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    KI 0,1 N at 5 ML Amilum 3 GR Dalam 100 ML Aquadest

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    panji_gomis8416
    This document contains calculations for determining reagent amounts and mass transfer coefficients in a reactor. It provides the area and volume calculations for the reactor based on dimensions provided. It then calculates the amounts of reagents needed based on molar masses. Experiments were run at different air flow rates and calculations shown to determine holdup, circulation rates, and the mass transfer coefficient (KLa) between gas and liquid in the reactor. KLa values were found to be around 0.25 L/s across the different flow conditions tested.

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    KI 0,1 N at 5 ML Amilum 3 GR Dalam 100 ML Aquadest

    Uploaded by

    panji_gomis8416
    14 views5 pages
    This document contains calculations for determining reagent amounts and mass transfer coefficients in a reactor. It provides the area and volume calculations for the reactor based on dimensions provided. It then calculates the amounts of reagents needed based on molar masses. Experiments were run at different air flow rates and calculations shown to determine holdup, circulation rates, and the mass transfer coefficient (KLa) between gas and liquid in the reactor. KLa values were found to be around 0.25 L/s across the different flow conditions tested.

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    This document contains calculations for determining reagent amounts and mass transfer coefficients in a reactor. It provides the area and volume calculations for the reactor based on dimensions provided. It then calculates the amounts of reagents needed based on molar masses. Experiments were run at different air flow rates and calculations shown to determine holdup, circulation rates, and the mass transfer coefficient (KLa) between gas and liquid in the reactor. KLa values were found to be around 0.25 L/s across the different flow conditions tested.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    14 views5 pages

    KI 0,1 N at 5 ML Amilum 3 GR Dalam 100 ML Aquadest

    Uploaded by

    panji_gomis8416
    This document contains calculations for determining reagent amounts and mass transfer coefficients in a reactor. It provides the area and volume calculations for the reactor based on dimensions provided. It then calculates the amounts of reagents needed based on molar masses. Experiments were run at different air flow rates and calculations shown to determine holdup, circulation rates, and the mass transfer coefficient (KLa) between gas and liquid in the reactor. KLa values were found to be around 0.25 L/s across the different flow conditions tested.

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    LEMBAR PERHITUNGAN REAGEN

    Tinggi Cairan

    = 90 cm

    Luas Area Riser (Ar)

    = ( 8,3 cm x 14 cm) = 116,2 cm2

    Luas Area Downcomer (Ad) = ( 5,2 cm x 14 cm) = 72,8 cm2


    Volume Reaktor

    = Luas alas total x tinggi cairan


    = (116,2 cm + 72,8 cm) x 90 cm
    = 18018 cm3 = 18,018 dm3

    BM Na2SO3

    = 126 gr/mol

    BM Na2S2O3.5H2O

    = 258 gr/mol

    a. Na2S2O3.5H2O 0,1 N ( basis 500 ml )

    = 6,45 gram
    b. Na2SO3 0,01 N ( basis volume reaktor)

    = 11,35 gram
    c. KI 0,1 N @ 5 ml
    d. Amilum 3 gr dalam 100 ml aquadest

    LEMBAR PERHITUNGAN

    1. Penentuan Hold Up Gas


    = 0,0012 gr/ml
    Z = 90 cm 15 cm = 75 cm
    a. Variabel 1 (laju alir udara 4 cm3/s) hr = 0,7 cm ; hd = 0,5 cm
    c ir n =
    =

    (79,12-29,29)gr
    50 ml
    hr

    0,9966 gr/ml
    (0,9966 0,0012)gr/ml
    d

    0,7
    75

    = 0,0093

    hd
    g
    0,9966 gr/ml

    = (0,9966
    =
    =

    = 0,9966 gr/ml

    0,0012)gr/ml
    r r

    0,2
    75

    = 0,0027

    d d

    (0,0186) 116,2) 0,0093) 72,8)


    116,2 72,8)

    = 0,015

    b. Variabel 2 (laju alir udara 5 cm3/s) hr = 0,9 cm ; hd = 0,5 cm


    c ir n =
    r

    (79,11-29,29)gr
    50 ml
    hr

    g
    0,9964 gr/ml

    = (0,9964
    d=

    0,0012)gr/ml

    0,9
    75

    = 0,012

    hd
    g

    0,9964 gr/ml

    = (0,9964
    =
    =

    = 0,9964 gr/ml

    0,0012)gr/ml
    r r
    r

    0,5
    75

    = 0,0067

    d d
    d

    (0,012) 116,2) 0,0027) 72,8)


    116,2 72,8)

