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TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020

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Sample: SiNPT60 | Sample:
Operator: NHA | Operator:
Submitter: | Submitter:
File: C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT60. | File:
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Started: 1/24/2019 3:1 Analysis AdsorN2 | Started:
Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time:
Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ Measured | Sample Mass:
Cold Free Spa32.8928 cm³ Equilibration In5 s | Cold Free Spa
Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure
Automatic DegNo | Automatic Deg
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Summary Report | Isotherm Tabular Report
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| Relative Press
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Surface Area | 0.010332355
| 0.106943542
Single point s 170.5875 m²/g | 0.218510397
| 0.299682175
BET Surface A173.0903 m²/g | 0.414845918
| 0.503686564
t-Plot Micropo 14.2074 m²/g | 0.599124587
| 0.704529933
t-Plot External 158.8829 m²/g | 0.800250646
| 0.904589121
BJH Adsorption | 0.989353782
between 1.700162.767 m²/g | 0.901419228
| 0.804926742
BJH Desorption | 0.704485602
between 1.700168.3517 m²/g | 0.597820844
| 0.498855992
D-H Adsorption | 0.408501033
between 1.700151.665 m²/g | 0.305531291
| 0.213662499
D-H Desorption | 0.113931636
between 1.700159.5068 m²/g | 0.009765924
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 |
Pore Volume |
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Single point ad |
less than 181. 0.395938 cm³/g |
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t-Plot micropo 0.007306 cm³/g |
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BJH Adsorption |
between 1.7000.380797 cm³/g |
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BJH Desorption |
between 1.7000.381852 cm³/g |
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Pore Size |
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Adsorption ave9.14986 nm |
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BJH Adsorption
9.3581 nm |
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BJH Desorption
9.0727 nm |
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D-H Adsorption9.7862 nm |
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D-H Desorption9.3603 nm |
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Freundlich |
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Qm·C: 18.9588 ± 0.4505 cm³/g STP |
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m: 5.1525 ± 0.3265 |
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Temkin |
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q·alpha/Qm: 0.073405 ± 0.011565 kJ/mol·(cm³/g STP) |
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A: 2.6706 ± 2.0364 mmHg |
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DFT Pore Size |
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Volume in Por < 1.483 nm : 0.01487 cm³/ |
Total Volume i<= 117.233 nm : 0.31777 cm³/ |
Area in Pores > 117.233 nm : 21.962 m²/g |
Total Area in >= 1.483 nm : 90.339 m²/g |
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DFT Surface Energy |
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Total Area : 212.517 m²/g |
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Nanoparticle Size: |
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Average Partic34.6640 nm |
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Horvath-Kawazoe |
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Maximum pore0.395938 cm³/g |
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Median pore wi15.9656 nm |
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MP-Method |
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Cumulative sur |
1.34314 nm and
104.7787 m²/g |
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Cumulative po |
1.34314 nm and
0.141616 cm³/g |
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Average pore h1.35157 nm |
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 |
TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020
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SiNPT60 | Sample: SiNPT60
NHA | Operator: NHA
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT60. | File: C:\TriStar II 3020\data\SAMPEL\2019\J
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1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1
1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1
0.2550 g Warm Free Sp11.3393 cm³ Measured | Sample Mass:0.2550 g
32.8928 cm³ Equilibration In5 s | Cold Free Spa32.8928 cm³
None Sample Densit1.000 g/cm³ | Low Pressure None
No | Automatic DegNo
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otherm Tabular Report | Isotherm Linear Plot
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Absolute Pres Quantity AdsoElapsed Time S( aturation Pr |
760 | SiNPT60 - Adsorption
7.852590084 28.5897894 00:42 | Relative PressQuantity Adso
81.27709198 43.04985539 00:46 | 0.010332355 28.5897894
166.0679016 50.82373037 00:50 | 0.106943542 43.04985539
227.7584534 55.95558472 00:53 | 0.218510397 50.82373037
315.2828979 63.79905641 00:58 | 0.299682175 55.95558472
382.8017883 71.07175902 01:02 | 0.414845918 63.79905641
455.3346863 81.22463396 01:07 | 0.503686564 71.07175902
535.442749 98.27979336 01:15 | 0.599124587 81.22463396
608.1904907 126.9262243 01:24 | 0.704529933 98.27979336
687.4877319 207.4584275 01:42 | 0.800250646 126.9262243
751.9088745 255.9722486 01:50 | 0.904589121 207.4584275
685.0786133 244.1895043 01:58 | 0.989353782 255.9722486
611.7443237 153.6293344 02:29 |
535.4090576 102.622354 02:48 |
454.3438416 82.19864037 02:58 |
379.1305542 71.0741473 03:03 |
310.4607849 63.50454496 03:07 |
232.2037811 56.47794832 03:12 |
162.3834991 50.66671434 03:16 |
86.58804321 43.7698636 03:22 |
7.422102451 28.29521702 03:48 |
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 |
Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1
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| Sample: SiNPT60
| Operator: NHA
| Submitter:
:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan
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Analysis AdsorN2 | Started: 1/24/2019 3:1 Analysis AdsorN2
Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C
Thermal Correc No | Report Time: 1/24/2019 7:1 Thermal CorrecNo
Warm Free Sp11.3393 cm³ M| Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M
Equilibration In5 s | Cold Free Spa32.8928 cm³ Equilibration In5 s
Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³
| Automatic DegNo
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| Isotherm Log Plot
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SiNPT60 - Desorption | SiNPT60 - Adsorption SiNPT60 - Desorption
Relative PressQuantity Adso| Relative PressQuantity AdsoRelative PressQuantity Adso
0.989353782 255.9722486 | 0.010332355 28.5897894 0.989353782 255.9722486
0.901419228 244.1895043 | 0.106943542 43.04985539 0.901419228 244.1895043
0.804926742 153.6293344 | 0.218510397 50.82373037 0.804926742 153.6293344
0.704485602 102.622354 | 0.299682175 55.95558472 0.704485602 102.622354
0.597820844 82.19864037 | 0.414845918 63.79905641 0.597820844 82.19864037
0.498855992 71.0741473 | 0.503686564 71.07175902 0.498855992 71.0741473
0.408501033 63.50454496 | 0.599124587 81.22463396 0.408501033 63.50454496
0.305531291 56.47794832 | 0.704529933 98.27979336 0.305531291 56.47794832
0.213662499 50.66671434 | 0.800250646 126.9262243 0.213662499 50.66671434
0.113931636 43.7698636 | 0.904589121 207.4584275 0.113931636 43.7698636
0.009765924 28.29521702 | 0.989353782 255.9722486 0.009765924 28.29521702
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| |
| TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
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| Sample: SiNPT60 | Sample:
| Operator: NHA | Operator:
| Submitter: | Submitter:
| File: C:\TriStar II 3020\data\SAMPEL\2019\Jan | File:
| |
| |
| Started: 1/24/2019 3:1 Analysis AdsorN2 | Started:
| Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
| Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time:
| Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M| Sample Mass:
| Cold Free Spa32.8928 cm³ Equilibration In5 s | Cold Free Spa
| Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure
| Automatic DegNo | Automatic Deg
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| Isotherm Linear Absolute Plot | Isotherm Log Absolute Plot
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| SiNPT60 - Adsorption SiNPT60 - Desorption | SiNPT60 - Adsorption
| Absolute Pres Quantity AdsoAbsolute Pres Quantity Adso| Absolute Pres
| 7.852590084 28.5897894 751.9088745 255.9722486 | 7.852590084
| 81.27709198 43.04985539 685.0786133 244.1895043 | 81.27709198
| 166.0679016 50.82373037 611.7443237 153.6293344 | 166.0679016
| 227.7584534 55.95558472 535.4090576 102.622354 | 227.7584534
| 315.2828979 63.79905641 454.3438416 82.19864037 | 315.2828979
| 382.8017883 71.07175902 379.1305542 71.0741473 | 382.8017883
| 455.3346863 81.22463396 310.4607849 63.50454496 | 455.3346863
| 535.442749 98.27979336 232.2037811 56.47794832 | 535.442749
| 608.1904907 126.9262243 162.3834991 50.66671434 | 608.1904907
| 687.4877319 207.4584275 86.58804321 43.7698636 | 687.4877319
| 751.9088745 255.9722486 7.422102451 28.29521702 | 751.9088745
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 |
TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108
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SiNPT60 | Sample: SiNPT60
NHA | Operator: NHA
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan
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1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1 Analysis Adsor
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath
1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1 Thermal Correc
0.2550 g Warm Free Sp11.3393 cm³ M| Sample Mass:0.2550 g Warm Free Sp
32.8928 cm³ Equilibration In5 s | Cold Free Spa32.8928 cm³ Equilibration In
None Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit
No | Automatic DegNo
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otherm Log Absolute Plot | Isotherm Pressure Composition
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NPT60 - Adsorption SiNPT60 - Desorption | SiNPT60 - Adsorption SiNPT60 - Desorption
Quantity AdsoAbsolute Pres Quantity Adso| Weight % N2 Absolute Pres Weight % N2
28.5897894 751.9088745 255.9722486 | 0.255105397 7.852590084 2.284028791
43.04985539 685.0786133 244.1895043 | 0.384131911 81.27709198 2.178891897
50.82373037 611.7443237 153.6293344 | 0.453497846 166.0679016 1.370827599
55.95558472 535.4090576 102.622354 | 0.49928915 227.7584534 0.915694621
