This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles

for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Designation: D1622/D1622M − 14

Standard Test Method for

Apparent Density of Rigid Cellular Plastics1
This standard is issued under the fixed designation D1622/D1622M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.

1. Scope* 3.2 Definitions of Terms Specific to This Standard:

1.1 This test method covers the density of a cellular plastic. 3.2.1 apparent core density (of a cellular plastic)—the
Density can be evaluated as the apparent overall density weight in air per unit volume of a sample, after all forming
(includes forming skins) or by apparent core density (forming skins have been removed.
skins removed). 3.2.2 apparent overall density (of a cellular plastic)—the
1.2 The values stated in either SI units or inch-pound units weight in air per unit volume of a sample, including all forming
are to be regarded separately as standard. The values stated in skins.
each system may not be exact equivalents; therefore, each
system shall be used independently of the other. Combining 4. Significance and Use
values from the two systems may result in non-conformance 4.1 If the material to be tested includes forming skins, the
with the standard. apparent overall density, or the apparent core density, or both,
1.3 This standard does not purport to address all of the shall be determined. If the material does not have forming
safety concerns, if any, associated with its use. It is the skins, the term overall density is not applicable.
responsibility of the user of this standard to establish appro- 4.2 This test method is also applicable to spray foam
priate safety and health practices and determine the applica- materials.
bility of regulatory limitations prior to use.
4.3 Before proceeding with this test method, reference shall
NOTE 1—This test method is equivalent to ISO 845. be made to the specification of the material being tested. Any
test specimen preparation, conditioning, dimensions, or testing
2. Referenced Documents
parameters, or combination thereof, covered in the relevant
2.1 ASTM Standards:2 ASTM materials specification shall take precedence over those
D618 Practice for Conditioning Plastics for Testing mentioned in this test method. If there are no relevant ASTM
D883 Terminology Relating to Plastics material specifications, then the default conditions in this
E691 Practice for Conducting an Interlaboratory Study to method apply.
Determine the Precision of a Test Method
4.4 When density or apparent density is used in reference to
2.2 ISO Standard:
a cellular plastic, without further qualification, it shall be
ISO 845 Cellular Plastics and Rubbers—Determination of
interpreted as follows:
Apparent (Bulk) Density3
4.4.1 density—shall be interpreted as being the apparent
3. Terminology overall density if the material is to be used with forming skins
3.1 For definitions of terms associated with plastic intact.
materials, see Terminology D883. 4.4.2 density—shall be interpreted as the apparent core
density if the forming skins have been, or will be, removed
1
before the material is used.
This test method is under the jurisdiction of ASTM Committee D20 on Plastics
and is the direct responsibility of Subcommittee D20.22 on Cellular Materials -
Plastics and Elastomers. 5. Apparatus
Current edition approved April 1, 2014. Published May 2014. Originally
approved in 1959. Last previous edition approved in 2008 as D1622 - 08. DOI: 5.1 Analytical Balance or Scale, capable of weighing the
10.1520/D1622-14. specimens to the nearest 60.1 %.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM 5.2 Micrometer Dial Gauge, Caliper, or Steel Rule, suitable
Standards volume information, refer to the standard’s Document Summary page on for measuring dimensions of the specimen to 60.1 %.
the ASTM website.
3
Available from American National Standards Institute (ANSI), 25 W. 43rd St., 5.3 Dual Component Spray Equipment, designed to meter
4th Floor, New York, NY 10036, http://www.ansi.org. the materials.

