly through the flowing discharge of concrete starting at the beginning of
discharge and repeated until entire batch is discharged. During paving operations, obtain
the sample from the batch immediately after depositing on the sub- grade. Take at
least five samples from different portions of the pile. Bring the composite sample
thus obtained to the place of molding the specimen. To prevent segregation mix
the concrete again until it is uniform in appearance.
2. Dampen the mold and place on a flat moist and non-absorbent surface from
the sample of concrete obtained, fill immediately the mold in 3 layers each layer
approximately 1/3 of the volume of the mold. In placing each scoop of concrete
move scoop around top edge of mold as the concrete slides. Tamp each layer with
25 strokes distributed uniformly over the surface. The rod should penetrate the
entire depth of the layer being tamped. After the top layer has been rodded, strike
off the surface with a trowel so that the mold is exactly filled.
3. Remove immediately the mold from the concrete by raising it slowly and
carefully in a vertical direction.
4. Measure immediately the slump by getting the difference between the height of
mold and the height of the vertical axis of the slumped concrete.
5. Record the consistency in terms of inches of subsidence of the specimen
during the test, which is known as the slump.
6. After the slump measurement tamp gently the side of the slumped
specimen with the tamping rod. The behavior of the concrete under this
treatment is a valuable indication of workability of the mix. A workable mix will
gradually slump and retain its original identity, while a poor mix will crumble and
segregate.
B. Compression test:
29
2. The rod should penetrate the entire depth of the layer being
tamped. Tap sides of the mold if voids are left by tamping rod. After
the top layer has been rodded strike off the surface with a trowel
and cover with a plate or damp material that will prevent evaporation.
3. After 24 hours remove specimen from mold and cure until the time
of test. Curing means to store specimen in a moist condition at
temperature range of 18 to 24 0C. Specimen shall not be exposed to
running water.
4. Prior to testing, cap the ends of the specimen with suitable material
to make ends approximately at right angles to the axis of cylinder.
The cap shall be as thin as possible.
5. Determine the average diameter by measuring two diameters at
right angles to each other near the center of height of specimen.
Measure also height of specimen including caps.
6. Place the specimen, which is in a moist condition, on the working
table of testing machine. Center specimen by aligning carefully
with the center of spherically seated block of middle platen. As the
block is brought to bear on top of specimen, rotate gently movable
portion to obtain a uniform seating.
7. Apply load at a constant rate within the range of 20 to 50 psi per
second. Increase load until specimen fails.
8. Record the maximum load carried by specimen.
C. Flexure Test
VII. Calculations :
R = PL/ bd2
Where:
R= modulus of rupture, psi
P= maximum load, lb
L= span, in
30
b= average width, in
D= average depth, in
b. If the fracture is outside of the middle third of the span length by not more than
5% of the span length, calculate the modulus of rupture by the formula:
R = 3 Pa / bd2
Where :
a = distance between line of fracture and the nearest
support measured along the center line of
the bottom of the beam, in inch
c. If fracture is outside of cases (a) and (b), discard the result of the test.
A. Slump Test
1. Slump, in
2. Description of mix after tapping slumped specimen
B. Compression Test
1. Age, days
2. Height , mm
3. Diameter, mm (a)
(b)
4. Ave. Diameter, mm, (3a) + (3B) / 2
5. Area, sq mm
6. Max. Load, kg
7. Compressive Strength , MPa, (6) / (5)
C. Flexure Test
1. Age, days
2. Width, mm (a)
(b)
3. Average Width, mm (2a) + (2b) / 2
4. Depth, mm (a)
(b)
5. Average depth (4a) + (4b) / 2
6. Span Length, mm
7. Max Load, kg
8. Location of Fracture ( check )
a. Within middle third of span
b. Outside middle third, less than 5% of span
c. Outside middle third, more than 50% of span
9. If case (8b) distance of fracture to nearest support, mm
10. Modulus of Rupture, MPa, ( use appropriate formula)
IX. Discussion:
31
Saint Peter’s College
Iligan City
Name Date
Performed
32
Offer # Rating
I. Experiment # 16
III. Objective :
IV. Apparatus :
Weighing Balance
Straight Edge
Wood, 14.5 cm x 1.9 cm x 2.2 cm
V. Procedure :
VI. Discussion :
VII. Calculation :
33
VIII. Conclusion :
Name Date
Performed
34
Offer # Rating
I. Experiment # 17
III. Objective :
IV. Apparatus :
V. Procedure :
35
the same manner as the concrete in the structure. After 24 hours, the
specimens shall be taken in the molds to a location preferably near the
field laboratory, removed from the molds and stored up near by placing
them on the ground as molded, with their top surfaces up. The sides and
ends shall then be banked with damp earth or sand which shall be kept
damp, leaving the top surfaces exposed to the specified curing treatment.