63.79905641 454.3438416 82.19864037 | 0.569276093 315.2828979 0.733454748
71.07175902 379.1305542 71.0741473 | 0.63417009 382.8017883 0.6341914
81.22463396 310.4607849 63.50454496 | 0.724763733 455.3346863 0.566648181
98.27979336 232.2037811 56.47794832 | 0.876946149 535.442749 0.503950177
126.9262243 162.3834991 50.66671434 | 1.132556956 608.1904907 0.452096799
207.4584275 86.58804321 43.7698636 | 1.851142161 687.4877319 0.390556512
255.9722486 7.422102451 28.29521702 | 2.284028791 751.9088745 0.252476941
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 | |
Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 |
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| Sample: SiNPT60 |
| Operator: NHA |
| Submitter: |
0\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan |
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N2 | Started: 1/24/2019 3:1 Analysis AdsorN2 |
-195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C |
No | Report Time: 1/24/2019 7:1 Thermal Correc No |
11.3393 cm³ M| Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M|
5s | Cold Free Spa32.8928 cm³ Equilibration In5 s |
1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³ |
| Automatic DegNo |
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| BET Surface Area Report |
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| BET Surface A173.0903 ± 1.8583 m²/g |
NPT60 - Desorption | Slope: 0.025057 ± 0.000265 g/cm³ STP |
Absolute Pres | Y-Intercept: 0.000093 ± 0.000051 g/cm³ STP |
751.9088745 | C: 269.527310 |
685.0786133 | Qm: 39.7616 cm³/g STP |
611.7443237 | Correlation Coe
0.9998881 |
535.4090576 | Molecular Cros0.1620 nm² |
454.3438416 | |
379.1305542 | |
310.4607849 | |
232.2037811 | |
162.3834991 | Relative PressQuantity Adso1/[Q(Po/P - 1)] |
86.58804321 | 0.010332355 28.5897894 0.000365173 |
7.422102451 | 0.106943542 43.04985539 0.002781659 |
| 0.218510397 50.82373037 0.005501516 |
| 0.299682175 55.95558472 0.007647549 |
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 |
TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020
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Sample: SiNPT60 | Sample: SiNPT60
Operator: NHA | Operator: NHA
Submitter: | Submitter:
File: C:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\J
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Started: 1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1
Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1
Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1
Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M| Sample Mass:0.2550 g
Cold Free Spa32.8928 cm³ Equilibration In5 s | Cold Free Spa32.8928 cm³
Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure None
Automatic DegNo | Automatic DegNo
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BET Surface Area Plot | BET Isotherm Plot
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SiNPT60 Not Fitted | SiNPT60
Relative Press1/[Q(Po/P - 1)]Relative Press1/[Q(Po/P - 1)]| Relative PressQuantity Adso
0.010332355 0.000365173 | 0.010332355 28.5897894
0.106943542 0.002781659 | 0.106943542 43.04985539
0.218510397 0.005501516 | 0.218510397 50.82373037
0.299682175 0.007647549 | 0.299682175 55.95558472
| 0.414845918 63.79905641
| 0.503686564 71.07175902
| 0.599124587 81.22463396
| 0.704529933 98.27979336
| 0.800250646 126.9262243
| 0.904589121 207.4584275
| 0.989353782 255.9722486
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 |
Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1
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| Sample: SiNPT60
| Operator: NHA
| Submitter:
:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan
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Analysis AdsorN2 | Started: 1/24/2019 3:1 Analysis AdsorN2
Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C
Thermal Correc No | Report Time: 1/24/2019 7:1 Thermal CorrecNo
Warm Free Sp11.3393 cm³ M| Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M
Equilibration In5 s | Cold Free Spa32.8928 cm³ Equilibration In5 s
Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³
| Automatic DegNo
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| Langmuir Reports
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| Primary Data
SiNPT60 - BET Equation |
Relative PressQuantity Adso|
0.010332355 29.64253178 |
0.106943542 43.18509467 |
0.218510397 50.21299724 |
0.299682175 56.28852232 |
0.414845918 67.59695095 |
0.503686564 79.82214041 |
0.599124587 98.94139239 |
0.704529933 134.3617056 |
0.800250646 198.8734655 |
0.904589121 416.5780878 |
0.989353782 3734.664172 |
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| |
| TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
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| Sample: SiNPT60 | Sample:
| Operator: NHA | Operator:
| Submitter: | Submitter:
| File: C:\TriStar II 3020\data\SAMPEL\2019\Jan | File:
| |
| |
| Started: 1/24/2019 3:1 Analysis AdsorN2 | Started:
| Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
| Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time:
| Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M| Sample Mass:
| Cold Free Spa32.8928 cm³ Equilibration In5 s | Cold Free Spa
| Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure
| Automatic DegNo | Automatic Deg
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| Freundlich Tabular Report | Freundlich Plot
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| Qm·C: 18.9588 ± 0.4505 cm³/g STP |
| m: 5.1525 ± 0.3265 | SiNPT60
| Correlation Coe
0.996010 | log(P)
| | 0.895012927
| | 1.909968157
| | 2.220285698
| | 2.357474505
| Absolute Pres Quantity Adsolog(P) log(Q) |
| 7.852590084 28.5897894 0.895012927 1.456210956 |
| 81.27709198 43.04985539 1.909968157 1.633971697 |
| 166.0679016 50.82373037 2.220285698 1.706066538 |
| 227.7584534 55.95558472 2.357474505 1.747843438 |
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 |
TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108
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SiNPT60 | Sample: SiNPT60
NHA | Operator: NHA
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan
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1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1 Analysis Adsor
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath
1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1 Thermal Correc
0.2550 g Warm Free Sp11.3393 cm³ M| Sample Mass:0.2550 g Warm Free Sp
32.8928 cm³ Equilibration In5 s | Cold Free Spa32.8928 cm³ Equilibration In
None Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit
No | Automatic DegNo
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reundlich Plot | Temkin Tabular Report
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| q·alpha/Qm: 0.073405 ± 0.011565 kJ/mol·(cm³/g STP)
| A: 2.6706 ± 2.0364 1/mmHg
log(Q) | Correlation Coe
0.964724
1.456210956 |
1.633971697 |
1.706066538 |
1.747843438 |
| Absolute Pres Quantity Adsoln(P)
| 7.852590084 28.5897894 2.060843424
| 81.27709198 43.04985539 4.397864205
| 166.0679016 50.82373037 5.112396751
| 227.7584534 55.95558472 5.428285652
| 315.2828979 63.79905641 5.753470325
|
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 | |
Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 |
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| Sample: SiNPT60 |
| Operator: NHA |
| Submitter: |
0\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan |
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| |
N2 | Started: 1/24/2019 3:1 Analysis AdsorN2 |
-195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C |
No | Report Time: 1/24/2019 7:1 Thermal Correc No |
11.3393 cm³ M| Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M|
5s | Cold Free Spa32.8928 cm³ Equilibration In5 s |
1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³ |
| Automatic DegNo |
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| Temkin Plot |
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1565 kJ/mol·(cm³/g STP) | |
| SiNPT60 |
| ln(P) Quantity Adsorbed (cm³/g STP) |
| 2.060843424 28.5897894 |
| 4.397864205 43.04985539 |
| 5.112396751 50.82373037 |
| 5.428285652 55.95558472 |
| 5.753470325 63.79905641 |
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 |
TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020
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Sample: SiNPT60 | Sample: SiNPT60
Operator: NHA | Operator: NHA
Submitter: | Submitter:
File: C:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\J
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|
Started: 1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1
Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1
Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1
Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M| Sample Mass:0.2550 g
Cold Free Spa32.8928 cm³ Equilibration In5 s | Cold Free Spa32.8928 cm³
Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure None
Automatic DegNo | Automatic DegNo
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t-Plot Report | t-Plot
| Harkins and Jura
Micropore Vol 0.007306 cm³/g |
Micropore Area14.2074 m²/g | SiNPT60
External Surfa158.8829 m²/g | Thickness (nmQuantity Adso
Slope: 102.717152 ± 0.000000 cm³/g·nm STP | 0.37312919 43.04985539
Y-Intercept: 4.723088 ± 0.000000 cm³/g STP | 0.448811536 50.82373037
Correlation Coe 1.000000 |
Surface Area C1.000 |
Density Conver0.0015468 |
Total Surface 173.0903 m²/g |
Thickness Ran0.35000 nm to 0.50000 nm |
Thickness Equa Harkins and Jura |
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Thickness Curve |
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t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
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t-Plot Report - Data |
|
Relative PressStatistical Thi Quantity AdsoFitted |
0.010332355 0.263181042 28.5897894 |
0.106943542 0.37312919 43.04985539 * |
0.218510397 0.448811536 50.82373037 * |
0.299682175 0.501013128 55.95558472 |
0.414845918 0.579833258 63.79905641 |
0.503686564 0.649298993 71.07175902 |
0.599124587 0.738549631 81.22463396 |
0.704529933 0.867031804 98.27979336 |
0.800250646 1.03430401 126.9262243 |
0.904589121 1.343141492 207.4584275 |
0.989353782 1.9025812 255.9722486 |
|
|
|
 |
Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1
|
|
| Sample: SiNPT60
| Operator: NHA
| Submitter:
:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan
|
|
Analysis AdsorN2 | Started: 1/24/2019 3:1 Analysis AdsorN2
Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C
Thermal Correc No | Report Time: 1/24/2019 7:1 Thermal CorrecNo
Warm Free Sp11.3393 cm³ M| Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M
Equilibration In5 s | Cold Free Spa32.8928 cm³ Equilibration In5 s
Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³
