Materials System Specification

09-SAMSS-069 31 October, 2004

Qualification Requirements for
Epoxy Coatings for Atmospheric Service
Paints and Coatings Standards Committee Members
Barouky, F.F., Chairman
Hammad, B.S., Vice Chairman
Al-Homayed, M.A.
Al-Khashram, M.S.
Al-Nujaim, S.A.
Al-Seba, Z.A.
Suller, A.A.

Saudi Aramco DeskTop Standards

Table of Contents

1 Scope.......................................................... 2
2 Conflicts and Deviations............................. 2
3 References................................................. 3
4 General Requirements................................ 4
5 Qualification Tests and Requirements........ 5
6 Method of Packaging................................... 10

Previous Issue: 28 February, 1999 Next Planned Update: 1 November, 2007

Revised paragraphs are indicated in the right margin Page 1 of 10
Document Responsibility: Paints and Coatings 09-SAMSS-069
Issue Date: 31 October, 2004 Qualification Requirements for
Next Planned Update: 1 November, 2007 Epoxy Coatings for Atmospheric Service

1 Scope

This Specification defines the minimum mandatory requirements for qualifying

individual coating products for use in Saudi Aramco's approved protective coating
systems APCS-1A through APCS-1F. It shall be used when any of the following
situations occur:

1.1 Initial Product Approval

This specification shall be given to coating manufacturers, or other vendors of

coating products, that wish to obtain initial approval for products that have not
previously been qualified in accordance with this specification.

1.2 Purchase Requisitions/Purchase Orders

This specification shall be attached to Purchase Requisitions or Purchase Orders

when those documents address the procurement of coating products that have
not been previously qualified in accordance with this specification.

This specification does not apply and should not be included with Purchase
orders or requisitions for coating products that have been previously qualified
per this specification. This specification should also not be included with
purchase orders or requisitions for coated items or equipment when a Saudi
Aramco approved protective coating system has been specified.

1.3 Periodic Product Compliance Checks

This specification may be used for periodic product compliance checks on

previously approved coatings. It shall be given to the organization conducting
the compliance tests.

2 Conflicts and Deviations

2.1 Any conflicts between this specification and other applicable Saudi Aramaco
Materials System Specifications (SAMSSs), Engineering Standards (SAESs),
Standard Drawings (SASDs), or industry standards, codes, and forms shall be
resolved in writing by the Company or Buyer Representative through the
Manager, Consulting Services Department, of Saudi Aramco, Dhahran.

2.2 Direct all requests to deviate from this specification in writing to the Company or
Buyer Representative, who shall follow internal company procedure SAEP-302
and forward such requests to the Mangaer, Consulting Services Department, of
Saudi Aramco, Dhahran.

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Document Responsibility: Paints and Coatings 09-SAMSS-069
Issue Date: 31 October, 2004 Qualification Requirements for
Next Planned Update: 1 November, 2007 Epoxy Coatings for Atmospheric Service

3 References

Material or equipment supplied to this specification shall comply with the latest edition
of the references listed below unless otherwise noted:

3.1 Saudi Aramco References

Saudi Aramco Engineering Procedure

SAEP-302 Instructions for Obtaining a Waiver of a
Mandatory Saudi Aramco Engineering
Requirement

Saudi Aramco Materials System Specifications

09-SAMSS-060 Packaging Requirements for Coatings
09-SAMSS-071 Inorganic Zinc Primer

Saudi Aramco Engineering Standards

SAES-H-101 APCS-1A Epoxy Coating System for Atmospheric Service
(with Inorganic Zinc Primer)
SAES-H-101 APCS-1B Epoxy Coating System for Atmospheric Service
(with Epoxy Primer)
SAES-H-101 APCS-1C Epoxy Coating System for Atmospheric Service
(with Zinc-rich Epoxy Primer)
SAES-H-101 APCS-1D Epoxy/Polyurethane Coating System for
Atmospheric Services (with Inorganic Zinc
Primer)
SAES-H-101 APCS-1E Epoxy/Polyurethane Coating System for
Atmospheric Service (with Epoxy Primer)
SAES-H-101 APCS-1F Epoxy/Polyurethane Coating System for
Atmospheric Service (with Zinc-Rich Epoxy
Primer)

