Lab Manual FOR Metallurgy and Mechanics of Solids: II B.Tech I Semester - Mechanical Engineering
Lab Manual FOR Metallurgy and Mechanics of Solids: II B.Tech I Semester - Mechanical Engineering
Lab Manual FOR Metallurgy and Mechanics of Solids: II B.Tech I Semester - Mechanical Engineering
FOR
METALLURGY
AND MECHANICS OF
SOLIDS
OBJECTIVE
In this laboratory, students will have the opportunity to apply loads to various
materials under different equilibrium conditions. The student will perform
tests on materials in tension, compression, torsion, bending, and impact.
These conditions and/or constraints are designed to reinforce classroom
theory by having the student perform required tests, analyze subsequent data,
and present the results in a professionally prepared report.
The machines and equipment used to determine experimental data include universal testing machines, torsion equipment, spring testing machine,
compression testing machine, impact tester, hardness tester, etc. Data will
be collected using Dial indicators, extensometers, strain gages and strain
indicator equipment, as well as load and strain readouts on the machinery
and graphing capabilities to print relevant plots for analysis.
OUTCOMES
Upon the completion of Mechanical of Solids practical course, the student
will be able to:
Determine the youngs modulus for ductile materials.
Analyze the various points on stress strain diagram.
Calculate the modulus of rigidity of ductile materials.
Calculate & Compare the hardness values for various materials.
Experiment on a spring to interpret the stiffeness and shear modulus.
Apply the concept of impact loading and to determine impact values
for various materials.
Analyse the compression strength of different materials
Determine the shear stress of different materials.
Contents
METALLURGY
2 Microstructure study
of alloy steel
13
16
II
Hardenability of steels by
Jominy End Quench Test
19
22
MECHANICS OF SOLIDS
25
26
9 TORSION TEST
28
10 HARDNESS TEST
33
11 Test on springs
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41
13 Impact test
45
48
Author: ACSReddy
Dept of Mech
Part I
METALLURGY
Experiment 1
Micro Structure of study pure
metals
1.1
AIM
To mount the given pure metals like Iron, Cu, and Al specimen in a thermosetting material by using a mounting press and to draw their microstructure.
1.2
APPARATUS
1. Mounting press
2. Thermosetting powder
3. Specimen
4. Belt, plate and disc polishing machines.
5. Microscope
1.3
DESCRIPTION
The mounting press consists of top plate and bottom plate with movable centre
stage plate which is moving up and down along the guide ways. The middle
part is raised and lowered by hydraulic jack. The mould part is the space
between the guide ways. Its temperature is controlled by a knob. A digital
timer is also provided on the panel to maintain the constant temperature of
the mould for a certain period of time. In belt polishing machine, an endless
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belt rotates between two shafts. In plate polishing machine different grades
of emery papers are placed on the stand. In disc polishing machine emery
cloth is placed over the two rotating plates.
1.4
PROCEDURE
The given specimen is placed in the desired position preferably at the centre
of the mould .Bakelite powder is poured up to the required level. The spindle
is tightened. Set 400 sec in the digital timer. Switch ON the power supply.
When 0 sec is reached in the digital timer, press the reset button, so that it
again shows 400 seconds. Then for every 100 sec apply the pressure through
hydraulic jack. When the digital timer shows 0 sec switch OFF the power.
After three to five minutes take out the mounted specimen. Finally the
specimen is mounted in the thermosetting material. The mounted specimen
is polished successively on belt, plate and disc polishing machines to obtain
the fine surface finish. Place the specimen under the microstructure ad draw
the microstructure of the same.
1.5
PRECAUTIONS
1.6
RESULT
1.7
CONCLUSION
Author: ACSReddy
Dept of Mech
Experiment 2
Microstructure study
of alloy steel
2.1
AIM
To prepare the specimens of pure metals like mild steels, low carbon steel and
High carbon steels and observes the microstructure of the same
2.2
APPARATUS
1. Given specimen
2. Specially designed files
3. Belt grinder
4. Emery papers (80,120,240,400,600)
5. Disc polishing machine
6. Microscope
2.3
THEORY
Plain carbon steels are steels having carbon as the predominant alloying
element and the other alloying elements are either Nil or negligible though
some amount of sulphur and phosphorous are present. Normally the amounts
are less than 0.05 percent and hence they are not considered. The plain
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carbon steels are broadly classified in to low carbon steels with carbon content
less than 0.3 percent and medium carbon steels contain Carbon between 0.3
to 0.7. The high carbon steels contain carbon from 0.7 to 1.5 percent.