| Automatic DegNo
|
|
|
|
|
|
|
| Alpha-S Method
|
| 4029- At least two fitted data points are needed for Alpha
Not Fitted |
Thickness (nmQuantity Adso|
0.263181042 28.5897894 |
0.501013128 55.95558472 |
0.579833258 63.79905641 |
0.649298993 71.07175902 |
0.738549631 81.22463396 |
0.867031804 98.27979336 |
1.03430401 126.9262243 |
1.343141492 207.4584275 |
1.9025812 255.9722486 |
|
| |
| TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
| |
| |
| Sample: SiNPT60 | Sample:
| Operator: NHA | Operator:
| Submitter: | Submitter:
| File: C:\TriStar II 3020\data\SAMPEL\2019\Jan | File:
| |
| |
| Started: 1/24/2019 3:1 Analysis AdsorN2 | Started:
| Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
| Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time:
| Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M| Sample Mass:
| Cold Free Spa32.8928 cm³ Equilibration In5 s | Cold Free Spa
| Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure
| Automatic DegNo | Automatic Deg
| |
| |
| |
| |
| |
| |
| |
| f-Ratio Method | BJH Adsorption Pore Distribution Repor
| |
| Primary Data |
| A reference file has not been chosen. |
| |
| |
|
|
|
| Diameter Rang
| Adsorbate Prop
| Density Conver
| Fraction of Po
|
|
|
|
| Pore Diameter
| 181.8 - 21.6
| 21.6 - 10.5
| 10.5 - 7.1
| 7.1 - 5.1
| 5.1 - 4.0
| 4.0 - 3.3
| 3.3 - 2.5
| 2.5 - 2.1
| 2.1 - 1.5
|
|
 |
TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
|
|
SiNPT60 | Sample:
NHA | Operator:
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT60.SMP | File:
|
|
1/24/2019 3:1 Analysis AdsorN2 | Started:
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
1/24/2019 7:1 Thermal Correc No | Report Time:
0.2550 g Warm Free Sp11.3393 cm³ Measured | Sample Mass:
32.8928 cm³ Equilibration In5 s | Cold Free Spa
None Sample Densit1.000 g/cm³ | Low Pressure
No | Automatic Deg
|
|
|
|
|
|
|
JH Adsorption Pore Distribution Report | BJH Desorption Pore Distribution Repo
|
Faas Correction |
Harkins and Jura |
t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
|
|
|
|
1.7000 nm to 300.0000 nm | Diameter Rang
0.95300 nm | Adsorbate Prop
0.0015468 | Density Conver
0.00 | Fraction of Po
|
|
|
|
Average Diame Incremental PoCumulative PoIncremental PoCumulative Por| Pore Diameter
23.48032474 0.09501235 0.09501235 16.18586636 16.18586636 | 181.8 - 20.9
12.45405363 0.17024322 0.26525557 54.67881385 70.8646802 | 20.9 - 10.8
8.109574073 0.053785457 0.319041027 26.52936222 97.39404243 | 10.8 - 7.1
5.762778712 0.02711359 0.346154617 18.81980316 116.2138456 | 7.1 - 5.1
4.409871525 0.012840119 0.358994736 11.64670574 127.8605513 | 5.1 - 3.9
3.539594601 0.007312961 0.366307696 8.264178741 136.1247301 | 3.9 - 3.2
2.772154943 0.006153986 0.372461683 8.879714599 145.0044447 | 3.2 - 2.5
2.246316517 0.003180959 0.375642642 5.664312106 150.6687568 | 2.5 - 2.0
1.704028155 0.005154009 0.380796651 12.09841205 162.7671688 | 2.0 - 1.5
|
|
 |
TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
|
|
SiNPT60 | Sample:
NHA | Operator:
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT60.SMP | File:
|
|
1/24/2019 3:1 Analysis AdsorN2 | Started:
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
1/24/2019 7:1 Thermal Correc No | Report Time:
0.2550 g Warm Free Sp11.3393 cm³ Measured | Sample Mass:
32.8928 cm³ Equilibration In5 s | Cold Free Spa
None Sample Densit1.000 g/cm³ | Low Pressure
No | Automatic Deg
|
|
|
|
|
|
|
JH Desorption Pore Distribution Report | Dollimore-Heal Adsorption Pore Distribu
|
Faas Correction |
Harkins and Jura |
t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
|
|
|
| Diameter Rang
1.7000 nm to 300.0000 nm | Adsorbate Prop
0.95300 nm | Density Conver
0.0015468 |
0.00 |
|
|
| Pore Diameter
| 181.9 - 21.7
Average Diame Incremental PoCumulative PoIncremental PoCumulative Por| 21.7 - 10.6
22.68494632 0.023187907 0.023187907 4.088686206 4.088686206 | 10.6 - 7.2
12.71190422 0.195862202 0.219050109 61.6311132 65.71979941 | 7.2 - 5.2
8.128477659 0.10830409 0.327354198 53.29612466 119.0159241 | 5.2 - 4.1
5.732665514 0.032073238 0.359427436 22.37928432 141.3952084 | 4.1 - 3.3
4.354655321 0.011556593 0.370984029 10.6153914 152.0105998 | 3.3 - 2.6
3.478080235 0.005162392 0.376146421 5.937058831 157.9476586 | 2.6 - 2.2
2.773493132 0.002520803 0.378667224 3.635563877 161.5832225 | 2.2 - 1.6
2.223723377 0.00123579 0.379903013 2.222919661 163.8061422 |
1.715281718 0.001949228 0.381852242 4.545558444 168.3517006 |
|
|
 |
TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
|
|
SiNPT60 | Sample:
NHA | Operator:
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT60.SMP | File:
|
|
1/24/2019 3:1 Analysis AdsorN2 | Started:
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
1/24/2019 7:1 Thermal Correc No | Report Time:
0.2550 g Warm Free Sp11.3393 cm³ Measured | Sample Mass:
32.8928 cm³ Equilibration In5 s | Cold Free Spa
None Sample Densit1.000 g/cm³ | Low Pressure
No | Automatic Deg
|
|
|
|
|
|
|
ollimore-Heal Adsorption Pore Distribution Report | Dollimore-Heal Desorption Pore Distribu
|
Harkins and Jura |
t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
|
|
|
|
1.7000 nm to 300.0000 nm | Diameter Rang
0.95300 nm | Adsorbate Prop
0.0015468 | Density Conver
|
|
|
|
Average Diame Incremental PoCumulative PoIncremental PoCumulative Por| Pore Diameter
101.787648 0.078278235 0.078278235 3.076138867 3.076138867 | 181.9 - 21.0
16.15815947 0.155708664 0.233986899 38.5461387 41.62227756 | 21.0 - 10.9
8.899245181 0.056146041 0.29013294 25.23631587 66.85859343 | 10.9 - 7.2
6.186983518 0.030862215 0.320995155 19.95299671 86.81159014 | 7.2 - 5.2
4.637754386 0.016481007 0.337476162 14.21464393 101.0262341 | 5.2 - 4.0
3.701889482 0.010481537 0.347957699 11.32560804 112.3518421 | 4.0 - 3.3
2.954837741 0.009562514 0.357520213 12.94489177 125.2967339 | 3.3 - 2.6
2.367268255 0.005658186 0.363178399 9.560701383 134.8574353 | 2.6 - 2.1
1.874846031 0.007877908 0.371056307 16.80758305 151.6650183 | 2.1 - 1.6
|
|
 |
TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
|
|
SiNPT60 | Sample:
NHA | Operator:
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT60.SMP | File:
|
|
1/24/2019 3:1 Analysis AdsorN2 | Started:
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
1/24/2019 7:1 Thermal Correc No | Report Time:
0.2550 g Warm Free Sp11.3393 cm³ Measured | Sample Mass:
32.8928 cm³ Equilibration In5 s | Cold Free Spa
None Sample Densit1.000 g/cm³ | Low Pressure
No | Automatic Deg
|
|
|
|
|
|
|
ollimore-Heal Desorption Pore Distribution Report | Horvath-Kawazoe Report
|
Harkins and Jura |
t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5 |
|
|
|
| Maximum Pore
1.7000 nm to 300.0000 nm | at Relative Pr
0.95300 nm | Median Pore W
0.0015468 | Relative Press
|
| Diameter of Ad
| Diameter of Ad
| Diameter of S
Average Diame Incremental PoCumulative PoIncremental PoCumulative Por| Diameter of Sa
101.4531792 0.018999485 0.018999485 0.749093745 0.749093745 | Interaction Pa
15.94867113 0.177803291 0.196802776 44.59388234 45.34297609 |
9.023673196 0.104852129 0.301654905 46.47869058 91.82166667 | Density Conver
6.177195438 0.034852508 0.336507413 22.56849963 114.3901663 |
4.605206636 0.014920628 0.351428042 12.9597906 127.3499569 |
3.65532196 0.008110117 0.359538159 8.874859426 136.2248163 |
2.948291394 0.005513732 0.365051891 7.480579718 143.705396 |
2.371752912 0.003751789 0.36880368 6.327454052 150.0328501 | Absolute Pres
1.880255594 0.004453361 0.373257042 9.473949166 159.5067993 | 7.852590084
| 81.27709198
| 166.0679016
| 227.7584534
| 315.2828979
| 382.8017883
| 455.3346863
| 535.442749
| 608.1904907
| 687.4877319
| 751.9088745
|
|
 |
TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
|
|
SiNPT60 | Sample:
NHA | Operator:
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT60.SMP | File:
|
|
1/24/2019 3:1 Analysis AdsorN2 | Started:
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
1/24/2019 7:1 Thermal Correc No | Report Time:
0.2550 g Warm Free Sp11.3393 cm³ Measured | Sample Mass:
32.8928 cm³ Equilibration In5 s | Cold Free Spa
None Sample Densit1.000 g/cm³ | Low Pressure
No | Automatic Deg
|
|
|
|
|
|
|
orvath-Kawazoe Report |
|
Slit Pore Geometry (Original H-K) |
|
|
|
|
0.395938 cm³/g |
0.989353782 |
15.9656 nm |
1.033e-002 to 9.894e-001 | Volume in Por
| Total Volume i
0.3000 nm | Area in Pores
0.2574 nm | Total Area in
0.3040 nm |
0.2609 nm |
3.49e-043 erg·cm^4 | Pore Size Table
|
0.0015468 | Pore Width (n
| 1.483289338
| 1.590515054
| 1.715611708
| 1.8585793
Relative PressQuantity AdsoPore Width (n Cumulative PoDifferential P | 2.001546978
0.010332355 28.5897894 1.028726 0.044222686 0.042987818 | 2.16238568
0.106943542 43.04985539 1.827028874 0.066589516 0.028017975 | 2.341095234
0.218510397 50.82373037 2.551578691 0.078614146 0.016596001 | 2.519804789
0.299682175 55.95558472 3.14268348 0.086552098 0.01342901 | 2.734256221
0.414845918 63.79905641 4.193921942 0.09868438 0.011540942 | 2.948707652
0.503686564 71.07175902 5.295912817 0.109933797 0.010208266 | 3.181030107
0.599124587 81.22463396 6.987086488 0.125638264 0.009286135 | 3.431223586
0.704529933 98.27979336 10.12225368 0.152019184 0.008414518 | 3.699287918
0.800250646 126.9262243 15.75243066 0.196329484 0.007870143 | 4.003093956
0.904589121 207.4584275 34.85958316 0.320896696 0.006519402 | 4.324771359
0.989353782 255.9722486 295.07 0.395937874 0.000288386 | 4.664319445
| 5.039609578
| 5.432770394
| 5.879544281
| 6.344189191
| 6.844575808
| 7.398575836
| 7.98831723
| 8.631671354
| 9.310767526
| 10.06134779
| 10.86554079
| 11.72334651
| 12.65263702
| 13.67128093
| 14.76140894
| 15.94089173
| 17.20973066
| 18.58579369
| 20.06908354
| 21.65959748
| 23.39307962
| 25.25166062
| 27.27107913
| 29.45133516
| 31.79242869
| 34.33010654
| 37.06436055
| 40.03094025
| 43.22984018
| 46.67893786
| 50.39609442
| 54.4170594
| 58.75969939
| 63.44189191
| 68.49937012
| 73.96788359
| 79.86529889
| 86.24523218
| 93.12554458
| 100.5598686
| 108.5660545
| 117.2334679
|
|
 |
TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020
|
|
SiNPT60 | Sample: SiNPT60
NHA | Operator: NHA
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT60. | File: C:\TriStar II 3020\data\SAMPEL\2019\J
|
|
1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1
1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1
0.2550 g Warm Free Sp11.3393 cm³ Measured | Sample Mass:0.2550 g
32.8928 cm³ Equilibration In5 s | Cold Free Spa32.8928 cm³
None Sample Densit1.000 g/cm³ | Low Pressure None
No | Automatic DegNo
|
|
|
|
|
|
|
|
|
Porosity Distribution by Original Density Functional Theor | Porosity Distribution by Original Density
Model: N2 @ 77K on Carbon, Slit Pores | Model: N2 @ 77K on Carbon, Slit Pores
Method: Non-negative Regularization: 0.00000 | Method: Non-negative Regularization:
Standard Deviation of Fit: 1.00869 cm³/g STP |
|
|
|