3.2 Industry Codes and Standards

American Society for Testing and Materials

ASTM A36 Structural Steel
ASTM B117 Salt Spray (Fog) Testing
ASTM D16 Definition of Terms Relating to Paints, Varnishes,
Lacquers and Related Products

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Document Responsibility: Paints and Coatings 09-SAMSS-069
Issue Date: 31 October, 2004 Qualification Requirements for
Next Planned Update: 1 November, 2007 Epoxy Coatings for Atmospheric Service

ASTM D523 Specular Gloss

ASTM D610 Evaluating Degree of Rusting on Painted Steel
Surfaces
ASTM D660 Evaluating Degree of Checking of Exterior Paints
ASTM D661 Evaluating Degree of Cracking of Exterior Paints
ASTM D714 Evaluating Degree of Blistering of Paints
ASTM D822 Operating Light-and-Water Exposure Apparatus
(Carbon-Arc Type) for Testing Paint, Varnish,
Lacquer, and Related Products
ASTM D1640 Drying, Curing or Film Formation of Organic
Coatings at Room Temperature
ASTM D1654 Method for Evaluation of Painted or Coated
Specimens Subjected to Corrosive
Environments
ASTM D1849 Package Stability of Paint
ASTM D2805 Hiding Power of Paints
ASTM G26 Operating Light-Exposure Apparatus (Xenon-Arc
Type) With and Without Water for Exposure of
Nonmetallic Materials

The Society for Protective Coatings

SSPC-PA2 Measurement of Dry Paint Thickness with
Magnetic Gages
SSPC-Paint 20 Zinc-rich Primers (Type II, Organic)
SSPC-Paint 22 Epoxy-Polyamide Paints (Primer, Intermediate,
and Topcoat) dated November 1, 1982
SSPC-Vis 1 Pictorial Surface Preparation Standards for
Painting Steel Surfaces

Swedish Standard SIS 055900-Pictorial Surface Preparation Standard for

Painting Steel Structures:
Sa 2-1/2 Very Thorough Blast Cleaning

4 General Requirements

4.1 For purposes of this specification, the Buyer's Representative shall be the
Responsible Standardization Agency Representative (RSA).

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Document Responsibility: Paints and Coatings 09-SAMSS-069
Issue Date: 31 October, 2004 Qualification Requirements for
Next Planned Update: 1 November, 2007 Epoxy Coatings for Atmospheric Service

4.2 In order to qualify a coating system as acceptable under this specification, the
coating supplier shall submit a certified test report documenting that the
proposed coating system meets the qualification tests and requirements of this
SAMSS. Preparation and testing shall be performed and/or witnessed by an
independent laboratory or inspection agency. This report shall be submitted to
the Saudi Aramco RSA for review. The RSA shall decide if the data presented
by the Supplier satisfies all the requirements.

4.3 All initial product qualification tests shall be carried out at no cost to Saudi
Aramco.

5 Qualification Tests and Requirements

5.1 Tests Applicable to Specific Generic Types of Coatings

5.1.1 Epoxy coatings (except zinc-rich primers) supplied in accordance with

this Specification shall meet the requirements of SSPC-Paint 22 except
as modified below:
a) Paragraphs 2.2, 2.3 and 2.4: Should read "percent by weight," not
"percent by volume."
b) Paragraph 4.3, Composition: Base component of topcoats need not
contain anti-corrosion pigments.
c) Paragraph 5.5, Pot Life: Shall be replaced by paragraph 5.2.3 of
this Specification.
d) Paragraph 5.7, Test Panels: Shall be replaced by paragraph 5.3 of
this Specification.
e) Paragraph 5.8, Elcometer Adhesion Test: Shall be replaced by
paragraph 5.4.2 of this Specification.
f) Paragraph 5.9, Salt Spray Resistance: Shall be replaced by
paragraph 5.4.1 of this Specification.
g) Paragraph 6, Labeling: Shall be replaced by section 6 of this
Specification.
h) Paragraphs 7 (Inspection) and 8 (Safety): Delete requirements.

