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    Perhitungan HDR

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    Lea A Farissa
    This document contains calculations for a chemical experiment. It determines: 1) The amounts of reagents Na2S2O3.5H2O and Na2SO3 needed. 2) The hold-up gas in the reactor based on dimensions, liquid density and gas density. 3) Circulation rates based on cross-sectional areas and flow rates. 4) The mass transfer coefficient (KLa) between gas and liquid phases for different flow rates.

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    Perhitungan HDR

    Uploaded by

    Lea A Farissa
    14 views6 pages
    This document contains calculations for a chemical experiment. It determines: 1) The amounts of reagents Na2S2O3.5H2O and Na2SO3 needed. 2) The hold-up gas in the reactor based on dimensions, liquid density and gas density. 3) Circulation rates based on cross-sectional areas and flow rates. 4) The mass transfer coefficient (KLa) between gas and liquid phases for different flow rates.

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    This document contains calculations for a chemical experiment. It determines: 1) The amounts of reagents Na2S2O3.5H2O and Na2SO3 needed. 2) The hold-up gas in the reactor based on dimensions, liquid density and gas density. 3) Circulation rates based on cross-sectional areas and flow rates. 4) The mass transfer coefficient (KLa) between gas and liquid phases for different flow rates.

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    © All Rights Reserved
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    Download as docx, pdf, or txt
    14 views6 pages

    Perhitungan HDR

    Uploaded by

    Lea A Farissa
    This document contains calculations for a chemical experiment. It determines: 1) The amounts of reagents Na2S2O3.5H2O and Na2SO3 needed. 2) The hold-up gas in the reactor based on dimensions, liquid density and gas density. 3) Circulation rates based on cross-sectional areas and flow rates. 4) The mass transfer coefficient (KLa) between gas and liquid phases for different flow rates.

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    LEMBAR PERHITUNGAN REAGEN

    1. Kebutuhan Na2S2O3.5H2O 0,1 N basis 500 ml


    gr 1000
    N= × × valensi
    Mr V
    gr 1000
    0,1 = × ×2
    248 50 0
    gr = 6,2 gr
    2. Kebutuhan Na2SO3 0,033 N
    Tinggi cairan : 90,5 cm
    Volume reactor : 14,3 cm x 14 cm x 90,5 cm
    = 18118,1 cm3
    gr 1000
    N= × × valensi
    Mr V
    gr 1000
    0,03 3 = × ×2
    126 18118,1
    gr = 38,01 gr

    Luas area riser :


    14,3 cm x 8,5 cm = 121,55 cm2
    Luas area downcomer :
    14,3 cm x 5,5 cm = 78,65 cm2
    Tinggi sparger : 10 cm
    Tinggi cairan : 90,5 cm
    Maka nilai z : 90,5 cm - 10 cm = 80,5 cm

    B-1
    LEMBAR PERHITUNGAN

    1. Penentuan Hold-up Gas


    25 oC = 298 K
    kg
    ρ gas250 =1,4128 ( Kalogirou , 2009 )
    m3
    kg
    ρ gas300 =1,1774 3 ( Kalogirou ,2009 )
    m
    X− X 1 Y −Y 1
    =
    X 2−X 1 Y 2−Y 1
    X−1,4128 298−250
    =
    1,1774−1,4128 300−250
    kg
    X =1,1868
    L
    kg m3 103 gr
    ρ gas298 =1,1868 3 × 6 × =0,0011868 gr /ml
    m 10 ml kg

     Variabel 1
    h = 90,5 cm ; Δhr = 0,3 cm ; Δhd = 0,1 cm
    Z = 90,5 cm – 10 cm = 80,5 cm
    ( 46 , 638 4−2 0,734 ) gr
    ρcairan = =1,0362 gr/ml
    25 ml
    ρL
    ε r=
    Δhr
    ρ¿ × ¿
    Z
    1,0362 0,3
    ε r= ×
    1,0362−0,0011868❑ 80,5
    ε r=3 , 73098 x 10−3
    ρL
    ε d=
    Δhd
    ρ¿ × ¿
    Z
    1,0362 0,1
    ε d= ×
    1,0362−0,0011868 ❑ 80,5
    ε d=1,2 4366 x 10−3
    Ar . ε r + Ad . ε d
    ε ❑=
    Ar . Ad
    ( 1 21,55 ×3,73098 x 10−3 ) +(78,65 ×1,24366 x 10−3)
    ε tot =
    1 21,55+7 8,65
    ε tot =2,75381 x 10−3

     Variabel 2

    B-2
    h = 90,5 cm ; Δhr = 0,5 cm ; Δhd = 0,4 cm
    Z = 90,5 cm – 10 cm = 80,5 cm
    ( 46,566−20,734 ) gr
    ρcairan = =1,0332 gr/ml
    25 ml
    ρL
    ε r=
    Δhr
    ρ¿ × ¿
    Z
    1,03 3 2 0 ,5
    ε r= ×
    1,03 32−0,0011868❑ 80,5
    ε r=6,21832 x 10−3
    ρL
    ε d=
    Δhd
    ρ¿ × ¿
    Z
    1,03 3 2 0 ,4
    ε d= ×
    1,03 3 2−0,0011868❑ 80,5
    ε d=4,97465 x 10−3
    Ar . ε r + Ad . ε d
    ε ❑=
    Ar . Ad
    ( 121,55 × 6,21832 x 10−3 ) +(78,65 × 4,97465 x 10−3 )
    ε tot =
    121,55+ 78,65
    ε tot =5,72973 x 10−3