2.4
PROCEDURE
1. The specimens of pure metals like Mild steel, Low carbon steel and high
carbon steels are mounted in a thermosetting material as explained in
the experiment no. 1.
2. Polish the specimen by using (80,120,240,400and 600) grade emery
papers. Subject the given specimen to mirror like finish by using disc
polishing machine and with suitable abrasive.
3. Clean the specimen with alcohol and wash it under the stream of flowing
water.
4. After washing the specimen is dried.
5. After drying apply the suitable etching agent for 30 to 60 sec.
6. After etching wash the specimen under the stream of flowing water.
7. Dry the specimen with the help of air blower.
8. Place the specimen under the microscope for metallurgical studies.
9. Draw the micro structure and identify the material for the given specimen.
2.4.1
As the microstructure shows the structure of the mild steel, it contains 25and
75% ferrite. The dark region defines the pearlite and bright portion is of
ferrite. The properties of low carbon steels are
1. The material is soft and ductile
2. It is easily weldable
3. It is cold workable
4. The tensile strength varies between 390 to 550 N/mm2
Author: ACSReddy
Dept of Mech
II B.Tech I Sem.
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5. The Brinell hardness number varies from115 to 140. The application includes making steel wire, sheets, rivets, screws, pipe chain and structural
parts.
2.4.2
The microstructure reveals two phases are to be about 50% each. Hence the
carbon content can be accessed to be equal to it. The properties of medium
carbon steels are invariably between low and high carbon steels. The tensile
strength varies between 75 to 800 N/ mm2 The medium carbon steels are
used in manufacture of drop forging dies, die block plates, punches, screws
and valve springs etc.
2.5
Microstructure of high carbon steels consists of continuous network of cementite in matrix to pearlite. This cementite structure is hard and brittle and
hence has poor machinability. As carbon content increases weldability and
cold working decreases. They have high strength and hardness. Its Tensile
N
strength is up to 1400 mm
2 hardness varies from 450 to 500 BHW.
High carbon steels are used in cutting machine tools, manufacturing cold
dies and wheels for railways.
2.6
PRECAUTIONS
2.7
RESULT
2.8
CONCLUSION
Author: ACSReddy
Dept of Mech
Experiment 3
Micro Structures study
of Cast Iron
3.1
AIM
To identify and draw the microstructures of Cast Iron specimens like Grey
Cast Iron, White Cast Iron, Malleable Cast iron, and S.G. Cast iron etc.
3.2
APPARATUS
1. Given specimen
2. Specially designed files
3. Belt grinder
4. Emery papers (80,120,240,400,600)
5. Disc polishing machine
6. Microscope
3.3
THEORY
Cast irons contain 2 to 6.67 % of carbon. Since high carbon content tends to
make the Cast iron very brittle, most commercially manufactured types are
in the range of2.5 to 4% of carbon. The ductility of Carbon is very low and it
cannot be rolled, drawn or worked at room temperature. However they melt
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readily and can be cast to complicated shapes which are usually machined
to final dimensions. Since the casting is only the suitable process applied to
these alloys, they are known as cast irons.
Although the common cast irons are brittle and have lower strength
properties than most steels, they are cheap, can cast more readily than steel
and have other useful properties. In addition by proper alloying good foundry
control and appropriate heat treatment is possible. The properties of any
cast iron can be varied over a wide range.
3.4
PROCEDURE
3.4.1
In white cast iron most of the carbon is present in the combed forms as
cementite.This is obtained by rapid cooling of the iron. White cast irons
contains large amount of cementite as continuous inter dendritic network. It
makes the cast iron hard, wear resistance but extremely brittle and difficult
to machine.
White cast irons are limited in engineering applications because of brittleness and lack of mach inability. They are used where resistant to wear
is important and service does not require, such as cement mixer, ball mills
certain types of drawing dies and extrusion nozzle. A large tonnage of white
cast iron is used as a raw material for manufacture of malleable cast iron.
