Short-Beam Strength of Polymer Matrix Composite Materials and Their Laminates
Short-Beam Strength of Polymer Matrix Composite Materials and Their Laminates
Short-Beam Strength of Polymer Matrix Composite Materials and Their Laminates
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
by means of a loading nose directly centered on the midpoint 6.1 Accurate reporting of observed failure modes is essen-
of the test specimen. tial for meaningful data interpretation, in particular, the detec-
tion of initial damage modes.
7. Apparatus
3
Boldface numbers in parentheses refer to the list of references at the end of this 7.1 Testing Machine, properly calibrated, which can be
standard. operated at a constant rate of crosshead motion, and which the
error in the loading system shall not exceed 61 %. The NOTE 2—Analysis reported by Lewis and Adams (6) has shown that a
width-to-thickness ratio of greater than 2.0 can result in a significant
load-indicating mechanism shall be essentially free of inertia width-wise shear-stress variation.
lag at the crosshead rate used. Inertia lag may not exceed 1 %
of the measured load. The accuracy of the testing machine shall 8.2.2.1 For curved beam specimens, it is recommended that
be verified in accordance with Practices E 4. the arc should not exceed 30°. Also, for these specimens, the
7.2 Loading Nose and Supports, as shown in Figs. 5 and 6, specimen length is defined as the minimum chord length.
shall be 6.00-mm (0.250-in.) and 3.00-mm (0.125-in.) diameter 8.3 Specimen Preparation—Guide D 5687/D 5687M pro-
cylinders, respectively, with a hardness of 60 to 62 HRC, as vides recommended specimen preparation practices and should
specified in Test Methods E 18, and shall have finely ground be followed where practical.
surfaces free of indentation and burrs with all sharp edges 8.3.1 Laminate Fabrication—Laminates may be hand-laid,
relieved. filament-wound or tow-placed, and molded by any suitable
7.3 Micrometers—For width and thickness measurements, laminating means, such as press, bag, autoclave, or resin
the micrometers shall use a 4- to 5-mm (0.16- to 0.2-in.) transfer molding.
nominal diameter ball interface on an irregular surface such as
the bag side of a laminate and a flat anvil interface on machined 8.3.2 Machining Methods—Specimen preparation is impor-
edges or very smooth tooled surfaces. A micrometer or caliper tant for these specimens. Take precautions when cutting
with flat anvil faces shall be used to measure the length of the specimens from the rings or plates to avoid notches, undercuts,
specimen. The accuracy of the instrument(s) shall be suitable rough or uneven surfaces, or delaminations as a result of
for reading to within 1 % of the sample dimensions. For typical inappropriate machining methods. Obtain final dimensions by
section geometries, an instrument with an accuracy of 60.002 water-lubricated precision sawing, milling, or grinding. The
mm (60.0001 in.) is desirable for thickness and width mea- use of diamond tooling has been found to be extremely
surement, while an instrument with an accuracy of 60.1 mm effective for many material systems. Edges should be flat and
(60.004 in.) is adequate for length measurement. parallel within the specified tolerances.
7.4 Conditioning Chamber, when conditioning materials at 8.3.3 Labeling—Label the specimens so that they will be
nonlaboratory environments, a temperature/vapor-level- distinct from each other and traceable back to the raw material,
controlled environmental conditioning chamber is required that in a manner that will both be unaffected by the test method and
shall be capable of maintaining the required temperature to not influence the test method.
11.2.1 Report any deviations from this test method, whether 11.2.3 Condition the specimens as required. Store the speci-
intentional or inadvertent. mens in the conditioned environment until test time, if the test
11.2.2 If specific gravity, density, reinforcement volume, or environment is different from the conditioning environment.
void volume are to be reported, then obtain these samples from 11.2.4 Following final specimen machining and any condi-
the same panels as the test samples. Specific gravity and tioning, but before testing, measure and record the specimen
density may be evaluated by means of Test Methods D 792. width and thickness at the specimen midsection and the
Volume percent of the constituents may be evaluated by one of specimen length to the accuracy specified in 7.3.
the matrix digestion procedures of Test Method D 3171, or for 11.3 Speed of Testing—Set the speed of testing at a rate of
certain reinforcement materials such as glass and ceramics, by crosshead movement of 1.0 mm (0.05 in.)/min.
the matrix burn-off technique of Test Method D 2584. Void 11.4 Test Environment—If possible, test the specimen under
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content may be evaluated from the equations of Test Method the same fluid exposure level as that used for conditioning.
D 2734 and are applicable to both Test Methods D 2584 and However, if the test temperature places too severe requirements
D 3171. upon the testing machine environmental chamber, test at a
temperature with no fluid exposure control. In this case, a 11.6 Loading—Apply load to the specimen at the specified
restriction must be placed upon the time from removal of the rate while recording data. Continue loading until either of the
specimen from the conditioning chamber until test completion following occurs:
to inhibit nonrepresentative fluid loss from the specimen. 11.6.1 A load drop-off of 30 %,
Record any modifications to the test environment and specimen 11.6.2 Two-piece specimen failure, or
weight change after removal from conditioning until test 11.6.3 The head travel exceeds the specimen nominal thick-
completion. ness.