*A Summary of Changes section appears at the end of this standard

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 D1622/D1622M − 14
6. Test Specimen 9.2 Measure specimens with a caliper or a dial-type gauge
6.1 The specimen shall be of a shape whose volume can be having a foot with a minimum area of 6.5 cm2 [1 in.2]. Hold the
readily calculated, and not less than 16.4 cm3 [1.0 in.3] in pressure of the dial foot to 2.7 6 0.7 kPa [0.4 6 0.1 psi], unless
volume. such pressure indents the specimen. In these cases, the pressure
shall be reduced accordingly. When a sliding caliper gauge is
6.2 If the sample is a single object whose weight and used, the proper setting shall be that point at which the
volume can be measured accurately, using the total weight and measuring faces of the gauge contact the surfaces of the
total volume to determine the sample density is acceptable. In specimen without compressing them. Do not use a steel rule for
this case, the test specimen is the entire sample. dimensions less than 25 mm [1 in.]. Measure all dimensions to
6.3 When testing spray foam materials, specimens shall be a precision of 60.1 %. In general, three measurements shall be
prepared as follows: made of each dimension. It is acceptable to use a lesser number
6.3.1 Test specimens shall be taken from finished foam when the following conditions apply:
samples that have been sprayed from compounds in accordance
with 6.3.2.
6.3.2 Spray the sample compounds at room temperature Maximum Allowed Maximum Allowed
(between 20 to 24°C), unless alternative conditions are other- Cross-Sectional Area Length of Longest
Perpendicular to Perpendicular
wise agreed upon by the contractual parties. Spray equipment Measurements Measured Dimension Dimension
shall be adjusted to the best spray pattern and optimum per Dimension
performance. Spray apply a minimum 1.27-cm [0.5-in.] layer 1 25 cm2 [4 in.2] 10 cm [4 in.]
of foam to a primed plywood base or other suitable substrate 2 100 cm2 [16 in.2] 30 cm [12 in.]
approximately 0.95-cm by 63.5-cm by 63.5-cm [0.375-in. by
25-in. by 25-in.]. After a minimum of 5 minutes, spray apply a 10. Calculation
second layer at least 3.8 cm [1.5 in.] in thickness.
6.3.3 Cut an approximate 2.54-cm [1-in.] thick specimen 10.1 Calculate the density to three significant figures as
from the second layer. For calculation of core density, remove follows:
the bottom layer and the top skin. For calculation of the D 5 W s /V
apparent overall density, cut a specimen that includes the where:
forming skin.
D = density of specimen, kg/m3,
6.4 If separate test specimens are cut from the sample, a Ws = weight of specimen, kg, and
minimum of three shall be used. The specimens shall be taken V = volume of specimen, m3.
from locations distributed throughout the sample. NOTE 2—To obtain density in g/cm3, divide D by 1000. To obtain
density in lb/ft3, divide D by 16.
6.5 When apparent overall density is determined using
specimens cut from a larger sample, the ratio of forming skin 10.2 See Appendix X1 for a density calculation that corrects
area to total volume shall be the same for the test specimens as for the buoyant effect of air.
for the sample. NOTE 3—The air buoyancy effect will vary with time and depends on
the open-cell content of the foam. Highly open-celled materials are
7. Conditioning essentially air-filled and will not exhibit the buoyant effects of air.
7.1 Conditioning—Condition the test specimens at However, freshly produced closed-cell materials are essentially air-void
and will exhibit maximum buoyant effects of air. An additional 1.22 kg/m3
23 6 2°C and 50 6 10 % relative humidity for not less than 40
[0.076 lb/ft3] would be added to the density of an air-void specimen if the
h prior to test in accordance with Procedure A of Practice correction is used.
D618, unless otherwise specified by the contract or relevant
10.3 Calculate the standard deviation (estimated) as follows
material specifications. In cases of disagreement, the tolerances
and report it to two significant figures:
shall be 61°C and 65 % relative humidity.
7.2 Test Conditions—Conduct tests in the standard labora-
tory atmosphere of 23 6 2°C and 50 6 10 % relative humidity,
s5 Œ ΣX 2 2 nX2
n21
or s 5 @ ~ ΣX 2 2 nX̄ 2 ! / ~ n 2 1 !
1/2

unless otherwise specified in this specification or by the where:

contract or relevant material specification. In cases of
s = estimated standard deviation,
disagreement, the tolerances shall be 61°C and 65 % relative X = value of a single observation,
humidity. n = number of observations, and
8. Number of Specimens X̄ = arithmetic mean of the set of observations.

8.1 A minimum of three specimens shall be tested, unless

11. Report
the entire sample is measured as a single specimen (see Section
6). 11.1 Report the following information:
11.1.1 Complete description of material tested, including
9. Procedure type, source, code numbers, form, etc.,
9.1 Weigh the test specimen on a balance or scale to a 11.1.2 Conditioning procedure used, if different from that
precision of 60.1 %. specified in Section 7,