| Standard Deviation of Fit: 1.00869 cm³/
< 1.483 nm : 0.01487 cm³/ |
<= 117.233 nm : 0.31777 cm³/ |
> 117.233 nm : 21.962 m²/g | Isotherm Table
>= 1.483 nm : 90.339 m²/g | Relative Pressure
| (P/Po) Experimental
| 0.01178367 28.86491828
ore Size Table | 0.01451552 29.3818598
| 0.017706521 29.98362025
Cumulative VoIncremental VoCumulative AreIncremental Ar| 0.02139844 30.67617713
0.015152287 0.000285818 0.385383481 0.385383481 | 0.02563123 31.46399486
0.01703532 0.001883033 2.75321103 2.367827549 | 0.03044224 32.34937068
0.019042397 0.002007077 5.092991267 2.339780236 | 0.035865448 33.3316487
0.02065411 0.001611713 6.827340275 1.734349008 | 0.041930798 34.40630608
0.02065411 0 6.827340275 0| 0.048663601 35.56391013
0.02065411 0 6.827340275 0| 0.056084011 36.78895824
0.02065411 0 6.827340275 0| 0.064206667 38.05864658
0.02065411 0 6.827340275 0| 0.073040441 39.34159595
0.022629388 0.001975278 8.272177736 1.444837461 | 0.082588248 40.59658776
0.02449541 0.001866022 9.537831846 1.26565411 | 0.092847057 41.77139358
0.026368327 0.001872918 10.71538603 1.177554188 | 0.103808001 42.80175754
0.02817612 0.001807793 11.76911679 1.053730754 | 0.115456402 43.69
0.02947067 0.00129455 12.46900813 0.699891344 | 0.127772301 44.60274576
0.032010177 0.002539507 13.73778028 1.26877215 | 0.140730694 45.54563511
0.035478107 0.00346793 15.34153224 1.603751961 | 0.154301897 46.51386408
0.040513764 0.005035656 17.50075666 2.159224417 | 0.168452203 47.5022936
0.046136793 0.005623029 19.73229023 2.231533567 | 0.183144197 48.50559143
0.052715127 0.006578334 22.15401385 2.421723617 | 0.198337302 49.51831981
0.060824114 0.008108987 24.91238646 2.75837261 | 0.213988706 50.53504442
0.068705286 0.007881172 27.39691896 2.484532507 | 0.230053101 51.55445686
0.076338669 0.007633383 29.6274102 2.230491242 | 0.246484801 52.58693732
0.084127988 0.007789319 31.73303681 2.105626604 | 0.263235897 53.63745587
0.094135969 0.010007973 34.23869107 2.505654258 | 0.280259013 54.71138406
0.110025024 0.015889216 37.92029929 3.681608225 | 0.297506303 55.81482651
0.130182445 0.020157261 42.25018091 4.329881614 | 0.314930797 56.95196416
0.151181447 0.020999001 46.42437344 4.174192529 | 0.332486212 58.11872748
0.173733351 0.022551904 50.57546075 4.151087316 | 0.35012731 59.30991992
0.195700405 0.021967054 54.32303475 3.747573996 | 0.367810607 60.52022108
0.215794217 0.020093765 57.4992598 3.176225056 | 0.385494202 61.74422388
0.233267596 0.01747338 60.0554767 2.556216895 | 0.40313831 62.9765397
0.247757353 0.014489757 62.01867102 1.963194325 | 0.420704991 64.21830218
0.259168724 0.01141137 63.45038142 1.431710393 | 0.4381589 65.54
0.267762325 0.008593601 64.44907239 0.998690971 | 0.455466807 66.93796988
0.274937036 0.007174711 65.22113637 0.772063983 | 0.472598106 68.38161889
0.281271978 0.006334942 65.8524499 0.631313531 | 0.489524394 69.84185692
0.286899718 0.00562774 66.37210311 0.519653204 | 0.506219923 71.29355458
0.291940356 0.005040638 66.80305435 0.430951248 | 0.522661209 72.82569987
0.296452331 0.004511976 67.16041505 0.357360698 | 0.5388273 74.46596634
0.300446681 0.003994349 67.45335169 0.292936637 | 0.5546996 76.17500492
0.303115715 0.002669035 67.6346022 0.181250507 | 0.570261598 77.91669127
0.305441415 0.0023257 67.78090747 0.146305276 | 0.585499227 79.65838574
0.308125839 0.002684424 67.93729637 0.156388893 | 0.60040009 81.37224819
0.310392632 0.002266793 68.05961293 0.122316561 | 0.614954293 83.21911319
0.31235646 0.001963828 68.15772843 0.098115504 | 0.629153311 85.27289985
0.313672918 0.001316459 68.21863352 0.060905092 | 0.642990828 87.46536463
0.314816534 0.001143616 68.26763274 0.048999219 | 0.656461716 89.73600931
0.316092868 0.001276334 68.31828483 0.050652083 | 0.669562697 92.03197455
0.31699659 0.000903722 68.35149949 0.033214664 | 0.682291925 94.30767439
0.317487551 0.000490961 68.3682103 0.016710814 | 0.694648683 96.52436372
0.31777201 0.000284459 68.37717784 0.00896754 | 0.706633508 98.653052
0.31777201 0 68.37717784 0| 0.71824801 100.8218187
0.31777201 0 68.37717784 0| 0.729494929 103.1449181
0.31777201 0 68.37717784 0| 0.740377605 105.6634868
0.31777201 0 68.37717784 0| 0.750900388 108.4079406
0.31777201 0 68.37717784 0| 0.761068285 111.3991725
0.31777201 0 68.37717784 0| 0.770887017 114.6497962
0.31777201 0 68.37717784 0| 0.780362606 118.1651715
0.31777201 0 68.37717784 0| 0.789501607 121.9445547
| 0.798311174 125.9821604
| 0.806798697 130.4477903
| 0.814971626 135.6058465
| 0.822837889 141.2446353
| 0.830405474 147.1721251
| 0.837682605 153.2291479
| 0.844677329 159.2850683
| 0.851397991 165.2345441
| 0.857852995 170.9940392
| 0.864050388 176.4984684
| 0.869998574 181.6991667
| 0.875705481 186.5607737
| 0.881179392 191.0598431
| 0.886428118 195.1822621
| 0.891459525 198.9220649
| 0.896281302 202.2797977
| 0.9009009 205.2612416
| 0.90532577 207.88
| 0.909563184 210.3052601
| 0.913620114 212.6271852
| 0.917503417 214.8497368
| 0.921219707 216.9767013
| 0.924775481 219.0117973
| 0.928177178 220.9587089
| 0.931430817 222.8208817
| 0.934542298 224.601693
| 0.937517405 226.3044518
| 0.940361619 227.9322965
| 0.943080306 229.4882975
| 0.945678592 230.9753885
| 0.948161721 232.3965716
| 0.950534225 233.7544393
| 0.95280093 235.051755
| 0.954966187 236.2910089
| 0.957034409 237.4747254
| 0.959009588 238.6051902
| 0.960896015 239.6848595
| 0.962697208 240.715746
| 0.964416981 241.7
| 0.96605891 242.6397672
| 0.967626274 243.5368251
| 0.969122529 244.3931851
| 0.970550597 245.2105189
| 0.971913695 245.9906685
| 0.973214507 246.7351692
| 0.974455774 247.4455902
| 0.975640416 248.123603
| 0.976770699 248.7705039
| 0.977849126 249.3877259
| 0.978878021 249.9765992
| 0.979859591 250.5383861
| 0.980795979 251.0743147
| 0.981689274 251.585579
| 0.982541502 252.0733388
| 0.98335427 252.5385153
| 0.984129488 252.9822001
| 0.984869003 253.4054506
| 0.985574186 253.8090516
| 0.986246824 254.1940264
| 0.986888289 254.5611597
| 0.987500012 254.9112701
| 0.988083303 255.2451083
| 0.988639593 255.5634929
| 0.989170074 255.8671061
|
|
 |
Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108
|
|
| Sample: SiNPT60
| Operator: NHA
| Submitter:
:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT60. | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan
|
|
Analysis AdsorN2 | Started: 1/24/2019 3:1 Analysis Adsor
Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath
Thermal Correc No | Report Time: 1/24/2019 7:1 Thermal Correc
Warm Free Sp11.3393 cm³ Measured | Sample Mass:0.2550 g Warm Free Sp
Equilibration In5 s | Cold Free Spa32.8928 cm³ Equilibration In
Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit
| Automatic DegNo
|
|
|
|
|
|
|
| Cumulative Surface Area vs. Pore Width
|
orosity Distribution by Original Density Functional Theor |
odel: N2 @ 77K on Carbon, Slit Pores | Cumulative Surface Area
ethod: Non-negative Regularization: 0.00000 | Pore Width (n Cumulative Surface Area (m²/g)
| 1.483289338 0.385383481
| 1.590515054 2.75321103
| 1.715611708 5.092991267
| 1.8585793 6.827340275
tandard Deviation of Fit: 1.00869 cm³/g STP | 2.001546978 6.827340275
| 2.16238568 6.827340275
| 2.341095234 6.827340275
| 2.519804789 6.827340275
| 2.734256221 8.272177736
Fitted Quantit Absolute ResidRelative Resid| 2.948707652 9.537831846
28.82481117 0.040107112 0.001389476 | 3.181030107 10.71538603
29.4257075 -0.0438477 -0.00149234 | 3.431223586 11.76911679
30.09586023 -0.11223997 -0.00374338 | 3.699287918 12.46900813
30.70315351 -0.02697637 -0.00087939 | 4.003093956 13.73778028
31.33657323 0.127421633 0.00404976 | 4.324771359 15.34153224
32.48609322 -0.13672254 -0.00422644 | 4.664319445 17.50075666
33.20434679 0.127301907 0.00381925 | 5.039609578 19.73229023
34.57336861 -0.16706254 -0.00485558 | 5.432770394 22.15401385
35.41915787 0.144752267 0.004070201 | 5.879544281 24.91238646
36.81662376 -0.02766551 -0.00075201 | 6.344189191 27.39691896
37.84535199 0.213294593 0.005604366 | 6.844575808 29.6274102
38.97216035 0.369435597 0.009390458 | 7.398575836 31.73303681
40.17840702 0.418180736 0.010300884 | 7.98831723 34.23869107
41.42066984 0.350723745 0.008396266 | 8.631671354 37.92029929
42.64713901 0.154618533 0.003612434 | 9.310767526 42.25018091
43.81901414 -0.12894358 -0.00295132 | 10.06134779 46.42437344
44.91887882 -0.31613305 -0.00708775 | 10.86554079 50.57546075
45.94588855 -0.40025344 -0.00878796 | 11.72334651 54.32303475
46.90794592 -0.39408184 -0.00847235 | 12.65263702 57.4992598
47.81625854 -0.31396493 -0.00660947 | 13.67128093 60.0554767
48.68261069 -0.17701926 -0.00364946 | 14.76140894 62.01867102
49.51829701 2.28029E-05 4.60494E-07 | 15.94089173 63.45038142
50.33396862 0.201075802 0.003978938 | 17.20973066 64.44907239
51.78313725 -0.22868039 -0.00443571 | 18.58579369 65.22113637
52.58243972 0.004497604 8.55268E-05 | 20.06908354 65.8524499
53.38898995 0.248465922 0.004632321 | 21.65959748 66.37210311
54.83358636 -0.1222023 -0.00223358 | 23.39307962 66.80305435
55.67524581 0.139580697 0.002500782 | 25.25166062 67.16041505
57.19660699 -0.24464284 -0.0042956 | 27.27107913 67.45335169
58.10494919 0.013778295 0.000237072 | 29.45133516 67.6346022
59.05910407 0.250815849 0.004228902 | 31.79242869 67.78090747
60.6950939 -0.17487282 -0.00288949 | 34.33010654 67.93729637
61.73148473 0.012739143 0.000206321 | 37.06436055 68.05961293
62.79913642 0.177403283 0.002816974 | 40.03094025 68.15772843
64.33888741 -0.12058522 -0.00187774 | 43.22984018 68.21863352
65.40911564 0.130921555 0.001997581 | 46.67893786 68.26763274
67.38291329 -0.44494341 -0.0066471 | 50.39609442 68.31828483
68.39238934 -0.01077045 -0.0001575 | 54.4170594 68.35149949
69.36973578 0.472121143 0.00675986 | 58.75969939 68.3682103
71.60148652 -0.30793194 -0.00431921 | 63.44189191 68.37717784
72.51041115 0.315288722 0.004329361 | 68.49937012 68.37717784
75.3205172 -0.85455086 -0.01147572 | 73.96788359 68.37717784
76.18197321 -0.0069683 -9.14773E-05 | 79.86529889 68.37717784
77.03860479 0.878086475 0.011269555 | 86.24523218 68.37717784
80.08776615 -0.42938041 -0.00539027 | 93.12554458 68.37717784
80.93865822 0.433589974 0.005328475 | 100.5598686 68.37717784
84.43614957 -1.21703639 -0.01462448 | 108.5660545 68.37717784
85.30419131 -0.03129146 -0.00036696 | 117.2334679 68.37717784
86.19842743 1.266937199 0.014485016 |
90.42184277 -0.68583347 -0.00764279 |
91.34312109 0.688853456 0.007484936 |
95.564926 -1.25725161 -0.01333138 |
96.49 0.03430951 0.000355449 |
97.41433264 1.238719361 0.012556321 |
101.5477975 -0.7259788 -0.00720061 |
102.4189568 0.725961355 0.007038266 |
106.6307503 -0.9672635 -0.00915419 |
107.4399157 0.968024888 0.008929465 |
112.6459134 -1.24674085 -0.01119165 |
113.4017205 1.248075764 0.010885983 |
121.3089049 -3.14373345 -0.02660457 |
122.020919 -0.07636426 -0.00062622 |
122.7376721 3.244488228 0.025753553 |
132.6785207 -2.23073046 -0.01710056 |
133.3731223 2.232724181 0.016464808 |