The composition of typical malleable cast iron is as follows
Carbon: 2.9%
Silicon: 1.15%
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Manganese: 0.6%
Phosphorous: 0.15% Sulphur: 0.5%
3.4.2
3.4.3
3.4.4
Nodular cast iron is also known as ductile iron. Spheroidal graphite iron
is a cast iron in which graphite is present as tiny balls or spheroids. The
compact spheroids interrupt the continuity of the matrix much less than
graphite flakes. This result in higher strength and toughness compared with
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a similar structure of grey cast iron. Nodular cast iron differs from malleable
cast iron in that it is usually obtained as a result of solidification and does
not require heat treatment. The spheroids are more rounded than irregular
aggregates of temper carbon found in malleable cast iron. The formation of
spherical graphite is due to addition of magnesium to the molten grey iron.
The composition of typical S.G.cast iron is as follows
Carbon: 3 to 3.5%
Silicon: 2 to 2.5%
Manganese: 0.15 to 0.6%
Phosphorous: 0.025 to 0.4%
Sulphur: 0.015 to 0.04 %
3.5
APPLICATIONS
Agricultural tractor and implement parts, automotive and diesel crank shafts,
piston and cylinder heads, electrical fittings, motor frames, hoist drums,
flywheels and elevator buckets, steel mill, furnace doors and bearings wrenches
levers and handles.
Author: ACSReddy
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Dept of Mech
Experiment 4
Micro Structures study of
Non-Ferrous alloys
4.1
AIM
4.2
APPARATUS
4.3
THEORY
Non ferrous metals ad alloys contain other than iron as a main constituent.
They exhibit different properties compared to ferrous metals and alloys.
Hence their application also differs from ferrous metals. We shall study the
microstructures of Al, Cu, and alloys.
4.4
PROCEDURE
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2. After washing the specimen is dried. After drying supply the suitable
etching agent for 30 to 50 sec.
3. After etching wash the specimen under stream of flowing water.
4. Dry the specimen with the help air drier.
5. Place the specimen for metallurgical studies.
6. Draw the microstructure and analyze the properties
4.4.1
CU- ALLOYS
BRASS
Brasses are the copper alloys containing zinc up to 30% they possess relatively
good corrosion resistance and good working propewrties. They also posses
high ductility hence they are suitable for drastic cold working. In common
to relieve the stresses annealing is done. Most normally used brass contains
30% zinc and 70% copper which is known as cartridge brass. This shows
higher ductility and malleability. The microstructure shows a typical equi
axied grain structure with twins in annealed structure. This brass is used
for making cartridge cases. Other applications include4s radiator cases, head
light reflectors, hardware, and plumbing accessories.
4.4.2
AL-ALLOYS
Author: ACSReddy
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4.4.3
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BEARING METAL
Bearing metal has high compressive strength and high wear r resistance,
high fatigue strength and better thermal conductivity for heat dissipation,
corrosion resistance and good machinability. They have hard and soft phases.
Most widely used bearing metal is a Babbitt metal. They are called as low
melting bearing alloy. Lead based ad tin based Babbitt contain Antimony as
most popular this group.
4.5
PRECAUTIONS
Polishing should be slow, smooth and flat Uniform pressure is applied through
out the polishing
4.6
RESULT
Author: ACSReddy
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Dept of Mech
Experiment 5
Micro structures study of
Heat treated steels
5.1
AIM
5.2
APPARATUS
1. Given specimen
2. Specially designed files
3. Belt grinder
4. Emery papers (80,120,240,400,600)
5. Disc polishing machine
6. Microscope
5.3
THEORY
Heat treatment is a process of heating the metal below its melting point
and holding it at that temperature for sufficient time and cooling at the
desired rate to obtain the required Properties. The various heat treatment
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5.4
PROCEDURE
5.5
PRECAUTIONS
Author: ACSReddy
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5.6
RESULT
5.7
CONCLUSION
Author: ACSReddy
sreyas
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Experiment 6
Hardenability of steels by
Jominy End Quench Test
6.1
AIM
To evaluate the hardenability of the low carbon steel or medium carbon steel
by Jomny end quench test Method.
6.2
APPARATUS
6.3
PROCEDURE
The various steps involved in evaluating the hardenability test for a given
specimen are
1. Determination of hardness no. by Rockwell hardness test
2. Heat treatment in the furnace
3. Quenching the specimen in Jomny end quench apparatus
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6.3.1
sreyas
6.3.2
6.4
SPECIMEN
Author: ACSReddy
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6.5
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PRECAUTIONS
6.6
RESULT
6.7
CONCLUSION
Author: ACSReddy
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Dept of Mech
Experiment 7
Hardness of various treated
and untreated steels
7.1
AIM
To find the hardness of the given treated and untreated steel specimens by
conducting the hardness test.