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 D1622/D1622M − 14
11.1.3 Number of specimens tested, if different from that TABLE 2 Within-Laboratory and Between-Laboratory Relative
specified in Section 8, Precision Based on Round-Robin Testing Data for D1622 – 83
11.1.4 Density, average value, and standard deviation, and Nomi- Values Expressed as Percent of the Average
nal Average,
11.1.5 Date of test. Material
Density, kg/m3
kg/m3 VrA VRB VIrC VIRD
11.2 Unless otherwise stated, the density is assumed to be
the density calculated as defined in 10.1. M1 38 37.51 1.12 1.49 3.17 4.22
M2 50 49.63 0.60 0.93 1.70 2.53
M3 24 28.03 0.50 2.35 1.42 6.65
12. Precision and Bias4 M4 21 20.79 2.84 5.34 8.04 15.11
12.1 Precision: A
Vris the within-laboratory coefficient of variation of the average.
B
12.1.1 Tables 1 and 2 are based on a round-robin conducted VRis the between-laboratories coefficient of variation of the average.
C
VIr= 2.83Vr.
in 1982 in accordance with Practice E691, involving four D
VIR= 2.83VR.
materials tested by five laboratories. For each material, all the
samples were prepared at one source, but the individual
specimens were prepared at the laboratories that tested them.
Each test result was the average of five individual determina-
If Sr and SR have been calculated from a large enough body
tions. Each laboratory obtained one test result for each mate-
of data, and for test results that were averages (medians/other
rial.
function) from testing five specimens:
12.1.2 Concept of Ir and IR—Warning—The following
12.1.3 Repeatability (Ir)—In comparing two test results for
explanations of Ir and IR (12.1.2 – 12.1.5) are only intended to
the same material, obtained by the same operator using the
present a meaningful way of considering the approximate
same equipment on the same day, those test results are judged
precision of this test method. Do not rigorously apply the data
as not equivalent if they differ by more than the Ir for that
in Tables 1 and 2 to the acceptance or rejection of material, as
material and condition.
those data are specific to the round-robin and are not neces-
12.1.4 Reproducibility (IR)—In comparing two test results
sarily representative of other lots, conditions, materials or
for the same material, obtained by different operators using
laboratories. Users of this test method shall apply the principles
different equipment on different days, those test results are
outlined in Practice E691 to generate data specific to their
judged as not equivalent if they differ by more than the IR value
laboratory and materials, or between specific laboratories. The
for that material and condition. (This applies between different
principles of 12.1.2 – 12.1.5 would then be valid for such data.
laboratories or between different equipment within the same
laboratory.)
4
Supporting data have been filed at ASTM International Headquarters and may 12.1.5 Any judgment made in accordance with 12.1.3 and
be obtained by requesting Research Report RR:D20-1105.
12.1.4 would have an approximate 95 % (0.95) probability of
being correct.
TABLE 1 Within-Laboratory and Between-Laboratory Estimate of
Precision Based on Round-Robin Testing Data for D1622 – 83 12.2 The precision has not been determined for the test
Values, kg/m 3 method specific to spray foam materials.
Material Nominal Density Average
SrA SRB IrC IRD 12.3 Bias—Bias is systematic error that contributes to the
M1 38 37.51 0.42 0.56 1.18 1.58 difference between a test result and a true (or reference) value.
M2 50 49.63 0.30 0.46 0.86 1.31 There are no recognized standards on which to base an estimate
M3 24 28.03 0.14 0.66 0.40 1.88
M4 21 20.79 0.59 1.11 1.68 3.14 of bias for this test method.
A
Sris the within-laboratory standard deviation of the average.
B
SRis the between-laboratories standard deviation of the average. 13. Keywords
C
Ir= 2.83Sr.
D
IR= 2.83SR. 13.1 apparent core density; apparent density; apparent over-
all density; density; rigid cellular plastics; spray foam

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 D1622/D1622M − 14
APPENDIX

(Nonmandatory Information)

X1. DENSITY CALCULATION USING A CORRECTION FOR THE BUOYANT EFFECT OF AIR

X1.1 Calculate the density to three significant figures as V = volume of specimen, m3 .

follows:
D 5 $ ~ W s 1W a ! /V %
X1.2 The error associated with the density not using the
correction for the buoyant effect of air is dynamic and
where: approaches zero as air infiltrates into a sample. Thus, the value
D = density of specimen, kg/m3, of Wa is zero in the above calculation when the sample is at
Ws = weight of specimen, kg, equilibrium with the air. In this case, the calculation for density
Wa = weight of displaced air, kg, calculated by multiplying is identical to the calculation in 10.1.
the volume of the specimen in cubic metres by the
density of air at atmospheric temperature and pressure.
(The density of air at 23°C and 760 mm Hg of
pressure = 1.22 kg/m3 [0.076 lb/ft3]), and

SUMMARY OF CHANGES

Committee D20 has identified the location of selected changes to this standard since the last issue (D1622 - 08)
that may impact the use of this standard. (April 1, 2014)

(1) Revised 1.2 with ASTM format requirements for combined (3) Revised Section 7 conditioning statements in accordance
units standards. with Practice D618.
(2) Revised 6.3 (spray foam materials) to clarify that dimen- (4) Removed terms “may” and “should” in 6.2, 6.3.2, 9.2,
sions are approximate. 12.1.2, 12.1.3, and 12.1.4, with no change in intent.

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