Usg Epsilon1 en
Usg Epsilon1 en
USER GUIDE
EPSILON 1
USER GUIDE
1
DISCLAIMER
Although diligent care has been used to ensure that the information in this material is
accurate, nothing herein can be construed to imply any representation or warranty as
to the accuracy, correctness or completeness of this information and we shall not be
liable for errors contained herein or for damages in connection with the use of this
material. Malvern Panalytical reserves the right to change the content in this material
at any time without notice.
COPYRIGHT NOTICE
© 2021 Malvern Panalytical. This publication or any portion thereof may not be copied
or transmitted without our express written permission.
info@malvernpanalytical.com
www.malvernpanalytical.com
2
TABLE OF CONTENTS
Chapter 1. Introduction. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
1.1 General. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
1.2 Intended use. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
1.3 Recommended skill levels. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Chapter 2. Safety. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.1 Introduction to safety aspects. . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.1.1 Authorized personnel. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.1.2 Safety guarantee. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
2.1.3 Alerts and labels. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
2.2 Safety standards. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
2.3 Malvern Panalytical's approach. . . . . . . . . . . . . . . . . . . . . . . . . 11
2.4 User responsibilities. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
2.4.1 What to do in case of an emergency. . . . . . . . . . . . . . . . 12
2.5 General hazards. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
2.5.1 Ionizing radiation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
2.5.2 Toxic material. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
2.5.3 Flammable material. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
2.6 Safety measures. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
2.6.1 HT keyswitch. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
2.6.2 X-RAYS lamps. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
2.6.3 Double independent safety loops. . . . . . . . . . . . . . . . . . 15
2.6.4 Xsafe. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
2.7 Safe use of the instrument. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 16
2.7.1 Location of alerts and hazards. . . . . . . . . . . . . . . . . . . . . 17
3
TABLE OF CONTENTS
Chapter 4. Installation. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
4.1 Introduction. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
4.1.1 Guided self installation. . . . . . . . . . . . . . . . . . . . . . . . . . . 25
4.1.2 Installation by Malvern Panalytical. . . . . . . . . . . . . . . . . . 25
4.2 Unpack the instrument. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26
4.2.1 Examine the external impact indicators. . . . . . . . . . . . . 28
4.3 Install the instrument. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28
4.4 Let the instrument become stable. . . . . . . . . . . . . . . . . . . . . . 29
4.4.1 Do an X-ray leakage test. . . . . . . . . . . . . . . . . . . . . . . . . . 29
4
TABLE OF CONTENTS
Chapter 8. Troubleshooting. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43
8.1 Introduction. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43
8.2 Instrument does not switch on. . . . . . . . . . . . . . . . . . . . . . . . . 43
8.2.1 Replace the mains power fuses. . . . . . . . . . . . . . . . . . . . 43
8.3 HT generator does not switch on. . . . . . . . . . . . . . . . . . . . . . . 44
8.3.1 Reset Xsafe. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44
8.4 Open the lid locks when the instrument has no power. . . . 45
Index. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51
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TABLE OF CONTENTS
6
CHAPTER 1 INTRODUCTION
1.1 General
This User Guide gives a description of the hardware and instructions that are related to
safety, operation, user maintenance and disposal of these systems:
Read this User Guide together with the Epsilon 1 Quick Start Guides.
For more information, refer to the Epsilon 1 Help that is supplied with the software.
It is expected that the system will mostly be used by laboratory or factory personnel.
The system must not be used for purposes other than intended.
If the equipment is used in a manner not specified by the manufacturer, the protection
provided by the equipment may be impaired.
Standard user
7
CHAPTER 1 INTRODUCTION
Advanced user
8
CHAPTER 2 SAFETY
This chapter helps you to maintain and operate the analytical X‑ray instrument in
accordance with very high safety standards. It gives you information on how to keep
the instrument in a safe condition and how to prevent accidents. It is important that
you read this information to know the safety aspects of the Malvern Panalytical
instrument.
A Malvern Panalytical instrument is fully safe when it is correctly installed and when the
instructions in this User Guide are obeyed during operation.
If the safety information in this chapter does not comply with the related local (national
or regional) rules, always obey the local rules.
Procedures given in this User Guide can be done by the user. The installation,
maintenance and repair procedures of the instrument that are not in this User Guide
must only be done by Authorized Personnel .