5.1.2 Zinc-rich epoxy primers for APCS-1C and APCS-1F, in addition to

meeting the requirements of Section 5.2, shall meet the requirements of
paragraphs 1, 2, 3, and 4 of SSPC-Paint 20 (Type II, Organic). The
vehicle shall be a catalyzed epoxy

5.1.3 Inorganic zinc silicate primers for APCS-1A and APCS-1D shall meet
the requirements of 09-SAMSS-071.

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Document Responsibility: Paints and Coatings 09-SAMSS-069
Issue Date: 31 October, 2004 Qualification Requirements for
Next Planned Update: 1 November, 2007 Epoxy Coatings for Atmospheric Service

5.1.4 Urethane coatings supplied in accordance with this Specification shall be

Type V Polyol-cured Aliphatic as defined in ASTM D16.

a) Specular gloss of the urethane coatings, when tested at a 60 degrees

angle in accordance with ASTM D523, shall be at least 85.

b) When tested in accordance with ASTM D2805, the minimum

contrast ratio of the polyurethane coating shall be 0.94 except for
red colors which shall be 0.88 minimum.

5.2 Physical Property Tests Applicable to All APCSs

5.2.1 Package Stability of Paint

When stored at 52 1C for 6 months in accordance with ASTM D1849,

the sample shall meet the following requirements:
a) Weight loss 0.
b) Skinning, pressure and corrosion 10.
c) Settling - 6 or better.
d) Grains, lumps, or streaks - 8 or better.
5.2.2 Spray Properties

The ready mixed paint shall be easily applied to a vertical surface at the
following dry film thicknesses with no tendency to orange peel, sag,
creep or run:

Inorganic zinc : See 09-SAMSS-071

(APCS-1A and APCS-1D)

Zinc-rich epoxy primers : 75 micrometers (3 mils)

(APCS-1C and APCS-1F)

Epoxy primers : 100 micrometers(4 mils)

(APCS-1B and APCS-1E):

Epoxy topcoats : 150 micrometers (6 mils)

(All APCSs)

Polyurethane (APCS-1D, : 65 micrometers (2.5 mils

APCS-1E and APCS-1F)

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Document Responsibility: Paints and Coatings 09-SAMSS-069
Issue Date: 31 October, 2004 Qualification Requirements for
Next Planned Update: 1 November, 2007 Epoxy Coatings for Atmospheric Service

5.2.3 Usable Potlife

At 40C, the viscosity of the ready-mixed paint shall remain within the
range recommended by the manufacturer for sprayability without
additional thinning for not less than 1 hour.

5.2.4 Drying Times

When tested in accordance with ASTM D1640, the Dry-Through (or

Dry-To-Handle) Time shall be 8 hours or less (2 hours or less for the
zinc-rich epoxy primers) and the Dry-To-Recoat Time shall be in
accordance with suppliers published data sheets.

5.3 Test Panel Preparation

5.3.1 Test panels shall be ASTM A36 hot-rolled steel approximately 100 mm
X 150 mm. Prior to preparing the surface, the condition of the test panel
shall be equivalent to SSPC-Guide to Vis 1 Rust Grade A, Adherent Mill
Scale. The minimum thickness of the test panel shall be 5 mm.

5.3.2 The test panel shall be abrasive blast cleaned to near white metal (SP-10
or Sa 2-).

5.3.3 Profile of blasted surface shall be as follows:

40-65 micrometers (1.5 - 2.5 mils) for APCS-1A, APCS-1B, APCS-1D,

and APCS-1E

25-40 micrometers (1.0 - 1.5 mils) for APCS-1C and APCS-1F.

The profile shall be determined with replica tape.

5.3.4 Coatings shall be mixed, applied and cured in accordance with the
Vendor's recommendations. The temperature of the test panel shall be
63 2C during coatings application. Dry film thickness shall be
measured and recorded in accordance with SSPC-PA2 and shall meet the
requirements in Table 1.