143.8663964 -2.62176106 -0.01856185 |
144.5469913 2.625133814 0.017837167 |
155.9286362 -2.69948833 -0.01761733 |
156.5824819 2.702586397 0.016966979 |
167.8116414 -2.57709724 -0.0155966 |
168.4155856 2.578453617 0.015079202 |
178.8284416 -2.3299732 -0.0132011 |
179.3702317 2.328935044 0.012817533 |
188.5678868 -2.00711314 -0.01075849 |
189.0556043 2.004238776 0.01049011 |
196.8282676 -1.64600547 -0.00843317 |
197.2802865 1.641778328 0.008253375 |
203.554754 -1.27495632 -0.00630293 |
203.9913057 1.269935869 0.006186925 |
208.8760529 -0.9960148 -0.0047913 |
209.3145864 0.990673678 0.004710646 |
213.5170261 -0.88984085 -0.00418498 |
213.9649843 0.884752464 0.004118006 |
217.7719831 -0.7952818 -0.00366529 |
218.2213835 0.790413731 0.003609001 |
221.6762128 -0.71750396 -0.00324723 |
222.1081953 0.71268637 0.003198472 |
225.251982 -0.65028901 -0.0028953 |
225.6588024 0.645649393 0.002853012 |
228.5176735 -0.585377 -0.00256821 |
228.9074034 0.580894166 0.002531258 |
231.4940509 -0.51866238 -0.00224553 |
231.8821455 0.514426129 0.00221357 |
233.7591051 -0.00466576 -1.996E-05 |
235.4658396 -0.41408459 -0.00176167 |
235.8805423 0.410466617 0.001737123 |
237.8241847 -0.3494593 -0.00147156 |
238.2591203 0.346069947 0.001450387 |
239.98584 -0.30098047 -0.00125573 |
240.4179811 0.297764853 0.001236998 |
241.9654547 -0.26542171 -0.00109815 |
242.377367 0.262400201 0.001081439 |
243.5399074 -0.00308232 -1.26565E-05 |
244.6030661 -0.20988104 -0.00085878 |
245.0032295 0.207289356 0.000845353 |
246.1547121 -0.16404362 -0.00066687 |
246.5735491 0.161620087 0.000655035 |
247.5580513 -0.11246115 -0.00045449 |
248.0134118 0.11019116 0.000444098 |
248.7726942 -0.0021903 -8.80446E-06 |
249.4167389 -0.02901305 -0.00011634 |
249.8879423 0.088656889 0.000354661 |
250.3491024 0.189283651 0.000755508 |
250.7999373 0.274377423 0.001092814 |
251.2452822 0.340296779 0.001352608 |
251.6909109 0.382427949 0.00151713 |
252.1453899 0.393125447 0.001556695 |
252.6179509 0.3642492 0.001439821 |
253.113386 0.292064613 0.001152559 |
253.6327958 0.176255792 0.000694442 |
254.1676019 0.026424504 0.000103954 |
254.6834042 -0.1222445 -0.00048022 |
255.2307202 -0.31945008 -0.00125318 |
255.7434538 -0.49834553 -0.00195242 |
256.251825 -0.6883321 -0.00269339 |
256.7609244 -0.89381824 -0.00349329 |
|
|
 | |
Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 |
| |
| |
| Sample: SiNPT60 |
| Operator: NHA |
| Submitter: |
0\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan |
| |
| |
N2 | Started: 1/24/2019 3:1 Analysis AdsorN2 |
-195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C |
No | Report Time: 1/24/2019 7:1 Thermal Correc No |
11.3393 cm³ M| Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M|
5s | Cold Free Spa32.8928 cm³ Equilibration In5 s |
1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³ |
| Automatic DegNo |
| |
| |
| |
| |
| |
| |
| |
| Incremental Surface Area vs. Pore Width |
| |
| |
| Incremental Surface Area |
ace Area (m²/g) | Pore Width (n Incremental Surface Area (m²/g) |
| 1.483289338 0.385383481 |
| 1.590515054 2.367827549 |
| 1.715611708 2.339780236 |
| 1.8585793 1.734349008 |
| 2.001546978 0 |
| 2.16238568 0 |
| 2.341095234 0 |
| 2.519804789 0 |
| 2.734256221 1.444837461 |
| 2.948707652 1.26565411 |
| 3.181030107 1.177554188 |
| 3.431223586 1.053730754 |
| 3.699287918 0.699891344 |
| 4.003093956 1.26877215 |
| 4.324771359 1.603751961 |
| 4.664319445 2.159224417 |
| 5.039609578 2.231533567 |
| 5.432770394 2.421723617 |
| 5.879544281 2.75837261 |
| 6.344189191 2.484532507 |
| 6.844575808 2.230491242 |
| 7.398575836 2.105626604 |
| 7.98831723 2.505654258 |
| 8.631671354 3.681608225 |
| 9.310767526 4.329881614 |
| 10.06134779 4.174192529 |
| 10.86554079 4.151087316 |
| 11.72334651 3.747573996 |
| 12.65263702 3.176225056 |
| 13.67128093 2.556216895 |
| 14.76140894 1.963194325 |
| 15.94089173 1.431710393 |
| 17.20973066 0.998690971 |
| 18.58579369 0.772063983 |
| 20.06908354 0.631313531 |
| 21.65959748 0.519653204 |
| 23.39307962 0.430951248 |
| 25.25166062 0.357360698 |
| 27.27107913 0.292936637 |
| 29.45133516 0.181250507 |
| 31.79242869 0.146305276 |
| 34.33010654 0.156388893 |
| 37.06436055 0.122316561 |
| 40.03094025 0.098115504 |
| 43.22984018 0.060905092 |
| 46.67893786 0.048999219 |
| 50.39609442 0.050652083 |
| 54.4170594 0.033214664 |
| 58.75969939 0.016710814 |
| 63.44189191 0.00896754 |
| 68.49937012 0 |
| 73.96788359 0 |
| 79.86529889 0 |
| 86.24523218 0 |
| 93.12554458 0 |
| 100.5598686 0 |
| 108.5660545 0 |
| 117.2334679 0 |
| |
 |
TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020
|
|
Sample: SiNPT60 | Sample: SiNPT60
Operator: NHA | Operator: NHA
Submitter: | Submitter:
File: C:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\J
|
|
Started: 1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1
Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1
Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1
Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M| Sample Mass:0.2550 g
Cold Free Spa32.8928 cm³ Equilibration In5 s | Cold Free Spa32.8928 cm³
Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure None
Automatic DegNo | Automatic DegNo
|
|
|
|
|
|
|
Differential Surface Area vs. Pore Width | Cumulative Pore Volume vs. Pore Width
|
|
Differential Surface Area | Cumulative Pore Volume
Pore Width (n Differential Surface Area (m²/g) | Pore Width (n Cumulative Pore Volume (cm³/g)
1.483289338 12.71392977 | 1.483289338 0.015152287
1.590515054 74.93940196 | 1.590515054 0.01703532
1.715611708 69.17994299 | 1.715611708 0.019042397
1.8585793 51.81276347 | 1.8585793 0.02065411
2.001546978 0 | 2.001546978 0.02065411
2.16238568 0 | 2.16238568 0.02065411
2.341095234 0 | 2.341095234 0.02065411
2.519804789 0 | 2.519804789 0.02065411
2.734256221 42.33036767 | 2.734256221 0.022629388
2.948707652 38.51153602 | 2.948707652 0.02449541
3.181030107 35.78251181 | 3.181030107 0.026368327
3.431223586 32.15026868 | 3.431223586 0.02817612
3.699287918 20.90889215 | 3.699287918 0.02947067
4.003093956 37.40207266 | 4.003093956 0.032010177
4.324771359 48.31123681 | 4.324771359 0.035478107
4.664319445 65.00384909 | 4.664319445 0.040513764
5.039609578 67.38427655 | 5.039609578 0.046136793
5.432770394 72.3477328 | 5.432770394 0.052715127
5.879544281 81.90577769 | 5.879544281 0.060824114
6.344189191 75.28558732 | 6.344189191 0.068705286
6.844575808 66.80917469 | 6.844575808 0.076338669
7.398575836 62.75265525 | 7.398575836 0.084127988
 7.98831723 74.85512384 | 7.98831723 0.094135969
8.631671354 110.6748313 | 8.631671354 0.110025024
9.310767526 130.102143 | 9.310767526 0.130182445
10.06134779 124.4803937 | 10.06134779 0.151181447
10.86554079 125.0413371 | 10.86554079 0.173733351
11.72334651 113.3401134 | 11.72334651 0.195700405
12.65263702 95.1569492 | 12.65263702 0.215794217
13.67128093 76.36566087 | 13.67128093 0.233267596
14.76140894 58.86339218 | 14.76140894 0.247757353
15.94089173 42.9644622 | 15.94089173 0.259168724
17.20973066 29.95990534 | 17.20973066 0.267762325
18.58579369 23.13180169 | 18.58579369 0.274937036
20.06908354 18.99565121 | 20.06908354 0.281271978
21.65959748 15.6146127 | 21.65959748 0.286899718
23.39307962 12.93379588 | 23.39307962 0.291940356
25.25166062 10.72914816 | 25.25166062 0.296452331
27.27107913 8.768583195 | 27.27107913 0.300446681
29.45133516 5.441211254 | 29.45133516 0.303115715
31.79242869 4.395521035 | 31.79242869 0.305441415
34.33010654 4.694050931 | 34.33010654 0.308125839
37.06436055 3.666528437 | 37.06436055 0.310392632
40.03094025 2.936397891 | 40.03094025 0.31235646
43.22984018 1.82555063 | 43.22984018 0.313672918
46.67893786 1.471155313 | 46.67893786 0.314816534
50.39609442 1.520761516 | 50.39609442 0.316092868
54.4170594 0.996200578 | 54.4170594 0.31699659
58.75969939 0.501517084 | 58.75969939 0.317487551
63.44189191 0.269267149 | 63.44189191 0.31777201
68.49937012 0 | 68.49937012 0.31777201
73.96788359 0 | 73.96788359 0.31777201
79.86529889 0 | 79.86529889 0.31777201
86.24523218 0 | 86.24523218 0.31777201
93.12554458 0 | 93.12554458 0.31777201
100.5598686 0 | 100.5598686 0.31777201
108.5660545 0 | 108.5660545 0.31777201
117.2334679 0 | 117.2334679 0.31777201
|
 |
Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1
|
|
| Sample: SiNPT60
| Operator: NHA
| Submitter:
:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan
|
|
Analysis AdsorN2 | Started: 1/24/2019 3:1 Analysis AdsorN2
Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C
Thermal Correc No | Report Time: 1/24/2019 7:1 Thermal CorrecNo
Warm Free Sp11.3393 cm³ M| Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M
Equilibration In5 s | Cold Free Spa32.8928 cm³ Equilibration In5 s
Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³
| Automatic DegNo
|
|
|
|
|
|
|
e Volume vs. Pore Width | Incremental Pore Volume vs. Pore Width
|
|
| Incremental Pore Volume
umulative Pore Volume (cm³/g) | Pore Width (n Incremental Pore Volume (cm³/g)
| 1.483289338 0.000285818
| 1.590515054 0.001883033
| 1.715611708 0.002007077
| 1.8585793 0.001611713
| 2.001546978 0
| 2.16238568 0
| 2.341095234 0
| 2.519804789 0
| 2.734256221 0.001975278
| 2.948707652 0.001866022
| 3.181030107 0.001872918
| 3.431223586 0.001807793
| 3.699287918 0.00129455
| 4.003093956 0.002539507
| 4.324771359 0.00346793
| 4.664319445 0.005035656
| 5.039609578 0.005623029
| 5.432770394 0.006578334
| 5.879544281 0.008108987
| 6.344189191 0.007881172
| 6.844575808 0.007633383
| 7.398575836 0.007789319
| 7.98831723 0.010007973
| 8.631671354 0.015889216
| 9.310767526 0.020157261
| 10.06134779 0.020999001
| 10.86554079 0.022551904
| 11.72334651 0.021967054
| 12.65263702 0.020093765
| 13.67128093 0.01747338
| 14.76140894 0.014489757
| 15.94089173 0.01141137
| 17.20973066 0.008593601
| 18.58579369 0.007174711
| 20.06908354 0.006334942
| 21.65959748 0.00562774
| 23.39307962 0.005040638
| 25.25166062 0.004511976
| 27.27107913 0.003994349
| 29.45133516 0.002669035
| 31.79242869 0.0023257
| 34.33010654 0.002684424
| 37.06436055 0.002266793
| 40.03094025 0.001963828
| 43.22984018 0.001316459
| 46.67893786 0.001143616
| 50.39609442 0.001276334
| 54.4170594 0.000903722
| 58.75969939 0.000490961
| 63.44189191 0.000284459
| 68.49937012 0
| 73.96788359 0
| 79.86529889 0
| 86.24523218 0
| 93.12554458 0
| 100.5598686 0
| 108.5660545 0
| 117.2334679 0
|
| |
| TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
| |
| |
| Sample: SiNPT60 | Sample:
| Operator: NHA | Operator:
| Submitter: | Submitter:
| File: C:\TriStar II 3020\data\SAMPEL\2019\Jan | File:
| |
| |
| Started: 1/24/2019 3:1 Analysis AdsorN2 | Started:
| Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
| Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time:
| Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M| Sample Mass:
| Cold Free Spa32.8928 cm³ Equilibration In5 s | Cold Free Spa
| Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure
| Automatic DegNo | Automatic Deg
| |
| |
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| |
| |
| |
| |
| Differential Pore Volume vs. Pore Width | Goodness of Fit
| | Standard Deviation of Fit: 1.00869 cm³/
| |
| Differential Pore Volume | Input Data
| Pore Width (n Differential Pore Volume (cm³/g) | Relative Press
| 1.483289338 0.009429218 | 0.010332355
| 1.590515054 0.059596123 | 0.106943542
| 1.715611708 0.05934296 | 0.218510397
| 1.8585793 0.048149065 | 0.299682175
| 2.001546978 0 | 0.414845918
| 2.16238568 0 | 0.503686564
| 2.341095234 0 | 0.599124587
| 2.519804789 0 | 0.704529933
| 2.734256221 0.057871036 | 0.800250646
| 2.948707652 0.05677963 | 0.904589121
| 3.181030107 0.056912624 | 0.989353782
| 3.431223586 0.05515738 |
| 3.699287918 0.038674006 |
| 4.003093956 0.074862006 |
| 4.324771359 0.104467527 |
| 4.664319445 0.151599359 |
| 5.039609578 0.169795223 |
| 5.432770394 0.19652431 |
| 5.879544281 0.240784323 |
| 6.344189191 0.238813005 |
| 6.844575808 0.22864023 |
| 7.398575836 0.232140139 |
| 7.98831723 0.298983238 |
| 8.631671354 0.477654385 |
| 9.310767526 0.605675404 |
| 10.06134779 0.626220267 |
| 10.86554079 0.679320874 |
| 11.72334651 0.664362712 |
| 12.65263702 0.601993169 |
| 13.67128093 0.522008202 |
| 14.76140894 0.434453302 |
| 15.94089173 0.34244592 |
| 17.20973066 0.257800951 |
| 18.58579369 0.214961447 |
| 20.06908354 0.190612656 |
| 21.65959748 0.169103113 |
| 23.39307962 0.151280658 |
| 25.25166062 0.135464404 |
| 27.27107913 0.119564363 |
| 29.45133516 0.080125468 |
| 31.79242869 0.069872145 |
| 34.33010654 0.080573634 |
| 37.06436055 0.067948766 |
| 40.03094025 0.058773384 |
| 43.22984018 0.039459131 |
| 46.67893786 0.034335984 |
| 50.39609442 0.03832022 |
| 54.4170594 0.027105153 |
| 58.75969939 0.014734497 |
| 63.44189191 0.008541409 |
| 68.49937012 0 |
| 73.96788359 0 |
| 79.86529889 0 |
| 86.24523218 0 |
| 93.12554458 0 |
| 100.5598686 0 |
| 108.5660545 0 |
| 117.2334679 0 |
| |
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 |
TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108
|
|
SiNPT60 | Sample: SiNPT60
NHA | Operator: NHA
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan
|
|
1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1 Analysis Adsor
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath
1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1 Thermal Correc
0.2550 g Warm Free Sp11.3393 cm³ M| Sample Mass:0.2550 g Warm Free Sp
32.8928 cm³ Equilibration In5 s | Cold Free Spa32.8928 cm³ Equilibration In
None Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit
No | Automatic DegNo
|
|
|
|
|
|
|
oodness of Fit | Goodness of Fit
tandard Deviation of Fit: 1.00869 cm³/g STP | Standard Deviation of Fit: 1.00869 cm³/g STP
|
Model Fit | Input Data Model Fit
Quantity AdsoRelative PressQuantity Adso| Relative PressQuantity AdsoRelative Press
28.5897894 0.01178367 28.82481117 | 0.010332355 28.5897894 0.01178367
43.04985539 0.01451552 29.4257075 | 0.106943542 43.04985539 0.01451552
50.82373037 0.017706521 30.09586023 | 0.218510397 50.82373037 0.017706521
55.95558472 0.02139844 30.70315351 | 0.299682175 55.95558472 0.02139844
63.79905641 0.02563123 31.33657323 | 0.414845918 63.79905641 0.02563123
71.07175902 0.03044224 32.48609322 | 0.503686564 71.07175902 0.03044224
81.22463396 0.035865448 33.20434679 | 0.599124587 81.22463396 0.035865448
98.27979336 0.041930798 34.57336861 | 0.704529933 98.27979336 0.041930798
126.9262243 0.048663601 35.41915787 | 0.800250646 126.9262243 0.048663601
207.4584275 0.056084011 36.81662376 | 0.904589121 207.4584275 0.056084011
255.9722486 0.064206667 37.84535199 | 0.989353782 255.9722486 0.064206667
0.073040441 38.97216035 | 0.073040441
0.082588248 40.17840702 | 0.082588248
0.092847057 41.42066984 | 0.092847057
0.103808001 42.64713901 | 0.103808001
0.115456402 43.81901414 | 0.115456402
0.127772301 44.91887882 | 0.127772301
0.140730694 45.94588855 | 0.140730694
0.154301897 46.90794592 | 0.154301897
0.168452203 47.81625854 | 0.168452203
0.183144197 48.68261069 | 0.183144197
0.198337302 49.51829701 | 0.198337302
0.213988706 50.33396862 | 0.213988706
0.230053101 51.78313725 | 0.230053101
0.246484801 52.58243972 | 0.246484801
0.263235897 53.38898995 | 0.263235897
0.280259013 54.83358636 | 0.280259013
0.297506303 55.67524581 | 0.297506303
0.314930797 57.19660699 | 0.314930797
0.332486212 58.10494919 | 0.332486212
0.35012731 59.05910407 | 0.35012731
0.367810607 60.6950939 | 0.367810607
0.385494202 61.73148473 | 0.385494202
0.40313831 62.79913642 | 0.40313831
0.420704991 64.33888741 | 0.420704991
0.4381589 65.40911564 | 0.4381589
0.455466807 67.38291329 | 0.455466807
0.472598106 68.39238934 | 0.472598106
0.489524394 69.36973578 | 0.489524394
0.506219923 71.60148652 | 0.506219923
0.522661209 72.51041115 | 0.522661209
0.5388273 75.3205172 | 0.5388273
0.5546996 76.18197321 | 0.5546996
0.570261598 77.03860479 | 0.570261598
0.585499227 80.08776615 | 0.585499227
0.60040009 80.93865822 | 0.60040009
0.614954293 84.43614957 | 0.614954293
0.629153311 85.30419131 | 0.629153311
0.642990828 86.19842743 | 0.642990828
0.656461716 90.42184277 | 0.656461716
0.669562697 91.34312109 | 0.669562697
0.682291925 95.564926 | 0.682291925
0.694648683 96.49 | 0.694648683
0.706633508 97.41433264 | 0.706633508
0.71824801 101.5477975 | 0.71824801
0.729494929 102.4189568 | 0.729494929
0.740377605 106.6307503 | 0.740377605
0.750900388 107.4399157 | 0.750900388
0.761068285 112.6459134 | 0.761068285
0.770887017 113.4017205 | 0.770887017
0.780362606 121.3089049 | 0.780362606
0.789501607 122.020919 | 0.789501607
0.798311174 122.7376721 | 0.798311174
0.806798697 132.6785207 | 0.806798697
0.814971626 133.3731223 | 0.814971626
0.822837889 143.8663964 | 0.822837889
0.830405474 144.5469913 | 0.830405474
0.837682605 155.9286362 | 0.837682605
0.844677329 156.5824819 | 0.844677329
0.851397991 167.8116414 | 0.851397991
0.857852995 168.4155856 | 0.857852995
0.864050388 178.8284416 | 0.864050388
0.869998574 179.3702317 | 0.869998574
0.875705481 188.5678868 | 0.875705481
0.881179392 189.0556043 | 0.881179392
0.886428118 196.8282676 | 0.886428118
0.891459525 197.2802865 | 0.891459525
0.896281302 203.554754 | 0.896281302
0.9009009 203.9913057 | 0.9009009
0.90532577 208.8760529 | 0.90532577
0.909563184 209.3145864 | 0.909563184
0.913620114 213.5170261 | 0.913620114
0.917503417 213.9649843 | 0.917503417
0.921219707 217.7719831 | 0.921219707
0.924775481 218.2213835 | 0.924775481
0.928177178 221.6762128 | 0.928177178
0.931430817 222.1081953 | 0.931430817
0.934542298 225.251982 | 0.934542298
0.937517405 225.6588024 | 0.937517405
0.940361619 228.5176735 | 0.940361619
0.943080306 228.9074034 | 0.943080306
0.945678592 231.4940509 | 0.945678592
0.948161721 231.8821455 | 0.948161721
0.950534225 233.7591051 | 0.950534225
0.95280093 235.4658396 | 0.95280093
0.954966187 235.8805423 | 0.954966187
0.957034409 237.8241847 | 0.957034409
0.959009588 238.2591203 | 0.959009588
0.960896015 239.98584 | 0.960896015
0.962697208 240.4179811 | 0.962697208
0.964416981 241.9654547 | 0.964416981
0.96605891 242.377367 | 0.96605891
0.967626274 243.5399074 | 0.967626274
0.969122529 244.6030661 | 0.969122529
0.970550597 245.0032295 | 0.970550597
0.971913695 246.1547121 | 0.971913695
0.973214507 246.5735491 | 0.973214507
0.974455774 247.5580513 | 0.974455774
0.975640416 248.0134118 | 0.975640416
0.976770699 248.7726942 | 0.976770699
0.977849126 249.4167389 | 0.977849126
0.978878021 249.8879423 | 0.978878021
0.979859591 250.3491024 | 0.979859591
0.980795979 250.7999373 | 0.980795979
0.981689274 251.2452822 | 0.981689274
0.982541502 251.6909109 | 0.982541502
0.98335427 252.1453899 | 0.98335427
0.984129488 252.6179509 | 0.984129488
0.984869003 253.113386 | 0.984869003
0.985574186 253.6327958 | 0.985574186
0.986246824 254.1676019 | 0.986246824
0.986888289 254.6834042 | 0.986888289
0.987500012 255.2307202 | 0.987500012
0.988083303 255.7434538 | 0.988083303
0.988639593 256.251825 | 0.988639593
0.989170074 256.7609244 | 0.989170074
|
 | |
Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 |
| |
| |
| Sample: SiNPT60 |
| Operator: NHA |
| Submitter: |
0\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan |
| |
| |
N2 | Started: 1/24/2019 3:1 Analysis AdsorN2 |
-195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C |
No | Report Time: 1/24/2019 7:1 Thermal Correc No |
11.3393 cm³ M| Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M|
5s | Cold Free Spa32.8928 cm³ Equilibration In5 s |
1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³ |
| Automatic DegNo |
| |
| |
| |
| |
| |
| |
| |
| |
869 cm³/g STP | |
| Surface Energy Distribution by Modified De|
| Model: N2 @ 77K, Surface Energy Distribut|
Quantity Adso| Method: Non-negative Regularization: 0.0 |
28.82481117 | Standard Deviation of Fit: 0.07469 cm³/g S |
29.4257075 | |
30.09586023 | |
30.70315351 | |
31.33657323 | |
32.48609322 | Total Area : 212.517 m²/g |
33.20434679 | |
34.57336861 | |
35.41915787 | Surface Energy Table |
36.81662376 | |
37.84535199 | Energy (e/k) Cumulative AreIncremental Area (m²/g) |
38.97216035 | 20 45.86764957 45.86764957 |
40.17840702 | 22 45.86764957 0 |
41.42066984 | 24 45.86764957 0 |
42.64713901 | 26 45.86764957 0 |
43.81901414 | 28 45.86764957 0 |
44.91887882 | 30 45.86764957 0 |
45.94588855 | 32 63.60544594 17.73779637 |
46.90794592 | 34 63.60544594 0 |
47.81625854 | 36 63.60544594 0 |
48.68261069 | 38 63.60544594 0 |
49.51829701 | 40 63.60544594 0 |
50.33396862 | 42 63.60544594 0 |
51.78313725 | 44 130.2554326 66.64998668 |
52.58243972 | 46 130.2554326 0 |
53.38898995 | 48 130.2554326 0 |
54.83358636 | 50 130.2554326 0 |
55.67524581 | 52 130.2554326 0 |
57.19660699 | 54 130.2554326 0 |
58.10494919 | 56 130.2554326 0 |
59.05910407 | 58 142.4671391 12.21170645 |
60.6950939 | 60 142.4671391 0 |
61.73148473 | 62 142.4671391 0 |
62.79913642 | 64 159.2017392 16.73460009 |
64.33888741 | 66 159.2017392 0 |
65.40911564 | 68 159.2017392 0 |
67.38291329 | 70 168.1902533 8.988514095 |
68.39238934 | 72 168.1902533 0 |
69.36973578 | 74 168.1902533 0 |
71.60148652 | 76 168.1902533 0 |
72.51041115 | 78 168.1902533 0 |
75.3205172 | 80 168.1902533 0 |
76.18197321 | 82 175.1251424 6.934889144 |
77.03860479 | 84 175.1251424 0 |
80.08776615 | 86 191.901333 16.7761906 |
80.93865822 | 88 191.901333 0 |
84.43614957 | 90 191.901333 0 |
85.30419131 | 92 199.0570532 7.155720197 |
86.19842743 | 94 199.0570532 0 |
90.42184277 | 96 199.0570532 0 |
91.34312109 | 98 199.0570532 0 |
95.564926 | 100 212.5172387 13.46018552 |
96.49 | |
97.41433264 | |
101.5477975 | |
102.4189568 | |
106.6307503 | |
107.4399157 | |
112.6459134 | |
113.4017205 | |
121.3089049 | |
122.020919 | |
122.7376721 | |
132.6785207 | |
133.3731223 | |
143.8663964 | |
144.5469913 | |
155.9286362 | |
156.5824819 | |
167.8116414 | |
