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XI-SALT ANALYSIS FORMAT (1)

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17 views4 pages

XI-SALT ANALYSIS FORMAT (1)

Uploaded by

movieloverbooklover
Copyright
© © All Rights Reserved
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XI- DAV PKN- CHEMISTRY PRACTICAL- SALT ANALYSIS REPORT FORMAT

DATE: EXPT NO:

NAME OF THE STUDENT: _____________________ CLASS&SEC:

SYSTEMATIC ANALYSIS OF SIMPLE SALT –I

EXPERIMENT OBSERVATION INFERENCE


Colour of the salt

Smell of the salt

Action of heat- Take a pinch


of salt and heat it in a dry test
tube.

Flame test- Take a pinch of


salt and make a paste with few
drops of conc.HCl and
introduce it in the luminous
part of the flame.

Ash test- Take a pinch of salt


and add few drops of cobalt
nitrate solution. Dip a filter
paper and burn it. Look into the
colour of the ash.

DRY TESTS:
Dil. HCl test- To a pinch of
salt add dil HCl

Conc H2SO4 test- To a pinch


of salt,add conc sulphuric acid
and warm.

Chromyl chloride test- To a


pinch of salt add a pinch of
K2Cr2O7 and conc H2SO4 and
heat. Pass the fumes into a test
tube containing NaOH and add
acetic acid and lead acetate
solution.

1 |27-12-2023; prepared and compiled by R VANISHREE SHANKARI


XI- DAV PKN- CHEMISTRY PRACTICAL- SALT ANALYSIS REPORT FORMAT

MnO2 test- To a pinch of salt


add half a pinch of MnO2 and
conc H2SO4 and heat.

Cu turnings test- To a pinch


of salt , add Cu turnings and
conc. H2SO4 and heat. Pass the
fumes into a solution of FeSO4
solution.

NaOH test- To a pinch of salt,


add sodium hydroxide and
heat.

Ferric chloride test- To a pinch of


salt add 1 ml of ferric chloride
solution. Heat.

Ester test- To a pinch of salt add few


ml of ethyl alcohol and conc H2SO4
and heat.

SODIUM To a part of salt add two parts


of sodium carbonate and 10 ml
CARBONATE
of distilled water. Boil the
EXTRACT contents, cool and filter. The
filtrate is called as sodium
carbonate extract.

Silver nitrate test: To a part of


the extract, add dil HNO3 and
silver nitrate solution.

Barium chloride test: To a


part of the extract , add dil HCl
and barium chloride solution.

Lead acetate test: To a part of


the extract, add dil acetic acid
and lead acetate solution.

Brown ring test: To a part of


the extract, add dil H2SO4 till
the effervescence ceases and
then add freshly prepared
FeSO4 solution and conc
H2SO4 to the sides of the test
tube.

2 |27-12-2023; prepared and compiled by R VANISHREE SHANKARI


XI- DAV PKN- CHEMISTRY PRACTICAL- SALT ANALYSIS REPORT FORMAT

To part of the extract, Add a few drops


of Conc.HNO3 and boil. Then add
ammonium molybdate solution.

To a part of the extract, add dil HCl


and heat. Then add magnesia mixture.

Calcium chloride test: To part of


extract , add dil. Acetic acid and heat.
Then add Calcium chloride solution.

BASIC RADICAL PREPARATION OF OS:


Dissolve the salt in distilled
ANALYSIS
water to prepare a saturated
solution.

EXPERIMENT OBSERVATION INFERENCE


ZEROTH GROUP: To the
salt concentrated solution of
sodium hydroxide is add and
warmed.

A glass rod dipped in dil.HCl is


shown near the mouth of the
test tube.

FIRST GROUP: To the OS,


add dil. HCl.

SECOND GROUP: To the


OS, add dil.HCl and YAS

THIRD GROUP To the OS,


add NH4Cl and NH4OH

To the OS, add NH4Cl and NH4OH and


YAS.

To the OS , add NH4Cl and NH4OH and

(NH4)2 CO3.

To the OS, add some solid NH4Cl and


NH4OH in slight excess. Then add
ammonium phosphate solution and rub the
sides of the test tube with a glass rod.

3 |27-12-2023; prepared and compiled by R VANISHREE SHANKARI


XI- DAV PKN- CHEMISTRY PRACTICAL- SALT ANALYSIS REPORT FORMAT

CONFIRMATORY TESTS FOR IDENTIFIED BASIC RADICAL

EXPERIMENT OBSERVATION INFERENCE

RESULT: THE ACID RADICAL IS _________________________

THE BASIC RADICAL IS _____________________________

The given simple salt is ___________________________________________.

4 |27-12-2023; prepared and compiled by R VANISHREE SHANKARI

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