Scribd Logo
Upload

Welcome to Scribd!

  • 193 views

    Yosephine Intan Ayuningtyas 13/348284/TK/40866 Example 11.11 Coulson

    Uploaded by

    Yosephine Intan Ayuningtyas
    This document provides calculations for the design of a distillation column with 16 stages that separates a mixture of acetone and air. Key details include: - Feed flow rate of 13,000 kg/h with 58% acetone and 18% air by mass - Calculations determine the number of theoretical plates needed is 25 - Column diameter is calculated to be 0.95 m at the bottom and 0.71 m at the top - Plate spacing, hole size, and downcomer area are provisionally designed and checked against design criteria

    Copyright:

    © All Rights Reserved
    Download as XLSX, PDF, TXT or read online from Scribd

    Yosephine Intan Ayuningtyas 13/348284/TK/40866 Example 11.11 Coulson

    Uploaded by

    Yosephine Intan Ayuningtyas
    193 views12 pages
    This document provides calculations for the design of a distillation column with 16 stages that separates a mixture of acetone and air. Key details include: - Feed flow rate of 13,000 kg/h with 58% acetone and 18% air by mass - Calculations determine the number of theoretical plates needed is 25 - Column diameter is calculated to be 0.95 m at the bottom and 0.71 m at the top - Plate spacing, hole size, and downcomer area are provisionally designed and checked against design criteria

    Original Description:

    This is an excel version of Example 11-11 in Coulson edition 4.

    Original Title

    Coulson 11.11

    Copyright

    © © All Rights Reserved

    Available Formats

    XLSX, PDF, TXT or read online from Scribd

    Did you find this document useful?

    Is this content inappropriate?

    This document provides calculations for the design of a distillation column with 16 stages that separates a mixture of acetone and air. Key details include: - Feed flow rate of 13,000 kg/h with 58% acetone and 18% air by mass - Calculations determine the number of theoretical plates needed is 25 - Column diameter is calculated to be 0.95 m at the bottom and 0.71 m at the top - Plate spacing, hole size, and downcomer area are provisionally designed and checked against design criteria

    Copyright:

    © All Rights Reserved
    Download as XLSX, PDF, TXT or read online from Scribd
    Download as xlsx, pdf, or txt
    193 views12 pages

    Yosephine Intan Ayuningtyas 13/348284/TK/40866 Example 11.11 Coulson

    Uploaded by

    Yosephine Intan Ayuningtyas
    This document provides calculations for the design of a distillation column with 16 stages that separates a mixture of acetone and air. Key details include: - Feed flow rate of 13,000 kg/h with 58% acetone and 18% air by mass - Calculations determine the number of theoretical plates needed is 25 - Column diameter is calculated to be 0.95 m at the bottom and 0.71 m at the top - Plate spacing, hole size, and downcomer area are provisionally designed and checked against design criteria

    Copyright:

    © All Rights Reserved
    Download as XLSX, PDF, TXT or read online from Scribd
    Download as xlsx, pdf, or txt
    You are on page 1of 12

    Yosephine Intan Ayuningtyas

    13/348284/TK/40866
    Example 11.11 Coulson
    Diketahui data :
    N
    Lm'/Vm'
    L/V
    R
    F

    16 stages
    5 bottom
    0.57 top
    1.35
    13000 kg/h

    BM aseton
    BM air
    XD
    XF

    58
    18
    0.94
    0.033

    FLOWRATES
    BM Feed
    19.32 kg/kmol
    F
    672.8778 kmol/h
    Neraca massa aseton
    Top product
    D
    23.62231 kmol/h
    Vapor rate
    V
    55.51242 kmol/h
    Neraca massa overall
    Bottom product
    B
    649.2555 kmol/h
    V'm=L'm-B
    V'm=
    162.3139 kmol/h
    L'm=
    811.5694 kmol/h
    PHYSICAL PROPERTIES
    Asumsi efiesi column sebesar 60% dan stage reboiler equivalen 1
    Nreal
    25 stages
    Asumsi 100mm air, pressure drop per plate
    P Column
    24525 Pa
    P Top
    101400 Pa
    125925 Pa
    P Bottom
    1.25925 bar