11.4.1 Monitor the test temperature by placing an appropri- 11.7 Data Recording—Record load versus crosshead dis-
ate thermocouple at specimen mid-length to be located on the placement data throughout the test method. Record the maxi-
underside of the beam. mum load, final load, and the load at any obvious discontinui-
11.5 Specimen Insertion—Insert the specimen into the test ties in the load-displacement data.
fixture, with the toolside resting on the reaction supports as 11.8 Failure Mode—Typical failure modes that can be
shown in Fig. 5 or Fig. 6. Align and center the specimen such identified visually are shown in Fig. 7. However, these may be
that its longitudinal axis is perpendicular to the loading nose preceded by less obvious, local damage modes such as transply
and side supports. Adjust the span such that the span-to- cracking. Record the mode and location of failure, if possible
measured thickness ratio is 4.0 to an accuracy of 60.3 mm identifying one or a combination of the modes shown.
(0.012 in.). The loading nose should be located equidistant
between the side supports to within 60.3 mm (0.012 in.). Both
12. Calculation
the loading nose and side supports should overhang the
specimen width by at least 2 mm (0.08 in.) at each side. In the 12.1 Short-Beam Strength—Calculate the short-beam
case of the flat laminate test, each specimen end should strength using Eq 1 as follows:
overhang the side support centers by at least the specimen Pm
Fsbs 5 0.75 3 b 3 h (1)
thickness.
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i51
xi2 – n~x!2 !/~n–1! (3) content, and prepreg volatiles content.
13.1.7 Description of the fabrication steps used to prepare
the laminate including: fabrication start date, fabrication end
CV 5 100 3 sn–1/x (4)
date, process specification, cure cycle, consolidation method,
where: and a description of the equipment used.
x̄ = sample mean (average); 13.1.8 Ply orientation and stacking sequence of the lami-
sn–1 = sample standard deviation; nate.
CV = sample coefficient of variation, %; 13.1.9 If requested, report density, volume percent rein-
n = number of specimens; and forcement, and void content test methods, specimen sampling
xi = measured or derived property. method and geometries, test parameters, and test results.
13.1.10 Average ply thickness of the material.
13. Report
13.1.11 Results of any nondestructive evaluation tests.
13.1 Report the following information, or references point- 13.1.12 Method of preparing the test specimen, including
ing to other documentation containing this information, to the specimen labeling scheme and method, specimen geometry,
maximum extent applicable (reporting of items beyond the sampling method, and coupon cutting method.
control of a given testing laboratory, such as might occur with 13.1.13 Calibration dates and methods for all measurements
material details or panel fabrication parameters, shall be the and test equipment.
responsibility of the requester): 13.1.14 Details of loading nose and side supports including
NOTE 4—Guides E 1309, E 1434, and E 1471 contain data reporting diameters and material used.
recommendations for composite materials and composite materials me- 13.1.15 Type of test machine, alignment results, and data
chanical testing. acquisition sampling rate and equipment type.
13.1.1 This test method and revision level or date of issue. 13.1.16 Dimensions of each test specimen.
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13.1.22 Maximum load observed during the test, for each
specimen. 15. Keywords
13.1.23 Load-displacement curves for each specimen. 15.1 composite materials; resin and interlaminar properties;
13.1.24 Failure mode of each specimen, identified if pos- short-beam strength
sible from Fig. 7.
REFERENCES
(1) Berg, C. A., Tirosh, J., and Israeli, M., “Analysis of Short Beam (4) U.S. Department of Transportation, Federal Aviation Administration,
Bending of Fiber Reinforced Composites,” in Composite Materials: “Test Methods for Composites a Status Report: Volume III Shear Test
Testing and Design (Second Conference), ASTM STP 497, ASTM, Methods,” Report No. DOT/FAA/CT-93/17, III, FAA Technical Cen-
1972, pp. 206-218. ter, Atlantic City, 1993.
(2) Whitney, J. M., and Browning, C. E., “On Short-Beam Shear Tests for (5) Cui, W., Wisnom, M. R., and Jones, M., “Effect of Specimen Size on
Composite Materials,” Experimental Mechanics, Vol 25, 1985, pp.
Interlaminar Shear Strength of Unidirectional Carbon Fibre-Epoxy,”
294-300.
Composites Engineering, Vol 4, No. 3, 1994, pp. 299-307.
(3) Sullivan, J. L., and Van Oene, H., “An Elasticity Analysis for the
Generally and Specially Orthotropic Beams Subjected to Concentrated (6) Adams, D. F. and Lewis, E. Q., “Current Status of Composite Material
Loads,” Composites Science and Technology, Vol 27, 1986, pp. Shear Test Methods,” SAMPE, Vol 31, No. 6, 1994, pp. 32-41.
182-191.
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