7.2
APPARATUS
7.3
THEORY
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7.4
2F
(7.1)
D(D (D2 d2 )
PROCDEDURE
1. The face of the specimen is lightly grind and rubbed with fine emery
paper if required.
2. Select the proper test table based o the size and shape of the specimen
and place it on main screw or elevating screw
3. Select the diameter of the indenter as 10mm or 5 mm based on the
thickness of the specimen and place it I the corresponding ball holder
and fix the ball holder.
4. Place the required weights on the weight hanger based on the type of
material of the specimen and diameter of the indenter
5. Check and keep the operating level in horizontal position
6. Place the specimen securely on testing table
7. Turn the hand wheel in clock wise direction so that the specimen touches
the ball indenter
8. Lift the operating lever fro the horizontal position upwards slightly,
after which it rotates automatically.
9. Wait for 10 to 15 sec after lever becomes stand still.
10. Bring the lever back to horizontal position
11. Turn back the hand wheel and remove the specimen Measure the
diameter of impression of indentation by Brinnel microscope and find
the Brinnel hardness number.
12. Repeat the above procedure for three to four times
Author: ACSReddy
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7.5
sreyas
PRECAUTIONS
7.6
RESULT
Author: ACSReddy
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Part II
MECHANICS OF SOLIDS
25
Experiment 8
Tensile strength test
8.1
AIM:
8.2
OBJECTIVE
To conduct a tensile test on a mild steel specimen and determine the following:
1. Limit of proportionality
2. Elastic limit
3. Yield strength
4. Ultimate strength
5. Youngs modulus of elasticity
6. Percentage elongation
7. Percentage reduction in area.
8.3
APPARATUS
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4. Scale
5. Vernier Caliper
8.4
DIAGRAM
Author: ACSReddy
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Experiment 9
TORSION TEST
9.1
AIM
9.2
APPARATUS
9.3
9.4
M/C SPECIFICATIONS
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9.5
THEORY
9.6
Torsion equation
G
=
=
J
R
L
G=
TL
J
(9.1)
(9.2)
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9.7
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9.8
PROCEDURE
1. Select the driving dogs to suit the size of the specimen and clamp it
in the machine by adjusting the length of the specimen by means of a
sliding spindle.
2. Measure the diameter at about three places and take the average value.
3. Choose the appropriate range by capacity change lever
4. Set the maximum load pointer to zero.
5. Set the protractor to zero for convenience and clamp it by means of
knurled screw.
6. Carry out straining by rotating the hand wheel in either direction.
7. Load the machine in suitable increments.
8. Then load out to failure as to cause equal increments of strain reading.
9. Plot a torque- twist (T ) graph.
10. Read off co-ordinates of a convenient point from the straight line portion
of the torque twist (T ) graph and calculate the value of G by
using relation.
Author: ACSReddy
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9.9
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OBESERVATIONS
9.10
TABULATION
Sl. No.
9.11
Torque,
kg-cm
Angle of twist
Modulus of
N - mm radians
Regidity
N/mm2
Average G
N/mm2
RESULT
Thus the torsion test on given mild steel specimen is done and the modulus
of rigidity is - N/mm2
9.12
GRAPH
9.13
PRECAUTIONS
Author: ACSReddy
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9.14
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Viva Questions
1. Define torque.
2. Give the expression for torque.
3. Define modulus of rigidity.
4. Give the values of G for different materials.
Author: ACSReddy
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Experiment 10
HARDNESS TEST
10.1
OBJECTIVE
To conduct hardness test on mild steel, carbon steel, brass and aluminum
specimens.
10.2
APPARATUS
Hardness tester, soft and hard mild steel specimens, brass, aluminum etc.
10.3
DIAGRAM
10.4
THEORY
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10.5
BRINELLS HARDNESS
10.5.1
AIM
10.5.2
APPARATUS
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3. Brinell microscope.
10.5.3
THEORY
2F
q
D(D D2 d2 )
kg/mm2
(10.1)
where HB is the load applied (kgf.)/ Spherical surface area indentation (in
mm.)
Author: ACSReddy
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10.5.4
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PROCEDURE
1. Select the proper size of the ball and load to suit the material under
test.
2. Clean the test specimen to be free from any dirt and defects or blemishes.
3. Mount the test piece surface at right angles to the axis of the ball
indenter plunger.
