Filtration DEC07
Filtration DEC07
Filtration DEC07
Filtration
the facts
A survey of systems and methods
In my early
Whitbread days, it
was always Process
and Packaging but
when the bigger
breweries were built
it became part of the
brewing area, mainly
because filtration
problems were often
pushed back upstream in the
brewery. We were
brewing lager and
had to deal with beta
glucans which
gummed up the
works and yeast that
refused to settle to
the bottom of tall
cylindroconical
tanks.
By Paul Buttrick
Beer Dimensions
The basics
Like all things, the laws of science
dictate performance and Darcy from
way back in 1856 still shows the
way. The table below develops his
law and applies it to filtration :
Applying this equation, it is easy to
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(Photo: Puresep.)
Choice of powders
(Schematic: Krones.)
Beer viscosity:
I can remember, over 25 years ago,
spending many hours in the
Samlesbury Brewery brewhouse
doing starch tests on wort with my
fellow brewer the late Bill Barker
we were known as Starchy and
Husk after a well know pair of
American detectives. Better
brewhouse procedures and a malt
specification to reduce beta glucans
in the wort, sometimes with the aid
of added beta glucanase, made sure
we were able to filter plenty of lager
in the hot summers of the late
seventies.
Schematic of the
Steinecker TFS filter.
This filter is specifically
designed to give an even
powder coating over the
whole candle.
Permeability:
The pressure differential across a
filter bed is determined by the
permeability of the filter bed, which
is dictated by the size and porosity
of the filter powder. Very fine
powder produces a quicker pressure
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FILTRATION
Big Bags
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RIGHT: Diagram of a
KHS Kometronic
precoat filter using
regenerable cellulose
fibres instead of
kieselguhr
Disposal
Disposal costs for spent kieselguhr
is an increasing part of the total
filtration costs. With landfill being
carefully controlled, costs will only
increase. Soil injection is used by
many companies in the UK. In parts
of Germany spent kieselguhr is
already considered as a chemical
waste which is extremely expensive
to dispose of and more countries will
follow suit.
KHS are in final stages of
developing a filter system called
Kometronic incorporating a precoat
filter replacing kieselguhr with
regenerable cellulose fibres.
I know that a number of
companies are looking at
manufacturing a replacement
powder but they are not at the
commercial stage yet. I am sure
there will be long queues of
interested brewers when they
eventually come on the market as
long as the economics are sound and
the material can be used on existing
filters.
Regeneration
Pall Food and Beverage has
developed a kieselguhr regeneration
system called Befis which is used in
conjunction with their Primus filter.
This system works on the principle
Norit BMS.
ABOVE: Schematic of a
600 hl/h Norit BMF,
showing from left to
right: cold store tank,
stabilisation dosing,
recirc/retentate tank,
filter, buffer tank,
carbonator, bright beer
tank.
LEFT: A 600 hl/hr (72
module) Norit BMF
installed in a brewery in
Belgium.
of regenerating and cleaning the
spent kieselguhr from a filter with
caustic, acid and an enzyme
preparation. This material is used as
the body feed for subsequent
filtrations. A fresh, new precoat is
needed on each filter run. Overall
kieselguhr savings of 70-80% are
possible.
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FILTRATION
Membrane modules
(each of 12m2) on a Pall
Profi filter installed at
Carlsberg in Fredericia
which processes up to
480hl per hour.
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Kieselguhr-free filtration
The issues associated with powder
handling and disposal of spent filter
powder have led to companies
developing kieselguhr-free systems
based on cross flow technology. This
technology is extensively used for
cider and wine, so what is the
situation with beer? Early attempts
by APV in the 1980s to filter beer
using ceramic membranes were
unsuccessful, but at least three major
players currently have systems in
use in breweries. The 0.7- 1.0 hl/m2
flow rates on cross flow filters are
slow compared with powder filters.
The principal of cross flow filtration
is straight forward with the
unfiltered beer circulating across a
polymeric 0.450.6 micron
membrane. A cross-flow rate of
approx 1.2 m/s has a pressure which
is above the pressure on the filtered
beer side of the membrane (this is
called the trans-membrane
differential pressure).
The pressure difference between
the rough and bright side of the
membrane provides the force to
push the beer through the membrane
and take out any particles. Because
there is a fast flow across the
membrane perpendicular to the flow
through the membrane, there is little
build up of solids. There is no dead
end filter bed to go through as in a
conventional filter, so there is no
static filter bed build up and hence
little pressure build up. There will
be some build up of solid material
on the membrane which will cause a
rise in the trans-membrane pressure,
and the process will continue until a
pressure difference of about 1.5 bar
is reached. The manufacturers of
cross-flow filters all use an interim
pulsing or backwashing
technique to disturb any solid build
up and reduce the trans membrane
pressure. A stage is reached when
the trans membrane pressure will
not reduce, in which case a chemical
clean is carried out.
If we are looking at the physics of
filtration, the same principles apply
crossflow filtration is enhanced by
a large surface area, thin filter bed,
and slow flow rate/m2, so there is
slower pressure build up compared
with conventional filtration.
The three systems presented by Pall,
Norit and Alfa Laval, all use
polyethersulphone membranes put
together in a series of modules.
FILTRATION
Another
development by
Steinecker (Krones)
is the TFS-Twin Flow
System candle filter
introduced in 2000.
This filter is different
in that there is no
filtered beer section
of the filter vessel.
The rough beer
comes into the
vessel, filtered beer
comes out through
the candles into a
manifold within the
body of the filter
which feeds directly
into the filter outlet
pipe.
Horizontal screen
Candle
Filtrox
KHS
Pall/Schenk
Krones/Steinecker
Novox
Orion
Niro
-
Filter-o-mat
Cosmos
Primus
Steineker FS 130K
Synox PF
Getra Eco
Ecoflux
Steineker TFS
Configuration
Module size
Size/modules etc
Membrane
Pore size
Flow rates
Number in use
18
Norit
Batch or continuous
9.8 m2
Blocks of 24 modules up to max
of 72 (600 hl/h)
Polyethersulphone
0.5 micron
0.8 hl/m2/h
19
Pall Alfa
Continuous
12 m2
Blocks of 20 modules (up to
240 hl/h per block)
Polyethersulphone
0.65 micron
0.5 1hl/m2/h
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Laval
Continuous
0.7 m2 cassette
Up to 432 cassettes
(up to 300 hl/h)
Polyethersulphone
0.6 micron
0.7 hl/m2/h
2
Another unknown
is the robustness
and reliability of the
membranes and
until better
guarantees and
replacement costs
are substantiated,
many brewers will
not take the
kieselguhr-free
route.
Acknowledgements
The author would like to thank those
companies who supplied information
and images in the preparation of this
article
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