    = 0,0084

    c. Variabel 3 (laju alir udara 6 cm3/s) hr = 1,4 cm ; hd = 0,7 cm


    c ir n =
    r=

    (79,06-29,29)gr
    50 ml

    hr
    g
    0,9954 gr/ml

    = (0,9954
    d=

    = 0,9954 gr/ml

    0,0012)gr/ml

    1,4
    75

    = 0,0186

    hd
    g
    0,9954 gr/ml

    = (0,9954

    0,0012)gr/ml
    r r

    0,7
    75

    = 0,0093

    d d
    d

    (0,0093) 116,2) 0,0067) 72,8)

    116,2 72,8)

    = 0,0083

    2. Perhitungan Laju Sirkulasi


    Lc = 30 cm

    r=

    d
    r

    a. Variabel 1 (laju alir udara 4 cm3/s) tc = 2,85 s


    d=

    30 cm

    =
    =10,53 cm/
    c 2,85

    r=

    = 10,53 m/
    r

    72,8 cm2
    116,2 cm2

    = 6,6 cm/

    b. Variabel 2 (laju alir udara 5 cm3/s) tc = 2,43 s


    d=

    30 cm

    =
    =12,35 cm/
    c 2,43

    r=

    = 12,35 m/
    r

    72,8 cm2
    116,2 cm2

    = 7,74 cm/

    c. Variabel 3 (laju alir udara 6 cm3/s) tc = 2,32 s


    d=
    r=

    30 cm

    =
    =12,93 cm/
    c 2,32
    d

    = 12,93 m/
    r

    72,8 cm2
    116,2 cm2

    = 8,1 cm/

    3. Perhitungan Koefisien Transfer Massa Gas-Cair (KLa)


    Reaksi dalam reaktor :
    Na2SO3 + 0,5 O2 Na2SO4 + Na2SO3(sisa)
    Reaksi saat analisa :
    Na2SO3(sisa) + KI + KIO3 Na2SO4 + 2KIO2 + I2(sisa)
    I2 (sisa) + 2 Na2S2O3 Na2S4O6 + 2NaI

    Mol Na2SO3 mula-mula (a) =


    Mol I2 excess (b) =

    re

    or

    e
    1

    Mol Na2SO3 sisa (c) = - 2 (


    Mol O2 yang bereaksi (d) =

    e
    1

    2 2

    -c)

    O2 yang masuk reaktor (e) =

    2
    60

    Koefisien transfer massa gas-cair (KLa)

    a. Variabel 1 (laju alir udara 4 cm3/s)


    t
    (menit)

    V titran
    (ml)

    a
    (mmol)

    0
    5
    10
    15
    20

    7,9
    8,9
    8,3
    8,3
    8,3

    90,09
    90,09
    90,09
    90,09
    90,09

    b
    (mmol)

    c (mmol)

    d (mmol)

    e
    (mgr/s)

    KLa
    (L/s)

    0,5
    0,48025
    0,5
    0,47775
    0,5
    0,47925
    0,5
    0,47925
    0,5
    0,47925
    KLa rata-rata (L/s)

    44,8049
    44,8061
    44,8054
    44,8054
    44,8054

    0
    4,78
    2,39
    1,593
    1,195

    0
    0,597
    0,299
    0,199
    0,149
    0,249

    c (mmol)

    d (mmol)

    e
    (mgr/s)

    KLa
    (L/s)

    0,5
    0,47575
    0,5
    0,48
    0,5
    0,4795
    0,5
    0,4795
    0,5
    0,4795
    KLa rata-rata (L/s)

    44,8071
    44,805
    44,80525
    44,80525
    44,80525

    0
    4,78
    2,39
    1,593
    1,195

    0
    0,597
    0,299
    0,199
    0,149
    0,249

    b. Variabel 2 (laju alir udara 5 cm3/s)


    t
    (menit)

    V titran
    (ml)

    a
    (mmol)

    0
    5
    10
    15
    20

    9,7
    8
    8,2
    8,2
    8,2

    90,09
    90,09
    90,09
    90,09
    90,09

    b
    (mmol)

    c. Variabel 3 (laju alir udara 6 cm3/s)


    t
    (menit)

    V titran
    (ml)

    a
    (mmol)

    0
    5
    10
    15
    20
    25

    7,6
    7,8
    7,9
    7,8
    7,8
    7,8

    90,09
    90,09
    90,09
    90,09
    90,09
    90,09

    b
    (mmol)

    c (mmol)

    d (mmol)

    e
    (mgr/s)

    KLa
    (L/s)

    0,5
    0,481
    0,5
    0,4805
    0,5
    0,48025
    0,5
    0,4805
    0,5
    0,4805
    0,5
    0,4805
    KLa rata-rata (L/s)

    44,8045
    44,80475
    44,8049
    44,80475
    44,80475
    44,80475

    0
    4,779
    2,39
    1,593
    1,195
    0,956

    0
    0,597
    0,299
    0,199
    0,149
    0,119
    0,227

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