At the end of the curing period the specimens shall be left in place with
the top surfaces exposed to the weather in the same manner as the
structure. Specimens shall be tested in the moist condition resulting from
the specified curing treatment.
VI. Discussion
Name Date
Performed
36
Signature
Offer # Rating
I. Experiment # 18
III. Objective :
IV. Apparatus :
Weighing Balance
Straight Edge
Wood 2 cm x 2 cm x 13 cm
Glass Cylinder
V. Procedure :
VI. Discussion :
37
Name Date
Performed
Offer # Rating
I. Experiment # 19
III. Objective :
IV. Theory :
V. Apparatus :
1. Compression Machine
2. Capping Material ( cement - gypsum or sulfur - fillr )
3. Bearing Blocks, hardened metal
4. Steel Plate, surfaces machined to true planes
5. Oven
6. Container for saturating samples
7. Steel tape measure
VI. Procedure :
Sampling :
Five (5) full size units shall be tested for compressive strength
within 72 hours after delivery to the laboratory. Five full sized units shall
be tested for absorption and moisture content, and shall be weighed
immediately after sampling and marking.
38
2. Cap the bearing surface of the strength test units by using either
cement gypsum or sulfur-filler capping material. The
average thickness of the cap shall be not more than 1/8” .
The axis of the specimen shall be perpendicular to the
surface of cap. The unit shall remain undisturbed until
solidification of the capping material is complete. A minimum of 2
hours shall be allowed for the caps to cool before testing.
3. Set the specimen on the lower bearing block and center it beneath
the upper bearing block. The position of the specimen shall
be the same position in service the upper bearing shall be
spherically seated hardened metal block firmly attached at the
center of the sensitive platen of the universal testing machine. If
the bearing area is not sufficient to cover the area of the
specimen, a steel plate shall be placed between the spherical
bearing block and the capped specimen. A hardened metal bearing block
and the capped specimen. A hardened metal bearing block
shall be used beneath the specimen to minimize wear of the lower
platen.
4. Apply the load at a uniform rate until failure occurs. Record the
maximum load.
5. Calculate the compressive strength by dividing the maximum load
in kgs. By the cross sectional of the unit in square meter. The gross
area of the unit is the total area of a section perpendicular to the
direction of the load, including area within the cells.
1. Dry the specimen in a ventilating oven at 110 to 1150C for not less than 2
1/2 hours to constant weight. Get the dry weight.
2. Immerse completely the test specimen’s in water at room temperature of
60 to 80 degrees Celsius for 24 hours.
3. Weigh the specimen completely submerge in water suspended with a metal
wire.
4. Remove specimens from the water and allow to drain for 1 minute by
placing on a coarse mesh wire. Wipe visible surface water with damp cloth.
Weigh immediately.
5. Calculate the absorption by the following formula.
The results of the strength absorption and moisture content tests are
compared with the requirements in Table 1.0, to determine the
acceptability of the units represented by the samples.
39
Masonry Units Kind : ________________
1. Nominal Size
2. Gross Area
3. Identification a b c d e
4. Ultimate Comp. Load, lb
5. Ultimate Comp. Strength, psi 4/2
6. Ave. Comp. Strength, psi
7. Sampled Weight, g
8. Dry Weight, g
9. Suspended Immersion Wt., g
10. Wet weight, g
11. Abs. pcf (10)- (8)/ (10) - (9) x 62.4 pcf
12. Abs., % (10)-(8) / (8) x 100
13. Moist Cont., % of Abs.
(7)-(8) / (10)-(8) x 100
14. Ave. Absorption, pcf
15. Ave., Absorption, %
16. Ave. Moisture Cont, % of Abs
17. Conclusion
VIII. Discussion :
1. What are the significance of the strength and absorption test in CHB ?
40
Name Date
Performed
Offer # Rating
I. Experiment # 20
III.Objective :
III. Theory :
IV. Apparatus :
A. Static Bending
41
2. Bearing block assembly containing a horizontal are pivoted on the neutral
exis of the block and flattened at the ends.
