BS 812-124 1989
BS 812-124 1989
BS 812-124 1989
Testing aggregates —
Part 124: Method for determination of
frost-heave
Licensed Copy: Giorgio Cavalieri, none, 17-Nov-00, Uncontrolled Copy. © BSI
Contents
Page
Committees responsible Inside front cover
Foreword ii
1 Scope 1
2 Definitions 1
3 Principle 1
4 Sampling 1
5 Apparatus 1
6 Setting-up of the self-refrigerated unit 5
7 Operating temperatures and self-refrigerated unit tuning procedures 13
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© BSI 02-1999 i
BS 812-124:1989
Foreword
This Part of BS 812, prepared under the direction of the Cement, Gypsum,
Aggregates and Quarry Products Standards Committee, forms part of a general
revision that is being made of the 1975 edition of BS 812. As each of the tests or
collection of related tests, is prepared, it is intended to issue it as a separate
Part of BS 812.
This Part contains the test procedure for the determination of the frost-heave of
aggregates which have been compacted at a pre-determined moisture content and
density. The test was not included in previous editions of BS 812 but has now
been included because there is a need for a test to identify frost-susceptible
aggregates which could otherwise be used in an unbound form in road bases and
Summary of pages
This document comprises a front cover, an inside front cover, pages i and ii,
pages 1 to 22, an inside back cover and a back cover.
This standard has been updated (see copyright date) and may have had
amendments incorporated. This will be indicated in the amendment table on
the inside front cover
ii © BSI 02-1999
BS 812-124:1989
© BSI 02-1999 1
BS 812-124:1989
Figure 1 — Main features and dimensions of test chamber Licensed Copy: Giorgio Cavalieri, none, 17-Nov-00, Uncontrolled Copy. © BSI
5.3.2.2 The test chamber shall be provided with a NOTE The device shown in Figure 3 has been found to be a
hinged lid having a stainless-steel lower surface. simple and convenient method of maintaining a constant level of
water in the apparatus but it is permissible for other means of
The lid shall have nine holes at the same centres as keeping the water level constant to be used if preferred.
the holes in the specimen cradle to allow push-rods 5.3.3.2 A device for gently circulating the water in
(see 5.3.4.1) to be located. These holes shall be not the water-bath to maintain an even temperature
less than 10 mm and not more than 15 mm in distribution (see 7.2.1).
diameter. The water-bath shall be provided with an
overflow tube (see 5.3.3.1) and shall also be fitted
with a separate drain-cock. An interior light shall be
fitted to the underside of the lid.
5.3.3 The refrigeration and control equipment
5.3.3.1 A means of maintaining the water in the
water-bath at a constant level between 8 mm
and 11 mm from the underside of the specimen
cradle (i.e. as close as possible to the tops of the
porous discs). The principle of a suitable device is
illustrated in Figure 3 (see note).
2 © BSI 02-1999
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© BSI 02-1999 3
BS 812-124:1989
4 © BSI 02-1999
BS 812-124:1989
5.3.3.6 A rigid detachable metal datum frame, to 5.5 Tared glass flask, at least one of each of the
support the push-rods (Figure 1) which can be following capacities:
positively located above the lid of the test chamber 250 mL, 500 mL, 1 000 mL.
having horizontal bars with holes 6.5 mm diameter
5.6 A mechanical mixer, with a capacity of at
at the same centres as the holes in the specimen
least 20 kg. The mixer shall not cause any
cradle and the test chamber lid. The upper surface
significant degradation of the particles.
of the datum frame shall be not less than 125 mm
and not more than 175 mm above the top of the lid. 5.7 Containers, at least nine, which can be made
airtight, capable of holding 15 kg samples of mixed
5.3.4 Additional equipment for use with the SRU
material.