All repairs, adjustments and alignments to any part of the instrument must obey all
applicable local regulations.
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CHAPTER 2 SAFETY
Obey all instructions in the alerts in the manual and on the labels attached to the
different parts of the instrument.
NOTE: Gives the user more information about the procedure or system.
Another important declaration for users of analytical X‑ray instruments is the X‑ray
Safety Declaration, which is also supplied with all instruments.
10
CHAPTER 2 SAFETY
The instrument complies with the requirements of the Machine Directive 2006/42/EC
and EMC Directive 2004/108/EC and the applicable X‑ray safety regulations.
Organizational requirements such as ISO 9001, ISO 14001, radiation safety board
inspections and audits make sure that these approaches are obeyed.
1. The user must make sure that the instrument is correctly installed. The user s site
facilities must comply with the specifications in the pre-installation and installation
11
CHAPTER 2 SAFETY
information, and comply with the applicable safety requirements. The user is also
responsible for these installation requirements:
a. A correct ground (earth) must be available.
b. The floor or table must be sufficient for the weight distribution of the
instrument.
2. Installation and maintenance must be done by Authorized Personnel.
3. Safety devices must NEVER be bypassed.
4. The user must make sure that persons that use the system are fully instructed in
the safety procedures.
5. The user must make sure that when the system is operated, the applicable local
safety regulations are obeyed.
6. All X‑ray analysis systems must be monitored regularly (based on a local risk
assessment) with a suitable X‑ray radiation monitor.
7. If the instrument is left unattended in a dangerous condition, do as follows:
a. Remove the HT (high-tension) key.
b. Disconnect the instrument from the mains power supply.
c. Attach a DO NOT OPERATE warning notice to all power buttons and mains
power switches or connections.
8. When X‑rays are generated, the fail-safe X‑rays warning lamps must be on. This
lamp must be clearly in view to all persons in the area.
9. In some countries, an X‑rays warning lamp and the international ionizing radiation
sign must be installed on the outer side of the room.
10. After installation or a maintenance/repair procedure is done, the user and the
service engineer must make sure that the safety interlocks operate correctly.
11. A Malvern Panalytical service engineer or application specialist can do a remote
support session on the instrument to troubleshoot, to examine the system after
repair or for application support. Before the remote support session is started,
the user must take precautions to make sure that the instrument can be operated
safely without local intervention.
12. Although the instrument is made and tested to be safe, maintenance is very
important. Information about user maintenance is given in this manual. Other
maintenance must be done by Authorized Personnel.
1. Switch off the instrument and make sure that it cannot be switched on again.
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CHAPTER 2 SAFETY
4. Put a sign on the instrument to make sure that the instrument will not be used or
changed.
5. You must tell these persons about the emergency:
• The user
• The (Radiation) Safety officer
• The local Malvern Panalytical representative
6. If it is an X‑ray exposure accident and the exposure is more than the level set in
local regulations, refer the exposed person for medical examination.
When the instrument is correctly operated within the specifications, the radiation level
at a distance of 10 cm from the outer surface of the instrument is less than 1 µSv/h.
It is important for the health and safety of the user that the instructions given
in the instrument manuals are obeyed.
Unknown samples can contain poisonous material. Take precautions when you touch
unknown samples.
13
CHAPTER 2 SAFETY
2.5.2.1 Beryllium
Do not get beryllium on your bare skin. Always wear gloves when you touch
items that contain beryllium.
If there are dust or fumes of beryllium, use a dust mask and protective
clothing.
Refer to the safety information in this document and the related Safety Data
Sheet for more details.
14
CHAPTER 2 SAFETY
2.6.1 HT keyswitch
All instruments have an HT keyswitch. The removable HT key helps the local radiation
safety officer to control who uses the system.
To prevent unauthorized use of the system, remove the HT key. A normal mains power
is available for other functions.
Only when the instrument senses that all conditions are safe, can the X‑RAYS lamps
come on and X‑rays be generated.
2.6.4 Xsafe
Xsafe is a safety protection system that gives the user protection against X‑rays. This
system contains an electronic board that permanently monitors switches in the
instrument to make sure that it is safe for X‑rays to be generated.
15
CHAPTER 2 SAFETY
The X‑ray tube in an instrument is energized by a high tension power supply. The safety
circuits automatically make sure that the high tension and X‑rays are immediately
switched off if there is a dangerous situation.