168.4155856 | |
178.8284416 | |
179.3702317 | |
188.5678868 | |
189.0556043 | |
196.8282676 | |
197.2802865 | |
203.554754 | |
203.9913057 | |
208.8760529 | |
209.3145864 | |
213.5170261 | |
213.9649843 |
217.7719831 |
218.2213835 |
221.6762128 |
222.1081953 |
225.251982 |
225.6588024 |
228.5176735 |
228.9074034 |
231.4940509 |
231.8821455 |
233.7591051 |
235.4658396 |
235.8805423 |
237.8241847 |
238.2591203 |
239.98584 |
240.4179811 |
241.9654547 |
242.377367 |
243.5399074 |
244.6030661 |
245.0032295 |
246.1547121 |
246.5735491 |
247.5580513 |
248.0134118 |
248.7726942 |
249.4167389 |
249.8879423 |
250.3491024 |
250.7999373 |
251.2452822 |
251.6909109 |
252.1453899 |
252.6179509 |
253.113386 |
253.6327958 |
254.1676019 |
254.6834042 |
255.2307202 |
255.7434538 |
 256.251825 |
256.7609244 |
|
 |
TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
|
|
Sample: SiNPT60 | Sample:
Operator: NHA | Operator:
Submitter: | Submitter:
File: C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT60. | File:
|
|
Started: 1/24/2019 3:1 Analysis AdsorN2 | Started:
Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time:
Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ Measured | Sample Mass:
Cold Free Spa32.8928 cm³ Equilibration In5 s | Cold Free Spa
Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure
Automatic DegNo | Automatic Deg
|
|
|
|
|
|
|
| Cumulative Surface Area vs. Energy
|
Surface Energy Distribution by Modified Density Function |
Model: N2 @ 77K, Surface Energy Distribution | Cumulative Surface Area
Method: Non-negative Regularization: 0.00000 | Energy (e/k)
| 20
| 22
| 24
| 26
Standard Deviation of Fit: 0.07469 cm³/g STP | 28
| 30
| 32
Isotherm Table | 34
Relative Pressure | 36
(P/Po) Experimental Fitted Quantit Absolute ResidRelative Resid| 38
0.010592537 28.63913376 28.3835504 0.255583359 0.00892427 | 40
0.011220185 28.75813236 28.57818084 0.179951517 0.006257413 | 42
0.011885022 28.88412046 28.77058651 0.113533947 0.00393067 | 44
0.012589254 29.0174977 28.96136946 0.056128239 0.001934289 | 46
0.013335214 29.15868427 29.15112825 0.007556024 0.000259135 | 48
0.014125375 29.30812156 29.34048237 -0.03236081 -0.00110416 | 50
0.014962357 29.46627262 29.53 -0.06379949 -0.00216517 | 52
0.015848932 29.63362258 29.72055751 -0.08693494 -0.00293366 | 54
0.01678804 29.81067886 29.91266732 -0.10198846 -0.00342121 | 56
0.017782794 29.99797122 30.10719402 -0.1092228 -0.00364101 | 58
0.018836491 30.19605155 30.30500219 -0.10895064 -0.00360811 | 60
0.019952623 30.40549335 30.50710649 -0.10161314 -0.00334193 | 62
 0.02113489 30.62689078 30.71467535 -0.08778457 -0.00286626 | 64
0.022387211 30.86085735 30.92910253 -0.06824518 -0.00221138 | 66
0.023713737 31.10802387 31.15209775 -0.04407388 -0.0014168 | 68
0.025118864 31.36903581 31.38582657 -0.01679076 -0.00053527 | 70
0.026607251 31.64454967 31.63308289 0.011466777 0.000362362 | 72
0.028183829 31.93522839 31.89759765 0.037630741 0.001178346 | 74
0.029853826 32.24173537 32.18436904 0.057366337 0.001779257 | 76
0.031622777 32.56472702 32.49981891 0.064908113 0.001993203 | 78
0.033496544 32.90484329 32.85032754 0.05451575 0.00165677 | 80
0.035481339 33.26269607 33.23646608 0.026229988 0.000788571 | 82
0.03758374 33.63885473 33.64632895 -0.00747423 -0.00022219 | 84
0.039810717 34.0338284 34.06399405 -0.03016565 -0.00088634 | 86
0.04216965 34.44804437 34.48414161 -0.03609725 -0.00104788 | 88
0.044668359 34.88182158 34.91109839 -0.02927682 -0.00083931 | 90
0.047315126 35.33533862 35.35247334 -0.01713472 -0.00048492 | 92
0.050118723 35.80859478 35.81495641 -0.00636164 -0.00017766 | 94
0.053088444 36.30136304 36.30049068 0.000872364 2.40311E-05 | 96
0.056234133 36.81313334 36.80544495 0.007688391 0.000208849 | 98
0.059566214 37.34304417 37.32737779 0.015666384 0.000419526 | 100
0.063095734 37.88980037 37.86950353 0.020296838 0.000535681 |
0.066834392 38.45157431 38.43613949 0.015434815 0.000401409 |
0.070794578 39.02588736 39.02362835 0.002259001 5.78846E-05 |
0.074989421 39.60946777 39.61772156 -0.00825379 -0.00020838 |
0.079432823 40.1980805 40.20524513 -0.00716462 -0.00017823 |
0.084139514 40.78632356 40.78073927 0.005584287 0.000136916 |
0.089125094 41.36738442 41.34125587 0.026128554 0.000631622 |
0.094406088 41.93274899 41.88472127 0.048027722 0.001145351 |
0.1 42.47185393 42.41281328 0.05904065 0.001390112 |
0.105925373 42.97167159 42.9304939 0.04117769 0.000958252 |
0.112201845 43.44621109 43.44409818 0.002112913 4.86328E-05 |
0.118850223 43.94317377 43.96035714 -0.01718337 -0.00039104 |
0.125892541 44.46448482 44.48638018 -0.02189536 -0.00049242 |
0.133352143 45.01094449 45.0295308 -0.01858631 -0.00041293 |
0.141253754 45.58331826 45.59643402 -0.01311576 -0.00028773 |
0.149623566 46.18232399 46.19071422 -0.00839023 -0.00018168 |
0.158489319 46.80861686 46.81178444 -0.00316759 -6.76708E-05 |
0.167880402 47.46277184 47.45886387 0.003907971 8.23375E-05 |
0.177827941 48.14526322 48.13565536 0.009607858 0.00019956 |
0.188364909 48.85644069 48.8484842 0.00795649 0.000162854 |
0.199526231 49.59650166 49.59983829 -0.00333663 -6.72755E-05 |
0.211348904 50.3654591 50.38477951 -0.01932041 -0.0003836 |
0.223872114 51.16393142 51.19715528 -0.03322387 -0.00064936 |
0.237137371 52.00033759 52.03816988 -0.03783229 -0.00072754 |
0.251188643 52.88178853 52.91603867 -0.03425014 -0.00064767 |
0.266072506 53.81573189 53.83985149 -0.0241196 -0.00044819 |
0.281838293 54.81164431 54.81602207 -0.00437777 -7.98691E-05 |
0.298538262 55.88153478 55.8530008 0.028533978 0.000510616 |
0.316227766 57.03747073 56.96871465 0.068756079 0.001205455 |
0.334965439 58.28505892 58.18883296 0.096225959 0.001650954 |
0.354813389 59.62917135 59.53257447 0.096596873 0.00161996 |
0.375837404 61.07427124 61.00672035 0.067550888 0.001106045 |
0.398107171 62.62417639 62.62472659 -0.0005502 -8.78578E-06 |
0.421696503 64.29055889 64.40839729 -0.11783839 -0.0018329 |
0.446683592 66.21933006 66.37506613 -0.15573607 -0.00235182 |
0.473151259 68.42894143 68.5456352 -0.11669377 -0.00170533 |
0.501187234 70.85486507 70.96669226 -0.1118272 -0.00157826 |
0.530884444 73.64547315 73.69359823 -0.04812508 -0.00065347 |
0.562341325 77.02384597 76.74473491 0.279111056 0.003623697 |
|
|
 |
TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108
|
|
SiNPT60 | Sample: SiNPT60
NHA | Operator: NHA
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan
|
|
1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1 Analysis Adsor
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath
1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1 Thermal Correc
0.2550 g Warm Free Sp11.3393 cm³ M| Sample Mass:0.2550 g Warm Free Sp
32.8928 cm³ Equilibration In5 s | Cold Free Spa32.8928 cm³ Equilibration In
None Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit
No | Automatic DegNo
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|
umulative Surface Area vs. Energy | Incremental Surface Area vs. Energy
|
|
umulative Surface Area | Incremental Surface Area
Cumulative Surface Area (m²/g) | Energy (e/k) Incremental Surface Area (m²/g)
45.86764957 | 20 45.86764957
45.86764957 | 22 0
45.86764957 | 24 0
45.86764957 | 26 0
45.86764957 | 28 0
45.86764957 | 30 0
63.60544594 | 32 17.73779637
63.60544594 | 34 0
63.60544594 | 36 0
63.60544594 | 38 0
63.60544594 | 40 0
63.60544594 | 42 0
130.2554326 | 44 66.64998668
130.2554326 | 46 0
130.2554326 | 48 0
130.2554326 | 50 0
130.2554326 | 52 0
130.2554326 | 54 0
130.2554326 | 56 0
142.4671391 | 58 12.21170645
142.4671391 | 60 0
142.4671391 | 62 0
159.2017392 | 64 16.73460009
159.2017392 | 66 0
159.2017392 | 68 0
168.1902533 | 70 8.988514095
168.1902533 | 72 0
168.1902533 | 74 0
168.1902533 | 76 0
168.1902533 | 78 0
168.1902533 | 80 0
175.1251424 | 82 6.934889144
175.1251424 | 84 0
191.901333 | 86 16.7761906
191.901333 | 88 0
191.901333 | 90 0
199.0570532 | 92 7.155720197
199.0570532 | 94 0
199.0570532 | 96 0
199.0570532 | 98 0
212.5172387 | 100 13.46018552
|
 | |
Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 |
| |
| |
| Sample: SiNPT60 |
| Operator: NHA |
| Submitter: |
0\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan |
| |
| |
N2 | Started: 1/24/2019 3:1 Analysis AdsorN2 |
-195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C |
No | Report Time: 1/24/2019 7:1 Thermal Correc No |
11.3393 cm³ M| Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M|
5s | Cold Free Spa32.8928 cm³ Equilibration In5 s |
1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³ |
| Automatic DegNo |
| |
| |
| |
| |
| |
| |
| |
| Differential Surface Area vs. Energy |
| |
| |
| Differential Surface Area |
face Area (m²/g) | Energy (e/k) Differential Surface Area (m²/g-K) |
| 20 22.93382479 |
| 22 0 |
| 24 0 |
| 26 0 |
| 28 0 |
| 30 0 |
| 32 8.868898183 |
| 34 0 |
| 36 0 |
| 38 0 |
| 40 0 |
| 42 0 |
| 44 33.32499334 |
| 46 0 |
| 48 0 |
| 50 0 |
| 52 0 |
| 54 0 |
| 56 0 |
| 58 6.105853226 |
| 60 0 |
| 62 0 |
| 64 8.367300045 |
| 66 0 |
| 68 0 |
| 70 4.494257048 |
| 72 0 |
| 74 0 |
| 76 0 |
| 78 0 |
| 80 0 |
| 82 3.467444572 |
| 84 0 |
| 86 8.3880953 |
| 88 0 |
| 90 0 |
| 92 3.577860099 |
| 94 0 |
| 96 0 |
| 98 0 |
| 100 6.730078125 |
| |
|
|
|
|
|
|
|
|
|
|
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|
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|
|
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|
|
|
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|
|
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 |
TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020
|
|
Sample: SiNPT60 | Sample: SiNPT60
Operator: NHA | Operator: NHA
Submitter: | Submitter:
File: C:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\J
|
|
Started: 1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1
Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1
Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1
Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M| Sample Mass:0.2550 g
Cold Free Spa32.8928 cm³ Equilibration In5 s | Cold Free Spa32.8928 cm³
Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure None
Automatic DegNo | Automatic DegNo
|
|
|
|
|
|
|
Goodness of Fit | Goodness of Fit
Standard Deviation of Fit: 0.07469 cm³/g STP | Standard Deviation of Fit: 0.07469 cm³/g STP
|
Input Data Model Fit | Input Data
Relative PressQuantity AdsoRelative PressQuantity Adso| Relative PressQuantity Adso
0.010332355 28.5897894 0.010592537 28.3835504 | 0.010332355 28.5897894
0.106943542 43.04985539 0.011220185 28.57818084 | 0.106943542 43.04985539
0.218510397 50.82373037 0.011885022 28.77058651 | 0.218510397 50.82373037
0.299682175 55.95558472 0.012589254 28.96136946 | 0.299682175 55.95558472
0.414845918 63.79905641 0.013335214 29.15112825 | 0.414845918 63.79905641
0.503686564 71.07175902 0.014125375 29.34048237 | 0.503686564 71.07175902
0.599124587 81.22463396 0.014962357 29.53 | 0.599124587 81.22463396