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Document Responsibility: Paints and Coatings 09-SAMSS-069
Issue Date: 31 October, 2004 Qualification Requirements for
Next Planned Update: 1 November, 2007 Epoxy Coatings for Atmospheric Service

Table 1 - Dry Film Thickness (DFT) Requirements

Intermediate Total
Primer Coat (1 or Topcoat (2 or Topcoat System(Min
(1 coat) more coats) more coats) (1 coat) 3 coats)
DFT in DFT in Max. DFT in DFT in DFT in
Micrometers Micrometers Micrometers Micrometers Micrometers
APCS Min-Max Min-Max Min-Max Min-Max
APCS-1A 65 - 100 N/A 150 N/A 275 - 400
APCS-1B 50 - 100 N/A 150 N/A 275 - 400
APCS-1C 40 75 N/A 150 N/A 250 - 375
APCS-1D 65 - 100 100 - 150 N/A 25 - 65 190 - 315
APCS-1E 50 - 100 100 - 150 N/A 25 - 65 175 - 315
APCS-1F 40 75 125 - 175 N/A 25 - 65 175 - 290

5.4 Performance Tests

5.4.1 Weather-o-Meter and Salt Fog Performance Tests

Each panel shall be scribed in accordance with ASTM D1654 and

exposed alternately in a Weather-o-Meter in accordance with ASTM
D822, Procedure B, or ASTM G26, Method B, and a salt fog cabinet in
accordance with ASTM B117. Panels shall be rotated every 100 hours
until a total of 500 hours in each device has been achieved. At the
conclusion of the test, each coating will be evaluated for and meet the
criteria in Table 2.

Table 2
Standard Acceptable Rating
ASTM D714 No blisters
Evaluating Degree of
Blistering of Paints
ASTM D660 No checking
Evaluating Degree of
Checking of Exterior Paints
ASTM D661 No cracking
Evaluating Degree of
Cracking of Exterior Paints
ASTM D610 9 or better for APCS-1B and
Evaluating Degree of APCS-1E.
Rusting on Painted 10 for APCS-1A, APCS-1C,
Steel Surfaces System APCS-1D, and APCS-1F.
ASTM D1654 Rating of Failure at Scribe
Standard Evaluation of shall not exceed:
Painted or Coated 9 for APCS-1B and APCS-1E.
Specimens Subjected to 10 for APCS-1A, APCS-1C,
Corrosive Environments APCS-1D, and APCS-1F.

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Document Responsibility: Paints and Coatings 09-SAMSS-069
Issue Date: 31 October, 2004 Qualification Requirements for
Next Planned Update: 1 November, 2007 Epoxy Coatings for Atmospheric Service

N/A No more than 10% of the total

Erosion average thickness has been removed.
ASTM D 523 The reduction in gloss of the
Specular Gloss tested sample shall not exceed
(Polyurethane Coatings Only) 20% compared to an untested sample.

5.4.2 Adhesion Test

a) Test panels shall be prepared in accordance with paragraph 5.3

except that the coatings shall be cured as shown in Table 3.

Table 3
Coating Drying Time at 25 1C
Inorganic zinc primer 14 days
Zinc rich primer 24 hours
Epoxy primer 72 hours
Epoxy intermediate coat 72 hours
Epoxy topcoat 5 days
Polyurethane topcoat 5 days

b) Determine the adhesion of the prime coat to the substrate,

intercoat adhesion, or cohesion of any coat of the painting system
by using an adhesion tester, 450 kg capacity. Lightly sand the
coated surface and aluminum dolly and apply an epoxy adhesive.
Allow the adhesive to cure as directed by adhesive supplier.
Scribe the coating and adhesive around the dolly prior to testing.
Make a minimum of three trials and report the average. The
average shall be at least 2750 kPa (400 psi).

5.4.3 Maximum Service Temperature

The maximum service temperatures of the coating systems shall be as

follows:

For APCS-1A, APCS-1B, and APCS-1C: 150C

For APCS-1D, APCS-1E, and APCS-1F: 80C

To verify compliance with these requirements, conduct adhesion tests on

coated panels that have been prepared in accordance with paragraph
5.4.2 and then exposed in an oven for 14 days at the appropriate
temperature listed above. The adhesion shall be at least 90% of that
obtained on samples prepared and tested in accordance with paragraph
5.4.2 but not subsequently exposed in an oven.

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Document Responsibility: Paints and Coatings 09-SAMSS-069
Issue Date: 31 October, 2004 Qualification Requirements for
Next Planned Update: 1 November, 2007 Epoxy Coatings for Atmospheric Service

6 Method of Packaging

Coatings shall be packaged in accordance with 09-SAMSS-060.

Revision Summary
31 October, 2004 Revised the "Next Planned Update". Reaffirmed the contents of the document and
reissued with no other changes.

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