    T base
    V
    L

    105.8631 C
    0.72 kg/m3
    954 kg/m3

    Surface tension

    0.057 N/m

    Top, 98% w/w aseton


    T top
    V
    L
    BM top
    Surface tension

    57 C
    2.05 kg/m3
    753 kg/m3
    55.6
    0.023 N/m

    COLUMN DIAMETER
    Flv bottom
    0.137361
    Flv top
    0.029741

    Asumsi plate spacing 0.25


    K1 base
    0.045
    K1 top
    0.051
    Koreksi untuk surface tensions
    K1 base
    0.055486
    K1 top
    0.052446
    Uf base
    2.01895 m/s
    Uf top
    1.00378 m/s
    Design untuk 85% flooding pada maksimum flowrate
    Uv base
    Uv top

    1.716107 m/s
    0.853213 m/s

    Maksimum volumetric flowrate


    base
    1.12718 m3/s
    top
    0.418224 m3/s
    Net area yang dibutuhkan

    bottom
    top

    0.656824 m2
    0.490175 m2

    First trrial : pilih downcomer area sebesar 12% dari total


    Column cross-sectioned area
    Base
    0.7463905 m2
    Top
    0.5570173 m2
    Column diameter
    Base
    Top

    LIQUID FLOW PATTERN


    Max. Volumetric Liquid Rate

    0.95081593 m
    0.70957618 m

    0.004254 m3/s

    Dari Fig. 11.28 terlihat bahwa single pass plate dapat digunakan.
    PROVISIONAL PLATE DESIGN
    Dc
    1m
    Ac
    0.7 m2
    Ad
    0.084 m2
    saat 12%
    An
    0.616 m2
    Aa
    0.532 m2
    Hole area Ah mengambil 10% dari Aa sebagai first trial
    Ah
    0.0532 m2
    Ad/Ac
    12 %
    Dari Fig 11.31 didapatkan Iw/Dc sebesar 0.76
    Iw
    0.76 m
    Asumsi yang diambil
    hw
    50 mm
    Hole Diameter
    9 mm

    Plate thickness

    CHECK WEEPING
    Max. Liquid Rate
    Min. Liquid Rate
    Max. how
    Min. how
    hw+how

    5 mm

    4.0578 kg/s
    2.84049298 kg/s
    23.6419742 mm liquid
    18.6387063 mm liquid
    68.6387063 mm

    Dari Fig. 11.30 didapat nilai K2 sebesar 30.6


    K2
    30.6

    pada 70% turn -down

    at minimum rate

    uh (min)
    18.667619 m/s
    actual min vapor velocity
    14.8313126 m/s
    Jadi, minimum operating rate akan berada di bawah weep point

    PLATE PRESSURE DROP


    Dry Plate drop
    Max. vapor velocity through holes
    uh
    21.18759 m/s

    plate thickness/hole dia.


    Ah/Aa
    C0
    hd
    hr
    ht

    0.6
    0.1
    0.74 Fig. 11.34
    31.55397 mm liquid
    13.10273 mm liquid
    118.2987 mm liquid

    Catatan : 100 mm diasusmsika untuk menghitung base pressure.


    Perhitungan dapat diulang dengan estimasi yang direvisi,
    tapi perubahan kecil pada physical properties akan sedikit berdampak pada p
    118 mm per plate dapat diterima.

    DOWNCOMER LIQUID BACK-UP


    Downcomer pressure loss
    hap
    40 mm
    Aap
    0.0304 m2
    Karena Aap lebih kecil daripada Ad (0.084 m2) maka gunakan Aap utk pers. 1
    hdc
    3.249792 mm
    hdc asumsi
    4 mm

    195.9406 mm
    0.195941 m
    0.5(plate spacing + hw)
    0.15
    Syarat : hb < 0.5(plate spacing + hw)
    sehingga plate spacing (0.25 m) tidak acceptable.
    Check residence time
    tr
    3.869515 s
    Syarat : tr> 3 s sehingga perhitungan memenuhi syarat
    hb

    CHECK ENTRAINMENT
    uv
    % flooding
    Flv bottom

    1.829837 m/s
    91
    0.14

    urn -down

    Dari Fig 11.29 didapatkan = 0.3, diatas nilai 0.1


    Karena % flooding perhitungan di atas % flooding design, maka column diam
    tapi akan menaikkan nilai pressure drop.

    pressure.

    ikit berdampak pada plate design.

    unakan Aap utk pers. 11.92

    n, maka column diameter bisa dikurangi,

    You might also like

    pFad - Phonifier reborn

    Pfad - The Proxy pFad of © 2024 Garber Painting. All rights reserved.

    Note: This service is not intended for secure transactions such as banking, social media, email, or purchasing. Use at your own risk. We assume no liability whatsoever for broken pages.


    Alternative Proxies:

    Alternative Proxy

    pFad Proxy

    pFad v3 Proxy

    pFad v4 Proxy