To make sure that Xsafe operates correctly, regularly do a test of the operation of the
safety switches.
Additionally, to make sure that all safety issues are sensed, the instrument must be
switched off and on at least once every 14 days as follows:
The next sections show possible safety risks from the instrument during sample
handling.
16
CHAPTER 2 SAFETY
3
4
17
CHAPTER 2 SAFETY
1 1
1 1
18
CHAPTER 3 SYSTEM DESCRIPTION
3.1 Introduction
The Epsilon 1 is a compact energy-dispersive X-ray spectrometer to do elemental
analysis of a wide range of samples.
You can control the system with an analytical software package installed on the
Epsilon 1.
7
3
6
4
4 5
19
CHAPTER 3 SYSTEM DESCRIPTION
2
4 3
5
2
3
4
20
CHAPTER 3 SYSTEM DESCRIPTION
1
2 2
3 3
4
5
6
1 2
6 5 4 3
1. USB connections 4. HDMI connection
2. Network connections 5. Display port connection
3. Audio connections 6. DC connection, do not use!
3.3 Controls
The hardware controls are installed on top and at the rear of the instrument.
21
CHAPTER 3 SYSTEM DESCRIPTION
2 4
The instrument is in the ON condition when the green light in the Power button is on.
When you press the Power button again, the instrument switches to the OFF condition.
The instrument is in the OFF condition when the green light in the Power button is off.
3.3.2 HT keyswitch
When you turn the HT keyswitch clockwise, it is possible to do a measurement. When
you start the measurement, the HT generator goes on.
The HT keyswitch is also used to reset the Xsafe system. Refer to Section 8.3.1.
If the HT key is removed from the instrument and an unsafe condition is sensed, you
cannot switch the high tension on again.
22
CHAPTER 3 SYSTEM DESCRIPTION
23
CHAPTER 3 SYSTEM DESCRIPTION
3
1
24
CHAPTER 4 INSTALLATION
4.1 Introduction
Before you install the system, make sure that the supplies are installed and agree with
the requirements in the Epsilon 1 Technical Specifications sheet.
If you are not sure, always contact your local Malvern Panalytical representative.
Instruction videos and a software wizard help the customer through all steps of the
installation. Some steps must be done by the service engineer via remote access to the
instrument.
Before the installation, the customer must have seen the instruction videos and read
the Epsilon 1 User Guide and the Guided Self Installation Instructions.
It is important for the health and safety of the user that the instructions given
in the instrument manuals are obeyed.
25
CHAPTER 4 INSTALLATION
9. Move the instrument to the final installation location with 2 persons. The
installation location must have a strong surface, for example a table.
NOTE: Keep 20 cm space behind the instrument for the airflow and to connect or
disconnect the mains power supply.
26
CHAPTER 4 INSTALLATION
364
20
0
37
5
395
27
CHAPTER 4 INSTALLATION
For more information, refer to the toxic material section in the Safety chapter.
NOTE: The recorded results of the impact indicator can help with any damage
claims procedure.
28
CHAPTER 4 INSTALLATION
NOTE: We recommend that the X-ray leakage test is done by a person trained in
X-ray safety.
NOTE: If the instrument is installed for the first time, a Malvern Panalytical service
engineer must do the X-ray leakage test.
An X-ray leakage test is done for each instrument and the X-ray radiation level is
measured before shipment. Our instruments are intrinsically safe when they are
operated and maintained correctly.
But also if it is not necessary in local regulations, Malvern Panalytical recommends that
you do an X-ray leakage test of the instrument regularly. This is specially important
during the installation, when the instrument is moved or when the instrument does
not get maintenance regularly.
29
CHAPTER 4 INSTALLATION
30
CHAPTER 5 OPERATE THE INSTRUMENT
5.1 Introduction
To prevent accidents, the floor around the instrument must be dry and there
must be no dirt or grease.
NOTE: We recommend that the X-ray leakage test is done by a person trained in
X-ray safety.
31
CHAPTER 5 OPERATE THE INSTRUMENT
NOTE: The gain measurement takes a snapshot of the instrument and this must
be done on a stable instrument.
2. For instruments with small spot analysis, remove the protection disk.
3. Put 2 fingers under the reference sample holder, push it up and lower the
reference sample holder on the measuring position.