     Variabel 3
    h = 90,5 cm ; Δhr = 1 cm ; Δhd = 0,8 cm
    Z = 90,5 cm – 10 cm = 80,5 cm
    ( 46,563−20,734 ) gr
    ρcairan = =1,0332 gr/ml
    25 ml
    ρL
    ε r=
    Δhr
    ρ¿ × ¿
    Z
    1,0332 1
    ε r= ×
    1,0332−0,0011868❑ 80,5
    ε r=12,43664 x 10−3
    ρL
    ε d=
    Δhd
    ρ¿ × ¿
    Z
    1,0332 0,8
    ε d= ×
    1,0332−0,0011868 ❑ 80,5
    ε d=9,94931 x 10−3

    B-3
    Ar . ε r + Ad . ε d
    ε ❑=
    Ar . Ad
    ( 121,55 × 12,43664 x 10−3 ) +(78,65 ×9,94931 x 10−3 )
    ε tot =
    121,55+ 78,65
    ε tot =11,45947 x 10−3

    Laju alir εr εd ε❑
    L/menit
    4 3,73098 x 10−3 1,24366 x 10−3 2,75381 x 10−3
    6 6,21832 x 10−3 4,97465 x 10−3 5,72973 x 10−3
    8 12,43664 x 10−3 9,94931 x 10−3 11,45947 x 10−3

    2. Perhitungan Laju Sirkulasi


    Lc
    Uld=
    tc
    Ad
    Ulr=Uld x
    Ar
    Lc = 30 cm
     Variabel 1
    Laju alir = 4 L/menit ; tc = 3 s
    30 cm
    Uld= =10 cm/s
    3s
    cm 7 8,65 cm2
    Ulr=10 x =6 , 47058 cm/ s
    s 1 21,55 cm2
     Variabel 2
    Laju alir = 6 L/menit ; tc = 2,1 s
    30 cm
    Uld= =1 4,28571cm/ s
    2,1s
    cm 78,65 cm2
    Ulr=14,28571 x =9,24369 cm/ s
    s 121,55 cm2
     Variabel 3
    Laju alir = 8 L/menit ; tc = 1 s
    30 cm
    Uld= =30 cm/s
    1s
    cm 78,65 cm2
    Ulr=30 x =1 9 , 41176 cm/s
    s 121,55 cm 2
    Laju alir L/menit Uld (cm/s) Ulr (cm/s)
    4 10 6,47058

    B-4
    6 14,28571 9,24369
    8 30 19,41176

    2. Perhitungan Koefisien Transfer Massa Gas-Cair (KLa)


    N Na 2 S O 3
    a. Mol N a2 S O 3 mula mula= ×v reaktor
    eq
    N KI
    b. Mol I 2 excess= × V KI
    eq

    1 N Na2 S 2 O3
    c. Mol N a2 S O3 sisa=b−
    2 ( eq )
    ×V Na2 S2 O3

    1
    d. Mol O 2 yang bereaksi= × ( a−c )
    2
    d × BM O2
    e. O 2 yang masuk reaktor =
    t × 60
    e
    Koefisien transfer massa gas-cair (KLa) K La=
    0,008
     Variabel 1 ( Laju alir = 4 L/menit )
    t V titran a b c e
    d (mmol) KLa
    (menit) (ml) (mmol) (mmol) (mmol) (mgr/s)
    0 7,5 298,948 0,5 0,3125 149,3175 0 0
    5 6,5 298,948 0,5 0,3375 149,3052 15,925 1990,62
    10 6 298,948 0,5 0,35 149,299 7,962 995,25
    15 6 298,948 0,5 0,35 149,299 5,308 663,5
    20 6 298,948 0,5 0,35 149,299 3,981 497,663
    KLa rata-rata 829,407

     Variabel 2 (Laju alir = 6 L/menit)


    t V titran a b c e
    d (mmol) KLa
    (menit) (ml) (mmol) (mmol) (mmol) (mgr/s)
    0 5 298,948 0,5 0,375 149,286 0 0
    5 4,5 298,948 0,5 0,3875 149,280 15,923 1990,375
    10 4,5 298,948 0,5 0,3875 149,280 7,961 995,125
    15 4,5 298,948 0,5 0,3875 149,280 5,307 663,375
    KLa rata-rata 912,218

     Variabel 3 (Laju alir = 8 L/menit)


    t V titran a b c
    d (mmol) e (mgr/s) KLa
    (menit) (ml) (mmol) (mmol) (mmol)
    0 4 298,948 0,5 0,4 149,274 0 0
    5 4 298,948 0,5 0,4 149,274 15,922 1990,31
    10 4 298,948 0,5 0,4 149,274 7,961 995,125
    KLa rata-rata 995,145

    B-5
    B-6

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