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    MB4 - Sampling of Bituminous Binders

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    ATHOLSCHWARZ
    This document describes the procedure for sampling bituminous binders from drums or tankers. It outlines the scope, apparatus needed, sample size, sampling methods for drums and tankers, reporting requirements, and notes on special considerations for different binder types.

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    © All Rights Reserved
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    MB4 - Sampling of Bituminous Binders

    Uploaded by

    ATHOLSCHWARZ
    19 views2 pages
    This document describes the procedure for sampling bituminous binders from drums or tankers. It outlines the scope, apparatus needed, sample size, sampling methods for drums and tankers, reporting requirements, and notes on special considerations for different binder types.

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    TMH

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    This document describes the procedure for sampling bituminous binders from drums or tankers. It outlines the scope, apparatus needed, sample size, sampling methods for drums and tankers, reporting requirements, and notes on special considerations for different binder types.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    19 views2 pages

    MB4 - Sampling of Bituminous Binders

    Uploaded by

    ATHOLSCHWARZ
    This document describes the procedure for sampling bituminous binders from drums or tankers. It outlines the scope, apparatus needed, sample size, sampling methods for drums and tankers, reporting requirements, and notes on special considerations for different binder types.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
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    SAMPLING METHOD MB4

    SAMPLING OF BITUMINOUS BINDERS

    1.

    2.
    2.1
    2.2

    2.3
    2.4

    SCOPE
    This method describes the procedure
    to be followed when sampling
    bituminous binders from drums or
    tankers.
    Bituminous binders
    include:
    Bitumen
    Tar
    Cut-back bitumen
    Emulsions
    Priming material

    4.2.4

    APPARATUS
    Gas or flame for heating the drum
    Sample container (5 L capacity).
    (Glass or plastic containers are
    preferred for emulsions.)
    Sampling tube or thief sample.
    Cleaning material.

    3.

    SAMPLE SIZE
    The sample size will depend on the
    purpose and type of material, as well
    as on the volume and method of
    storage. Normally the sample will
    be about 4 L.

    4.

    METHOD

    4.1

    Sampling of all bituminous may


    be done using the same basic
    principles. However, there are a few
    differences which should be taken
    into account. (See note 6.1 6.5 )

    4.2

    Sampling of bituminous binder in


    drums
    If the drum has to be heated, e.g in
    the case of tar or bitumen, this must
    be done slowly and uniformly after
    the plug has been removed toallow
    the gases to escape.
    Avoid
    overheating any area of the drum.
    (See note 6.4. )
    Close the drum tightly and roll it
    from side to side and invert it until
    the contents are thoroughly mixed
    Remove the plug from the drum
    and take a sample using the

    4.3
    4.3.1

    In this way samples are taken at


    least three levels in the tank and
    combined to form a total sample of
    a least 4 L.
    4.4

    4.2.1

    4.2.2

    4.2.3

    sampling tube. Let the tube down


    slowly into the drum so that the
    level of the binder in the tube stays
    the same as the level of the binder
    in the drum.
    Close the tube,
    remove it and once the binder
    adhering to the outside of the tube
    has run off, transfer it to a sample
    container.
    At least 4 L of binder must be taken
    for each individual sample. The
    quantity taken from each drum will
    therefore depend on the number of
    drums to be represented by one
    sample. (See notes. )
    Sampling of bituminous binders
    in tankers and distributors
    Using a samplig valve
    If the tanker or distributor is
    provided with a sampling valve, it
    is very easy to take a sample.
    Circulate the contents of the tanker
    or distributor to mix it touroughly.
    Draw at least 20 L of binder from
    the valve o clean it. Then draw at
    least 4 L of material into the clean
    sample container and seal it
    immediately. (See notes)

    If necessary, divide the samples as


    discussed in Chapter 7 paragraph
    1.2. Mark the sample clearly and
    indelibly immediately after sealing.
    (See paragraph 4 of Chapter 7)

    REPORTING
    Compose a report in the form of a letter
    stating the sampling method used, the
    purpose of and all other essential data.
    (See paragraph 4 of Chapter 7)

    5
    6.1

    NOTES
    Emulsion are chemically very reactive
    and special precautions must be taken to

    6.2

    6.3

    6.4

    prevent contamination. Therefore only


    take amples in clean new sample
    containers made of glass or plastic.
    The characteristics of emulsions change
    very quickly. Test on emulsions must
    therefore be completed within seven
    days.
    There for always dispatch
    samples immediately.
    Cut-back bitumens and road tars contain
    a fair amount of volatile material. If the
    volatile
    portions
    evaporate,
    the
    characteristics of the material will
    change. Therefore take care to seal the
    container with the sample as soon as
    possible. Ensure that cover of the
    container is air-tight and that it cannot
    become dislodge during transit.
    Penetration bitumens and some tars are
    usually too hard to sample when they
    are cold. They must be heated gradually
    while the binder is being stirred or
    circulated.
    The sample must be
    extracted slowly so that the hot binder
    does not splash. Use gloves and wear
    some protection on the arms when
    taking samples.

    6.5

    6.6

    The sample container may not be cleaned


    with solvent. If the container becomes
    soiled on the outside, it should be wiped
    down with a clean cloth.
    When binder distributors or tankers
    possess a circulation system the
    contents should be circulated before a
    sample is taken.

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