Perhitungan Piknometer

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LAMPIRAN

1.1 Perhitungan Densitas

Volume piknometer = 25 ml
Piknometer kosong = 16,86 gr
Rumus ρ = Piknometer isi – Piknometer kosong
Volume piknometer

1. Variabel 1
ρ = 39,71 – 16,86
25
= 0,914 gr/ml
2. Variabel 2
ρ = 39,43 – 16,86
25
= 0,903 gr/ml
3. Variabel 3
ρ = 39,18 – 16,86
25
= 0,893 gr/ml
4. Variabel 4
ρ = 38,82 – 16,86
25
= 0,878 gr/ml
5. Variabel 5
ρ = 38,79 – 16,86
25
= 0,877 gr/ml
1.2 Perhitungan Viskositas
μ0 = 1,004 Cp t0 = 1 s ρ0 = 1 gr/ml
𝑡𝑥 × ρx
Rumus: μx = × μ0
𝑡0 × ρ0

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1. Variabel 1

μx = 4,22 x 0,914 x 1,004


1x1
= 3,873 cp
2. Variabel 2
μx = 3,98 x 0,903 x 1,004
1x1
= 3,608 cp
3. Variabel 3
μx = 3,70 x 0,893 x 1,004
1x1
= 3,317 cp
4. Variabel 4
μx = 3,49 x0,878 x 1,004
1x1
= 3,078 cp
5. Variabel 2
μx = 3,21 x 0,877 x 1,004
1 x1
= 2,827 cp
1.3 Perhitungan α, Rm, Rc dan laju alir
1. Variabel 1
Diketahui :
Konsentrasi = 10 L : 10 L (Nira : Air)
= 15 kg/10 L
= 1500 kg/m3
a = 39.993 s/m6
b = 367.806 s/m3
kp = 79.986 s/m6
A = 470 x 470 mm
= 229.900 mm2
= 0,221 m2
-ΔP = 2 kg/cm2
= 20.000 kg/ms2
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μ = 3,873 cP

= 0,003873 kg/ms2
V = 10 L
= 0,01 m3
Jawab:
Kp x A2 x (−∆P)
α= μ x Cs

= (79.986 s/m6 (0,221 m2)2 x (20.000 kg/cm2)


0,008873 kg/ms2 x 1.500 kg/m3
= 1,34 x 107 m/kg
Jawab
B A(−∆P)
Rm = μ

= 367.806 s/m3 x (0,221 m2) x (20.000 kg/cm2)


0,008873 kg/ms2
= 4,2 x 1011 m-1
Jawab:
Rc = α x Cs x v
A
= 1,34 x 107 m/kg x 1.500 kg/m3 x 0,01 m3
(0,221 m2)
= 9,13 x 108 m-1
Jawab :
dv/dt = A x (-ΔP)
(Rm+Rc) x µ
= 0,221 m2 x (20.000 kg/cm2)

(4,2 x 1011 m-1 + 9,13 x 108 m-1) x 0,008873 kg/ms2)

= 4,07 x 10-11 m3/s

2. Variabel 2
Diketahui :
Konsentrasi = 10 L : 20 L (Nira : Air)
= 15 kg/20 L
= 750 kg/m3

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a = 15.507 s/m6
b = 198.923 s/m3
kp = 31.014 s/m6
A = 470 x 470 mm

= 229.900 mm2
= 0,221 m2
-ΔP = 2 kg/cm2
= 20.000 kg/ms2
μ = 3,608 cP
= 0,003608 kg/ms2
V = 20 L
= 0,02 m3
Jawab:
Kp x A2 x (−∆P)
α= μ x Cs

= 31.014 s/m6 x (0,221 m2)2 x 20.000 kg/ms2


0,003608 kg/ms2 x 750 kg/m3
= 1,19 x 107 m/kg
Jawab:
b x A x (−∆P)
Rm =
μ
= 198.923 s/m3 x 0,221 m2 x 20.000 kg/ms2
0,003608 kg/ms2
= 2,44 x 1011 m-1
Jawab :
Rc = α x Cs x v
A
= 1,19 x 107 m/kg x 750 kg/m3 x 0,02 m3
0,221 m2
= 7,60 x 108 m-1
Jawab :

dv/dt = A x (-ΔP)
(Rm+Rc) x µ

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= 0,221 m2 x 20.000 kg/ms2
(2,44 x 1011 m-1 + 7,60 x 108 m-1) x 0,003608 kg/ms2
= 6,52 x 10-11 m3/s
3. Variabel 3
Diketahui :
Konsentrasi = 10 L : 30 L (Nira : Air)
= 15 kg/30 L
= 500 kg/m3
a = 7.676 s/m6
b = 118.673 s/m3
kp = 15.352 s/m6
A = 470 x 470 mm

= 229.900 mm2
= 0,221 m2
-ΔP = 2 kg/cm2
= 20.000 kg/ms2
μ = 3,317 cP
= 0,003317 kg/ms2
V = 30 L
= 0,03 m3
Jawab:
Kp x A2 x (−∆P)
α= μ x Cs