5.3.4.1 Nine brass rods, 750 mm long and 6.0 mm in 5.8 A steel mould and end-plugs as shown in
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© BSI 02-1999 5
BS 812-124:1989
6 © BSI 02-1999
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Figure 5 — Mould and end plugs for the preparation of frost-heave test specimens
© BSI 02-1999 7
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© BSI 02-1999
Figure 6 — Hand-held tamper
BS 812-124:1989
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© BSI 02-1999 9
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© BSI 02-1999
Figure 8 — Specimen extruder
BS 812-124:1989
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© BSI 02-1999
Figure 9 — Extrusion cylinder
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BS 812-124:1989
BS 812-124:1989
12 © BSI 02-1999
BS 812-124:1989
g) Open tap O. Air should bubble through the After 20 h have elapsed switch on the SRU and
capillary tube as water flows into the water-bath. leave it for a further 20 h before any internal
When the bubbling stops adjust the water level in temperature measurements are made. Determine
the bath (see note) so that it is about 1 mm from the length of the initial cooling period (see note 2).
the top of the porous disc, i.e. the surface of the The air and water should reach their operating
disc appears wet but is not covered. If the level is temperatures between 4 h and 14 h from starting
too low, close tap O and raise the level of the the SRU.
capillary slightly. Re-open tap O and allow the NOTE 1 Although cement-bound specimens cannot be used in
water to find its new level (see note). Repeat this tuning tests because they affect the heat transfer characteristics,
process until the required setting has been they may be used for convenience in any preliminary trials to
adjust thermostats.
achieved.
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© BSI 02-1999 13
BS 812-124:1989
14 © BSI 02-1999
BS 812-124:1989
8.2.2.5 Use the mixed material to prepare and NOTE 2 The procedure given in this clause provides for mixing
extrude a trial specimen using the procedure all the material for three specimens at once and this is the
preferred method. However, if a small mixer is being used it may
in 9.3.1 and 9.3.2. be necessary to mix the material for each specimen separately. In
8.2.2.6 If immediately after extrusion the specimen this case use a representative mass of 1.360 ρd (g) of material
with 0.0136 wρd (g) of water, and the procedure repeated three
is unstable, i.e. cannot stand on the extruder times for each batch of three specimens.
without collapsing, some adjustment to the dry NOTE 3 The method given assumes that in sub-dividing the
density and/or the moisture content may be material to prepare the individual test specimens no segregation
necessary to achieve a specimen which is occurs and that the particle size distribution of the material in
the individual test specimens remains the same as that of the test
sufficiently stable but at the same time has not been portion. In materials subject to segregation it may be preferable
subjected to such a degree of compaction that undue at this stage to sieve the dried test portion on
Licensed Copy: Giorgio Cavalieri, none, 17-Nov-00, Uncontrolled Copy. © BSI
crushing of the individual particles has occurred. the 37.5 mm, 20 mm, 10 mm and 5 mm test sieves. These size
This has to be achieved systematically by trial and fractions (after rejecting the material retained on the 37.5 mm
sieve) can then be re-combined in the proportions represented by
error until a stable specimen has been made. the grading of the original test portion to produce three
8.2.2.7 When a stable specimen has been prepared individual test samples each having a mass of 1.360 ρd (g). These
test samples are mixed with 0.0136 wρd (g) of water as described
transfer the specimen to a suitable container, break and each used to prepare one frost-heave specimen as described
it up and dry. Determine the particle-size in 9.3.1.1.
distribution of the material in the specimen using 9.2.3 Place a tared flask on the balance and weigh
the procedure described in 7.2 of BS 812-103:1985. out a mass of water (see note to 6.5) equal
NOTE The degree to which crushing of the particles has to 0.0408 wρd (g) (where w is the percentage
occurred during the preparation of the specimen may then be moisture content for the stable trial specimen
assessed. The moisture content value and dry density used to
prepare the stable specimens will be the values to be substituted in 8.2).
for w and rd in clause 9 when mixing and preparing the actual 9.2.4 Add the water to the dry material already in
test specimens.
the mixer and thoroughly mix. Store the mixed
9 Preparation of test specimens material in a sealed container for a minimum period
of 16 h before proceeding with the test.