4. Turn the platform so that the ball is lifted up.
5. By shifting the lever applies the load and waits for some time.
6. Release the load by shifting the lever.
7. Take out the specimen and measure the diameter of indentation by
means of the Brinell microscope.
8. Repeat the experiments at other positions of the test piece.
9. Calculate the value of HB.
10.5.5
OBSERVATIONS
10.6
TABULATION
10.6.1
RESULT
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10.6.2
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PRECAUTIONS
Author: ACSReddy
37
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Experiment 11
Test on springs
11.1
AIM
To find the stiffness of the given spring using tensile testing machine
11.2
APPARATUS
KMI testing machine model 1.3-D ,,set of weight discs and springs.
11.3
PROCEDURE
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8. Note the tensile force from the measuring dial for every 10mm elongation
of spring
9. Draw the graph by taking elongation () on X-axis and force (F) on Yaxis.
10. Calculate the slope of the line joining all the measured points by a
straight line, which gives the stiffness of the given spring.
11. Repeated procedure for different springs of same material.
11.4
OBSERVATION TABLE
11.5
CALCULATION
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Deflection () mm
Tensile Force (F)
Loading
Un-loading
N
S.No Initial Final Net Initial Final Net Initial Final Net
mm
mm mm mm
mm mm
stiffness
k= F
4
5
11.6
GRAPH
11.7
RESULT
Author: ACSReddy
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Dept of Mech
N
mm
Experiment 12
COMPRESSION TEST ON
CUBE
12.1
AIM
12.2
12.3
THEORY
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12.4
sreyas
12.5
PROCEDURE
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7. Repeat the same procedure by keeping the specimen in such away that
the grains are along the axis of loading and take the ultimate crushing
load.
12.6
OBSERVATION TABLE
12.7
RESULT
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S.No
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Ultimate crushing
stress
c = PAc
Author: ACSReddy
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Experiment 13
Impact test
13.1
AIM
13.2
APPARATUS
13.3
THEORY
The loads that are suddenly applied to a structure are known as impact loads.
The performance on engineering materials like strength, toughness etc. vary
with rate of loading. Materials exhibits poor performance under dynamic or
shock loads.
Hence it is required to know how the strength and toughness varies with
impact or instant shock loads. In the impact test, the impact strength (i.e.
the resistance to shock loads) and the toughness of material under dynamic
load is determined.
The principle employed in all impact testing procedures is that a material
absorbs a certain amount of energy before it breaks or fractures. The quantity
of energy thus absorbed is characteristic of the physical nature of the materials.
If it is brittle it breaks more readily, i.e., absorbs a lesser quantity of energy
and if it is tough, it needs more energy for fracture.
The two important standard impact tests are
(1) Izod Impact test and
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13.4
DESCRIPTION
13.5
SPECIFICATIONS
13.6
PROCEDURE
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4. Calibrate the tester by releasing the clutch so that the pointer coincides
with zero on the scale with no specimen at the anvil
5. Re-clutch the hammer after calibration.
6. Place the specimen centrally over the supports such that the notch is
opposite to striking end.
7. Reset the pointer on the scale at its maximum value
8. Release the pendulum by operating the two levers simultaneously. The
striking edge strike against the specimen and ruptures it. The specimen
absorbs a part of the energy due to fall of the pendulum.
9. Stop the free swinging or oscillations of pendulum by a pedestal brake.
Author: ACSReddy
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Dept of Mech
Experiment 14
DOUBLE SHEAR TEST ON
STEEL BAR
14.1
AIM
14.2
14.3
Description
In actual practice when a beam is loaded the shear force at a section always
comes to play along with bending moment. It has been observed that the
effect of shearing stresses compared to bending stress is quite negligible. But
sometimes, the shearing stress at a section assumes much importance in
design calculations. Universal testing machine is used for performing shear,
compression and tension.
There are two types of UTM
1. Screw type
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2. Hydraulic type.
Hydraulic machines are easier to operate. They have a testing unit and
control unit connected to each other with hydraulic pipes. It has a reservoir of
oil, which is pumped into a cylinder, which has a piston. By this arrangement,
the piston is made to move up. Same oil is taken in a tube to measure the
pressure. This causes movement of the pointer, which gives reading for the
load applied.
14.4
Procedure:
14.5
OBSERVATIONS
14.6
Result
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