= 15.352 s/m6 x (0,221 m2)2 x 0,221 m2


0,003317 kg/ms2 x 500 kg/m3
= 9,03 x 106 m/kg
Jawab:
b A(−∆P)
Rm =
μ
= 118.673 s/m3 x 0,221 m2 x 20.000 kg/ms2
0,003317 kg/ms2
= 1,58 x 1011 m-1
Jawab :
Rc = α x Cs x v
A

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= 9,03 x 106 m/kg x 500 kg/m3 x 0,03 m3
0,221 m2
= 6,14 x 108 m-1
Jawab :
dv/dt = A x (-ΔP)
(Rm+Rc) x µ
= 0,221 m2 x 20.000 kg/ms2

(1,58 x 1011 m-1 + 6,14 x 108 m-1) x 0,003317 kg/ms2

= 9,23 x 10-11 m3/s

4. Variabel 4
Diketahui :
Konsentrasi = 10 L : 40 L (Nira : Air)
= 15 kg/40 L
= 375 kg/m3
a = 3.238,5 s/m6
b = 76.699 s/m3
kp = 6.477 s/m6
A = 470 x 470 mm

= 229.900 mm2
= 0,221 m2
-ΔP = 2 kg/cm2
= 20.000 kg/ms2
μ = 3,078 cP
= 0,003078 kg/ms2
V = 40 L
= 0,04 m3
Jawab:
Kp x A2 x (−∆P)
α= μ x Cs

= 6.477 s/m6 x (0,221 m2)2 x 20.000 kg/ms2


0,003078 kg/ms2 x 375 kg/m3
= 5,48 x 106 m/kg

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Jawab:
bx A x (−∆P)
Rm =
μ
= 76.699 s/m3 x 0,221 m2 x 20.000 kg/ms2
0,003078 kg/ms2
= 1,10 x 1011 m-1
Jawab :
Rc = α x Cs x v
A
= 5,48 x 106 m/kg x 375 kg/m3 x 0,04 m3
0,221 m2
= 3,72 x 108 m-1
Jawab :
dv/dt = A x (-ΔP)
(Rm+Rc) x µ
= 0,221 m2 x 20.000 kg/ms2
(1,10 x 1011 m-1 + 3,72 x 108 m-1) x 0,003078 kg/ms2
= 1,23 x 10-10 m3/s

5. Variabel 5
Diketahui :
Konsentrasi = 10 L : 50 L (Nira : Air)
= 15 kg/50 L
= 300 kg/m3

a = 2.276 s/m6
b = 35.928 s/m3
kp = 4.552 s/m6
A = 470 x 470 mm

= 229.900 mm2
= 0,221 m2
-ΔP = 2 kg/cm2
= 20.000 kg/ms2
μ = 2,827 cP
= 0,002827 kg/ms2

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V = 50 L
= 0,05 m3
Jawab:
Kp x A2 x (−∆P)
α= μ x Cs

= 4.552 s/m6 x (0,221 m2)2 x 20.000 kg/ms2


0,002827 kg/ms2 x 300 kg/m3
= 5,24 x 106 m/kg
Jawab:
b x A x(−∆P)
Rm =
μ
= 35.928 s/m3 x 0,221 m2 x 20.000 kg/ms2
0,002827 kg/ms2
= 5,61 x 1010 m-1
Jawab :
Rc = α x Cs x v
A
= 5,24 x 106 m/kg x 300 kg/m3 x 0,05 m3
0,221 m2
= 3,56 x 108 m-1
Jawab :

dv/dt = A x (-ΔP)
(Rm+Rc) x µ
= 0,221 m2 x 20.000 kg/ms2
(5,61 x 1010 m-1 + 3,56 x 108 m-1) x 0,002827 kg/ms2
= 2,21 x 10-10 m3/s

1.4 Perhitungan TSS


TSS
Rumus : ((A-B) x 1000)
v
A = berat cawan kertas saring + residu kering
B = berat cawan + kertas saring
Volume sampel = 25 ml
B = 44,57 gram

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1. Variabel 1
TSS = (45,17 – 44,57) x 1000
25
= 24 gr/ml
2. Variabel 2
TSS = (45,11 – 44,57) x 1000
25
= 21,60 gr/ml
3. Variabel 3
TSS = (45,04 – 44,57) x 1000
25
= 18,80 gr/ml
4. Variabel 4
TSS = (44,88 – 44,57) x 1000
25
= 12,40 gr/ml
5. Variabel 5
TSS = (44,80 – 44,57) x 1000
25
= 9,20 gr/ml
1.5 Perhitungan Centrifug
Centrifug = tinggi endapan x 100%
Tinggi keseluruhan

1. Variabel 1
Centrifug = 0,90 cm x 100
18
= 5%
2. Variabel 2
Centrifug = 0,86 cm x 100
18
= 4,78%

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3. Variabel 3
Centrifug = 0,74 cm x 100
18
= 4,11%
4. Variabel 4
Centrifug = 0,62 cm x 100
18
= 3,44%
5. Variabel 5
Centrifug = 0,47 cm x 100
18 cm
= 2,61%
1.6 Foto Praktikum

Serangkaian Alat Filtrasi Plate and Frame

pengadukan nira dengan air

42
Analisa Densitas

Analisa Viskositas

Analisa Centrifug

Analisa TSS

43

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