NOTE The frost-heave test is normally carried out on three
NOTE Because inadequate mixing can give rise to variable test
specimens and because the SRU can accommodate nine, three
results it is important that the water is thoroughly and
different materials are normally tested at a time. The test
adequately mixed with the material. The procedure given
procedure as described is based on measuring the frost-heave of
ensures that this will be so and although it may be unnecessarily
three specimens. Some other specifications may call for more
stringent for granular materials of low-absorbency it is
specimens in which case suitable adjustments should be made to
recommended that all materials should be stored before
the test procedure.
proceeding with the test.
9.1 Test portions 9.2.5 Repeat the procedure described in 9.2.1
9.1.1 Sub-divide the test portion, obtained as to 9.2.4 inclusive until three batches of mixed
described in 4.1 a), by riffling until a representative material have been prepared.
test sample of mass about 15 kg is obtained. Set 9.3 Method for preparing a single test
aside the remainder of the test portion in case it is specimen
needed for repeat tests and use the 15 kg test
NOTE The following method is used when preparing a single
sample to prepare a set of three specimens for specimen of mixed material prepared as described in 9.2.
testing as described in 9.3 (see note 3 to 9.2.2).
9.3.1 Compaction into the mould
9.1.2 Repeat the procedure given in 9.1.1 with the
test portions of the other aggregates to be included 9.3.1.1 Transfer the mixed material prepared as
in this test run. described in 9.2 to the balance until the balance
holds a mass, M, equal to 1/3 of the mass required
9.2 Mixing for one frost-heave specimen, to the nearest 2 g. M is
9.2.1 Sieve the test sample prepared as described calculated from the equation:
in 9.1 to remove material coarser than 37.5 mm. M = 0.00412 ρd (100 + w) (g)
9.2.2 Select a representative mass equal where ρd is the stable-specimen dry density and w is
to 4.08 ρd (g) (where ρd is the dry density in kg/m3 the stable-specimen moisture content determined as
determined for this material as described in 8.2) described in 8.2.
from the sieved material and place it in the mixer.
NOTE 1 The mass includes excess material to allow for
handling losses.
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BS 812-124:1989
9.3.1.2 Carefully transfer the weighed material into NOTE 2 If the end plugs cannot be removed by hand, the mould
the mould, which must be placed over its bottom assembly should be left to stand for 5 min to 10 min before a
further attempt is made. This allows excess moisture which may
(smaller) end plug. Level the material in the mould form a seal around the plugs to drain away. It is important not to
with a suitable spatula. Hold the tamper strike the mould or plugs with a heavy object since this is likely
(see Figure 5) inside the mould with the upper to damage them. If, however, after 10 min standing the plugs still
cannot be removed, gentle tapping with a suitable light (and
surface of its base level with the top of the mould preferably non-metallic) object may be employed e.g. a
then allow it to drop freely under its own weight, rubber-faced mallet. If plugs become persistently difficult to
taking care that the foot is level when it strikes the remove, the mould and plugs should be checked for damage and
material. Repeat this process until 25 drops have their dimensions checked. A mould can become distorted even
during normal use.
been completed.
9.3.2.2 Extrude the specimen from the
16 © BSI 02-1999
BS 812-124:1989
10 Procedure for determination of the 10.1.5 When the coarse sand has been placed check
frost-heave the positions of the thermocouples and any control
sensors and then close the lid of the test chamber.
10.1 Loading test specimens into the Locate the datum frames on the SRU, pass the
self-refrigerated unit push-rods through the holes in the frame and
10.1.1 Using mixed material from one of the batches chamber lid and locate in the central recesses of the
previously prepared (9.2) prepare a frost test corresponding Tufnol discs. Start the constant-level
specimen using the method described in 9.3. device by opening the outlet tap, O (Figure 3), to
10.1.2 Place the prepared specimen in one of the allow water to flow into the water-bath and restore
holes in the wooden cradle in the test chamber. If the correct level. The water level is controlled
automatically for the remainder of the test.