3. Testing machine
E. Hardness
V. Procedure :
A. Static Bending
Size of specimen ------------ 50 mm x 50 mm x 600 mm
1. Measure the actual height and width at the center and length of the
specimen.
2. Set the specimen for test. It shall be placed so that the load will be applied
through the bearing block to the tangential surface nearest the pith.
Use the center loading method and a span of 28 inches.
3. Apply the load at the center of the beam at a uniform speed of 0.10 in per
minute until the beam fails.
4. Take simultaneous readings of loads and deflection of the neutral plane at
t he center of the length, and plot the curve up to or beyond the
maximum load. In at least one third of the tests take readings up to a 6-
inch deflection or until the specimen fails to support a load of 200 lbs.
Within the proportion limit the deflection limit, the deflection readings
shall be taken to 0.001 in, after which less refinement is necessary
in observing deflections.
5. Observe and sketch the type of failure. Static bending failures are
classified according to the appearance of the fractured surface and the
manner in which the failure develops. The fractured surfaces may
be roughly divided into "brash" and "fibrous" and the term "brash"
indicating abrupt failure and the term "fibrous" indicating a fracture
showing splinters.
6. Calculations :
Where:
b= width of specimen
d= depth of specimen
L= span length
P= maximum load
P1= load of proportional limit
Y1 = center of deflection at proportional limit load
1. Measure the actual cross section dimensions and length of the specimen.
42
2. Set the specimen for test. It shall be so placed such that the load will be applied
through the metal bearing block to a radial surface.
3. Apply the load through the metal bearing block 50 mm in width, placed
across the upper surface of the specimen at equal distances from the ends and at
right angles to the length. The load shall be applied continuously throughout the
test at a rate of 0.012 inch per min.
4. Take simultaneous readings of load and deflection and plot the curve
up to 0.1 in compression . Measure deflection between the loading's surfaces.
5. Calculation:
D. Hardness :
1. Measure the actual cross section dimensions and length of the specimen.
2. Set the specimen for test on the working table of the testing machine or on
some suitable bearing surface and arrange the penetrator assembly for mounting on
the sensitive platen.
3. Apply the load continuously throughout the test at a rate of 0.25 against the
specimen. Record the load at this penetration of the "ball". The collar may be
rotated through a small angle by means of the handle, freedom to rotate
being indicative of insufficient penetration.
4. Make two penetrations shall be far enough from the edge to prevent
splitting or chipping.
A. Static Bending
Speed of Testing, in /min
1. Width of specimen, in
2. Depth of specimen, in
3. Span length, in
4. Load at P.L.
5. Max. Load, kg
43
6. Deflection at P.L., in
7. Modulus of Rupture, MPa 3x (5) x (3)/2x1x22
8. Stress at P.L., MPa 3x(4) x(3) /2x(1) x (2)2
9. Modulus of Elasticity, 6.91 MPa, (4) x (3)3/ 4 x (1) x(2)3x(6)
E. Hardness
Speed of Testing, in /min
1. On Tangential Surface
2. On Radial Surface
3. On end Surface
VII. Discussion:
44
Name Date
Performed
Offer # Rating
I. Experiment # 21
III. Objective :
IV. Theory :
The use of steel in the concrete reinforcement is in the form of steel bars.
It calls for the use of billet steel bars; the bars should be rolled from billets
directly reduced from ingots of properly identified heats of steel. It is also
required that the steel shall be made by one or more of the following processes:
open hearth, electric furnace, or acid Bessemer.
Two classes of steel bars are commonly used; plain and deformed. These
are classified into three grades; structural, intermediate and hard. The standard
sizes of deformed bars are listed in table II-1. The standard sizes of plain bars are
designated by their width and diameters.