3. Press OK.
32
CHAPTER 6 MEASURE SAMPLES
• Solid samples
These samples must be between 27 and 51.5 mm diameter with a maximum
height of 10 cm.
• Sample without a cup
These samples can be a maximum of 100 x 150 x 120 mm.
• Liquid samples
These samples are usually 5 mL or 10 mL. They must be put in the special P1
liquid cell or 'P2 liquid cell'. The liquid cells must be put in sample holders.
• Loose powders
Loose powders can also be measured in a 'P1 liquid cell' or 'P2 liquid cell'. The
liquid cells must be put in sample holders. For small quantities of the sample
(< 1 g), small mass holders are available.
33
CHAPTER 6 MEASURE SAMPLES
Only use sample cups that are approved for use in Malvern Panalytical
instruments.
For liquid cups, make sure that the cup lid is safely in position.
Do not keep temperature sensitive samples in the instrument for a long period.
34
CHAPTER 7 USER MAINTENANCE
7.1 Introduction
Follow the safety precautions of this User Guide when you do any of these procedures.
Refer to Chapter 2.
To do these procedures, it can be necessary to move the instrument from its normal
operating position.
35
CHAPTER 7 USER MAINTENANCE
For more information, refer to the toxic material section in the Safety chapter.
36
CHAPTER 7 USER MAINTENANCE
37
CHAPTER 7 USER MAINTENANCE
38
CHAPTER 7 USER MAINTENANCE
For more information, refer to the toxic material section in the Safety chapter.
4. Use laboratory tweezers to remove the clamping ring from the measuring
position.
39
CHAPTER 7 USER MAINTENANCE
40
CHAPTER 7 USER MAINTENANCE
41
CHAPTER 7 USER MAINTENANCE
42
CHAPTER 8 TROUBLESHOOTING
8.1 Introduction
This chapter gives the most common problems with the system and their solutions.
If a problem is not in this chapter, or if the solution did not remove it, collect all relevant
information about the problem and contact your local Malvern Panalytical service
organization.
The instrument is not switched on. Switch on the instrument. Refer to Section 5.2.
A fuse has blown in the mains power Replace the fuse. Refer to Section 8.2.1.
supply.
43
CHAPTER 8 TROUBLESHOOTING
HT keyswitch is in the OFF position. Turn the HT keyswitch Refer to Section 3.3.2.
clockwise.
1 or more of the X-RAYS lamps on the Contact your local
corners of the instrument is defective. Malvern Panalytical
service organization.
Xsafe is activated. Reset Xsafe. Refer to Section 8.3.1.
44
CHAPTER 8 TROUBLESHOOTING
8.4 Open the lid locks when the instrument has no power
When the instrument has no power and the lid locks are locked, you cannot open the
lid.
45
CHAPTER 8 TROUBLESHOOTING
5. Put a curved tool, for example an Allen key, in the holes of the lid locks and pull
the lid locks in the direction of the rear of the instrument. The lid can now be
opened.
46
CHAPTER 8 TROUBLESHOOTING
47
CHAPTER 8 TROUBLESHOOTING
48
CHAPTER 9 DISPOSAL INSTRUCTIONS
The function of the European WEEE Directive is to decrease the quantity of waste from
electrical and electronic equipment, and to decrease the hazardous substances of this
waste to protect human health and the environment.
On the instrument, the hazardous materials are identified with a label. Refer to Figure
2.1.
If you are not sure about the correct disposal procedure, contact your local
Malvern Panalytical representative.
9.2.1 Beryllium
Some items in the instrument contain beryllium (Be).
For more information, refer to the toxic material section in the Safety chapter.
49
CHAPTER 9 DISPOSAL INSTRUCTIONS
Refer to the Safety Data Sheet for the disposal procedure: (https://uqr.to/
epa4).
For disposal instructions, refer to the Tube Instruction Manual supplied with the X-ray
tube.
9.2.3 Detector
The window of the silicon drift detector contains beryllium (Be).
50
INDEX
51
INDEX
U
User responsibilities. . . . . . . . . . . . . . 11
W
WEEE Directive. . . . . . . . . . . . . . . . . . . 49
X
X-ray leakage test. . . . . . . . . . . . . . . . 29
X-RAYS lamps. . . . . . . . . . . . . . . . . . . . 15
Xsafe. . . . . . . . . . . . . . . . . . . . . . . . 44, 15
52