0.704529933 98.27979336 0.015848932 29.72055751 | 0.704529933 98.27979336
0.800250646 126.9262243 0.01678804 29.91266732 | 0.800250646 126.9262243
0.904589121 207.4584275 0.017782794 30.10719402 | 0.904589121 207.4584275
0.989353782 255.9722486 0.018836491 30.30500219 | 0.989353782 255.9722486
0.019952623 30.50710649 |
0.02113489 30.71467535 |
0.022387211 30.92910253 |
0.023713737 31.15209775 |
0.025118864 31.38582657 |
0.026607251 31.63308289 |
0.028183829 31.89759765 |
0.029853826 32.18436904 |
0.031622777 32.49981891 |
0.033496544 32.85032754 |
0.035481339 33.23646608 |
 0.03758374 33.64632895 |
0.039810717 34.06399405 |
0.04216965 34.48414161 |
0.044668359 34.91109839 |
0.047315126 35.35247334 |
0.050118723 35.81495641 |
0.053088444 36.30049068 |
0.056234133 36.80544495 |
0.059566214 37.32737779 |
0.063095734 37.86950353 |
0.066834392 38.43613949 |
0.070794578 39.02362835 |
0.074989421 39.61772156 |
0.079432823 40.20524513 |
0.084139514 40.78073927 |
0.089125094 41.34125587 |
0.094406088 41.88472127 |
0.1 42.41281328 |
0.105925373 42.9304939 |
0.112201845 43.44409818 |
0.118850223 43.96035714 |
0.125892541 44.48638018 |
0.133352143 45.0295308 |
0.141253754 45.59643402 |
0.149623566 46.19071422 |
0.158489319 46.81178444 |
0.167880402 47.45886387 |
0.177827941 48.13565536 |
0.188364909 48.8484842 |
0.199526231 49.59983829 |
0.211348904 50.38477951 |
0.223872114 51.19715528 |
0.237137371 52.03816988 |
0.251188643 52.91603867 |
0.266072506 53.83985149 |
0.281838293 54.81602207 |
0.298538262 55.8530008 |
0.316227766 56.96871465 |
0.334965439 58.18883296 |
0.354813389 59.53257447 |
0.375837404 61.00672035 |
0.398107171 62.62472659 |
0.421696503 64.40839729 |
0.446683592 66.37506613 |
0.473151259 68.5456352 |
0.501187234 70.96669226 |
0.530884444 73.69359823 |
0.562341325 76.74473491 |
|
 |
Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108 Page 1
|
|
| Sample: SiNPT60
| Operator: NHA
| Submitter:
:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Jan
|
|
Analysis AdsorN2 | Started: 1/24/2019 3:1 Analysis AdsorN2
Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C
Thermal Correc No | Report Time: 1/24/2019 7:1 Thermal CorrecNo
Warm Free Sp11.3393 cm³ M| Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M
Equilibration In5 s | Cold Free Spa32.8928 cm³ Equilibration In5 s
Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit1.000 g/cm³
| Automatic DegNo
|
|
|
|
|
|
|
| Dubinin Reports
ion of Fit: 0.07469 cm³/g STP |
| 4035- Cannot calculate optimized Astakhov exponent:
Model Fit | 4031- Not enough points with a relative pressure in the r
Relative PressQuantity Adso| 4026- Cannot calculate Dubinin-Astakhov: bad least squa
0.010592537 28.3835504 | 1017- (INTERNAL) Cannot calculate Radushkevich: bad le
0.011220185 28.57818084 |
0.011885022 28.77058651 |
0.012589254 28.96136946 |
0.013335214 29.15112825 |
0.014125375 29.34048237 |
0.014962357 29.53 |
0.015848932 29.72055751 |
0.01678804 29.91266732 |
0.017782794 30.10719402 |
0.018836491 30.30500219 |
0.019952623 30.50710649 |
0.02113489 30.71467535 |
0.022387211 30.92910253 |
0.023713737 31.15209775 |
0.025118864 31.38582657 |
0.026607251 31.63308289 |
0.028183829 31.89759765 |
0.029853826 32.18436904 |
0.031622777 32.49981891 |
0.033496544 32.85032754 |
0.035481339 33.23646608 |
 0.03758374 33.64632895 |
0.039810717 34.06399405 |
0.04216965 34.48414161 |
0.044668359 34.91109839 |
0.047315126 35.35247334 |
0.050118723 35.81495641 |
0.053088444 36.30049068 |
0.056234133 36.80544495 |
0.059566214 37.32737779 |
0.063095734 37.86950353 |
0.066834392 38.43613949 |
0.070794578 39.02362835 |
0.074989421 39.61772156 |
0.079432823 40.20524513 |
0.084139514 40.78073927 |
0.089125094 41.34125587 |
0.094406088 41.88472127 |
0.1 42.41281328 |
0.105925373 42.9304939 |
0.112201845 43.44409818 |
0.118850223 43.96035714 |
0.125892541 44.48638018 |
0.133352143 45.0295308 |
0.141253754 45.59643402 |
0.149623566 46.19071422 |
0.158489319 46.81178444 |
0.167880402 47.45886387 |
0.177827941 48.13565536 |
0.188364909 48.8484842 |
0.199526231 49.59983829 |
0.211348904 50.38477951 |
0.223872114 51.19715528 |
0.237137371 52.03816988 |
0.251188643 52.91603867 |
0.266072506 53.83985149 |
0.281838293 54.81602207 |
0.298538262 55.8530008 |
0.316227766 56.96871465 |
0.334965439 58.18883296 |
0.354813389 59.53257447 |
0.375837404 61.00672035 |
0.398107171 62.62472659 |
0.421696503 64.40839729 |
0.446683592 66.37506613 |
0.473151259 68.5456352 |
0.501187234 70.96669226 |
0.530884444 73.69359823 |
0.562341325 76.74473491 |
|
|
| TriStar II 3020TriStar II 3020Serial #: 1108 Page 1
|
|
| Sample: SiNPT60
| Operator: NHA
| Submitter:
| File: C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT60.SMP
|
|
| Started: 1/24/2019 3:1 Analysis AdsorN2
| Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C
| Report Time: 1/24/2019 7:1 Thermal CorrecNo
| Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ Measured
| Cold Free Spa32.8928 cm³ Equilibration In5 s
| Low Pressure None Sample Densit1.000 g/cm³
| Automatic DegNo
|
|
|
|
|
|
|
| MP Tabular Report
|
| t = [ 13.99 / ( 0.034 - log(P/Po) ) ] ^ 0.5
|
|
|
|
| Total Pore Sur238.9150 m²/g
| Density Conver0.0015468
|
|
|
|
| Pore HydraulicAverage Pore Incremental PoCumulative PoDifferential P Incremental Po
| 0.000 - 1.343 0.671570746 0 0 0 0
| 1.343 - 1.360 1.351570746 0.141615858 0.141615858 8.400260471 104.7787236
| 1.360 - 1.380 1.37 2.3752E-15 0.141615858 1.1876E-13 1.73372E-12
| 1.380 - 1.400 1.39 0 0.141615858 0 0
| 1.400 - 1.420 1.41 -3.12582E-15 0.141615858 -1.56291E-13 -2.21689E-12
| 1.420 - 1.440 1.43 3.17015E-15 0.141615858 1.58508E-13 2.21689E-12
| 1.440 - 1.460 1.45 0 0.141615858 0 0
| 1.460 - 1.480 1.47 -3.25883E-15 0.141615858 -1.62941E-13 -2.21689E-12
| 1.480 - 1.500 1.49 3.30317E-15 0.141615858 1.65158E-13 2.21689E-12
| 1.500 - 1.520 1.51 -3.34751E-15 0.141615858 -1.67375E-13 -2.21689E-12
| 1.520 - 1.540 1.53 3.39185E-15 0.141615858 1.69592E-13 2.21689E-12
| 1.540 - 1.560 1.55 0 0.141615858 0 0
| 1.560 - 1.580 1.57 -3.48052E-15 0.141615858 -1.74026E-13 -2.21689E-12
| 1.580 - 1.600 1.59 3.52486E-15 0.141615858 1.76243E-13 2.21689E-12
| 1.600 - 1.620 1.61 -3.56919E-15 0.141615858 -1.7846E-13 -2.21689E-12
| 1.620 - 1.640 1.63 3.61352E-15 0.141615858 1.80677E-13 2.21689E-12
| 1.640 - 1.660 1.65 0 0.141615858 0 0
| 1.660 - 1.680 1.67 -3.70221E-15 0.141615858 -1.8511E-13 -2.21689E-12
| 1.680 - 1.700 1.69 3.74654E-15 0.141615858 1.87327E-13 2.21689E-12
| 1.700 - 1.720 1.71 0 0.141615858 0 0
| 1.720 - 1.740 1.73 -3.83522E-15 0.141615858 -1.91761E-13 -2.21689E-12
| 1.740 - 1.760 1.75 3.87956E-15 0.141615858 1.93978E-13 2.21689E-12
| 1.760 - 1.780 1.77 0 0.141615858 0 0
| 1.780 - 1.800 1.79 -3.96823E-15 0.141615858 -1.98412E-13 -2.21689E-12
| 1.800 - 1.820 1.81 4.01256E-15 0.141615858 2.00629E-13 2.21689E-12
| 1.820 - 1.840 1.83 0 0.141615858 0 0
| 1.840 - 1.860 1.85 -4.10125E-15 0.141615858 -2.05063E-13 -2.21689E-12
| 1.860 - 1.880 1.87 4.14558E-15 0.141615858 2.0728E-13 2.21689E-12
| 1.880 - 1.900 1.89 -4.18993E-15 0.141615858 -2.09496E-13 -2.21689E-12
|
|
| |
| TriStar II 3020TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020
| |
| |
| Sample: SiNPT60 | Sample:
| Operator: NHA | Operator:
| Submitter: | Submitter:
| File: C:\TriStar II 3020\data\SAMPEL\2019\Jan | File:
| |
| |
| Started: 1/24/2019 3:1 Analysis AdsorN2 | Started:
| Completed: 1/24/2019 7:1 Analysis Bath -195.850 °C | Completed:
| Report Time: 1/24/2019 7:1 Thermal Correc No | Report Time:
| Sample Mass:0.2550 g Warm Free Sp11.3393 cm³ M| Sample Mass:
| Cold Free Spa32.8928 cm³ Equilibration In5 s | Cold Free Spa
| Low Pressure None Sample Densit1.000 g/cm³ | Low Pressure
| Automatic DegNo | Automatic Deg
| |
| |
| |
| |
| |
| |
| |
| Options Report | Sample log
| |
| | Date
| | 1/24/2019
| Analysis Conditions | 1/24/2019
| | 1/24/2019
| | 1/24/2019
| | 1/24/2019
| Preparation | 1/24/2019
| |
| Fast evacuatioNo |
| Evacuation rat5.0 mmHg/s |
| Evacuation tim0.10 h |
| Leak test: No |
| Use TranSeal:No |
| |
| |
| Free Space |
| |
| Measured |
| Lower dewar foYes |
| Evacuation tim0.10 h |
| Outgas test: No |
| |
| |
| Po and Temperature |
| |
| Po and T type:Enter Po below. Enter the Analysis Bath T |
| Po: 760.000 mmHg |
| Temperature: -195.850 °C |
| |
| |
| Dosing |
| |
| Use first pressNo |
| Use maximumNo v |
| Target toleran 5.0% or 5.000 mmHg |
| |
| |
| Equilibration |
| |
| Equilibration 5 s |
| Minimum equili600 s |
| |
| |
| Sample Backfill |
| |
| Backfill at star Yes |
| Backfill at end Yes |
| Backfill gas: N2 |
| |
| |
| Adsorptive Properties |
| |
| Adsorptive: Nitrogen |
| Maximum manif 1,050.00 mmHg |
| Non-ideality fa0.0000620 |
| Density conver0.0015468 |
| Therm. tran. h 0.38600 nm |
| Molecular cros0.162 nm² |
| Adsorbate Mol2.00 |
| |
| |
| Inside diamete9.53 mm |
| |
| |
 |
TriStar II 3020Serial #: 1108 Page 1 | TriStar II 3020TriStar II 3020Serial #: 1108
|
|
SiNPT60 | Sample: SiNPT60
NHA | Operator: NHA
| Submitter:
C:\TriStar II 3020\data\SAMPEL\2019\Jan | File: C:\TriStar II 3020\data\SAMPEL\2019\Januari\SiNPT6
|
|
1/24/2019 3:1 Analysis AdsorN2 | Started: 1/24/2019 3:1 Analysis Adsor
1/24/2019 7:1 Analysis Bath -195.850 °C | Completed: 1/24/2019 7:1 Analysis Bath
1/24/2019 7:1 Thermal Correc No | Report Time: 1/24/2019 7:1 Thermal Correc
0.2550 g Warm Free Sp11.3393 cm³ M| Sample Mass:0.2550 g Warm Free Sp
32.8928 cm³ Equilibration In5 s | Cold Free Spa32.8928 cm³ Equilibration In
None Sample Densit1.000 g/cm³ | Low Pressure None Sample Densit
No | Automatic DegNo
|
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|
|
|
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| Validation Report
|
Time Log Message |
3:11:07 PM Started analysis of file SiNP |
3:11:07 PM System volume: 18.1544 cm³| Isotherm Reports
3:22:31 PM Pressure transducer zeroed. |
3:30:08 PM Measured free space on port| Free Space: Low free space values may be
3:41:17 PM Pressure transducer zeroed. | observed when using liquid argon or ice baths.
7:14:39 PM Finished a sample analysis |
| Po Passed
|
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| Pressure/Volu Passed
|
|
| Desorption Not within limits. Increase the sample mass, increase
| the equilibration interval, or check the free space.
|
|
|
|
| BET Reports
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| C Value: Passed
|
|
| Correlation Coe
Passed
|
|
| Surface area: Passed
|
|
| Pressure RangThe selected BET relative pressure range is outside th
| recommended values of 0.05 to 0.30.
|
|
|
|
 Page 1

0\data\SAMPEL\2019\Januari\SiNPT60.SMP

N2
-195.850 °C
No
11.3393 cm³ Measured
5s
1.000 g/cm³

values may be
using liquid argon or ice baths.

Increase the sample mass, increase

interval, or check the free space.
ET relative pressure range is outside the
alues of 0.05 to 0.30.