Three important tests are performed on billet-steel bars-a chemical test for
determination of phosphorous content and the cold bend and tension tests to check
the mechanical characteristics.
The amount of phosphorous in steel is a critical quantity. A very small
amount is needed to improve its mechanical properties. However, beyond 0.10%
phosphorous causes "cold shortness" meaning brittle when cold or it makes the
steel less resistance to impact.
In the tension test, the yield and tensile strengths are obtained and these
are used to classify the bars into grade. After the grade is determined, the percent
elongation is computed and compared with the requirements for each grade. See
table II-2. Hard grade bars are sometimes not allowed by specifications because
this grade of steel is less ductile than the two other grades and even too brittle to
withstand cold bending.
Reinforcing steel bars are often bent when used thus a cold bend test is
necessary to check the ductile properties. Ductile bars will not break or crack on
the outside of the bent proportion.
V. Apparatus :
1. Testing machine
2. Extensometer
3. Cold bend apparatus
4. Balance
45
VI. Procedure :
A. Tensile Properties
B. Bending Properties
1. Place the on the rollers of the cold bend apparatus and bend thru
the desired angle by a pin attached to the head of the
machine.
2. Apply the continuous and uniform load through out the bending
operation. The size of pin and the angle of bend can be
obtained from Table II-3 & 4. They depend on the grade and
diameter of the sample.
3. Examine carefully the bent portion for any sign of cracking on thee
outside bend.
Table I
46
Bar No. 1 2
47
1. Class
2. Nominal Diameter,mm
3. Average Diameter, mm
4. Length, mm
5. Weight, kg
6. Tensile Load, kg
a. At yield point
b. Gage Length
7. Elongation, mm
a. Final Length
b. Gage Length
c. Change in Length
8. Area, Sq. Mm
a. Plain:
b. Deformed
9. Yield point, psi 6a/8a or b
10. Tensile Strength, psi: 6b/8a or b
11. Grade: Refer to Table II-2
12. Elongation, % 7c/7b x 100 %
13. Elongation requirement, min, %
Refer to Table II - 2
14. Bend test requirement, min, %
Refer to tables II-3 & 4
a. Pin Dia., mm
b. Degree of bend
c. Observation
15. Conclusion :
Suitable fo Concrete reinforcement
Table II
Tensile
Strength, MPa
Yield
Point,mm,
MPa
Elongation,m
m-min. %
VIII. Discussion :
48
Nominal Dimension
Note :
d = diameter of pin around which specimen is bent
t = diameter of the specimen
49
Name Date
Performed
Offer # Rating
I. Experiment # 22
III. Objective :
IV. Apparatus :
1. Hydrometer
2. Hydrometer jar
3. Thermometer
4. Beaker
5. Balance
V. Procedure :
50
water and immersed in water at 25 0C for 30 minutes. It shall then
be wiped dry and its weight determined to given weight "d".
51
Name Date
Performed
Offer # Rating
I. Experiment # 23
III. Objective :
IV. Apparatus
1. Chisel
2. Mallet
3. Water Bucket
4. Balance
5. Steel brush
V. Procedure:
1. Cut approximately 6" x 6" sample with a chisel from the compacted
pavement.
2. Weigh after brushing with a steel brush to remove loose materials.
3. Determine this weight know as "a"
4. Weigh the sample quickly under water.
5. Care should be taken to reduced the time of weighing to prevent absorption of
water. This weight shall be known as "b ".
6. Heat the sample after this determination to soften so that it may be disintegrated
by means of a little pressure.
VI. Calculation:
Specific Gravity = a
a - b
52
Percent Voids = 100 ( D - d )
D
D = 100
W + w
G g
Where:
W - percent of mineral aggregate
G - specific gravity of mineral aggregate
w - Per cent of Asphalt
G - specific gravity of asphalt
VII. Discussion :
53
Name Date
Performed
Offer # Rating
I. Experiment # 24
III. Objective :
To determine the time of initial and final set with the use of the
Gillmore Needle
IV. Apparatus :
Gillmore Needle
Glass Plates
Graduated Cylinder
Balance
V. Procedure :
VI. Discussion :
54