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10.1.3 Repeat the procedure in 10.1.1 and 10.1.2 10.2 Freezing the specimens and measuring
until three specimens for each of the materials or six frost-heave
specimens for one material and three of another 10.2.1 When 115 ± 5 h have elapsed from the time
material have been prepared and located in the that the last specimen was inserted in the cradle,
cradle. Fill all nine positions. check the push-rods to make sure that they are
10.1.4 When nine specimens have been positioned, correctly located. Use surgery wool or similar
position four thermocouples so that there is one absorbent material to plug the gaps between each
above each of the spots marked x on the floor of the push-rod, and the hole in the test-chamber lid
cradle in Figure 2, at a level 250 mm above the through which it passes. This prevents
plane containing the lower faces of the specimens. condensation, which may form on the rods when the
An acceptable method of achieving this is to attach SRU is cool, from running into the test chamber.
each thermocouple to a 6 mm diameter wooden Take care to avoid dislocating any of the push-rods.
dowel about 300 mm long so that the junction is Do not pack the surgery wool too tightly into the
exposed 205 ± 2 mm from the lower end of the holes.
dowel. The four dowels may then be positioned on 10.2.2 Record the distance between the top of the
the floor of the cradle (see note). Place the coarse rod and the top of the datum for each push-rod to the
sand carefully in the space around the specimens nearest 0.5 mm.
(and around the vertical dowels if these are used) 10.2.3 Record the temperature of each
until the sand is level with the tops of the thermocouple.
specimens. This should leave the waxed paper
10.2.4 Switch on the controls of the SRU to start the
standing approximately 50 mm above the level of
freezing process and note the time. The operating
the sand. Take care to remove any sand particles
temperatures defined in clause 7 should be reached
accidentally split on the Tufnol discs, particularly in
between 4 h and 14 h from switching on and
the recesses.
maintained for the duration of the test.
NOTE It is not usually necessary to provide support for the
dowels, they will be held in position by the coarse sand. However, 10.2.5 Measure the frost-heave after a period
if problems arise rubber tubing can be placed on the dowel ends of 24 ± 2 h from the time of switching on the
which are then pushed onto preset studs on the floor of the cradle. refrigeration by the following procedure.
Care should be taken to ensure that particles of sand do not get
under the dowels thus raising the thermocouples. a) Rotate the push-rods to ensure that they have
not stuck. Check the surgery wool and replace if
necessary.
b) Record the distance between the top of the rod
and the top of the datum frame for each of the
nine push-rods to the nearest 0.5 mm. Any heave
that has occurred may be obtained by
subtraction.
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BS 812-124:1989
10.2.6 Continue to record the frost-heave as 10.4.4 Carefully remove the thermocouples in the
described in 10.2.5 at intervals of 24 ± 2 h until at air above the specimens from above the cradle and
least 96 h have elapsed from the time of switching put on one side.
on the refrigeration. 10.4.5 Remove the coarse sand (a vacuum cleaner
10.3 Monitoring the temperature conditions may be used) and dry and remove any material to
allow re-use of the sand (see note to 6.2). Do not
10.3.1 Employ the procedure described in 10.3.2
re-use the sand until it has returned to room
to 10.3.4 during every test.
temperature.
NOTE Although it is not necessary to carry out a detailed
tuning check of the SRU before or during every test, it is 10.4.6 Remove the specimens from the cradle,
important to ensure that the equipment continues to operate taking care not to damage any thermocouples as
18 © BSI 02-1999
BS 812-124:1989
11.2 For each material tested determine for each NOTE If each laboratory had determined the moisture content
specimen the maximum heave observed and density for its own tests it is probable that larger values of
R1, R2 and VL than given in Table 2 would have been obtained.
within 96 h, and calculate the mean of the maxima However, recent research at the Transport and Road Research
to the nearest 0.1 mm. Regard these mean values of Laboratory with two sub-base materials (with mid-range
frost-heave as the frost-heave of the aggregate gradings) has shown that changes in the moisture content and
density of the frost-heave test specimens have little effect on the
under test, subject to the following conditions. values of heave recorded.
a) If all nine specimens of the material under test 12.2 The tests for outliers given in BS 5497-1:1979
have heaves of less than 2.0 mm the results are were applied to the data. All the results from one
suspiciously low. The test should therefore be laboratory were rejected (they had not used the
repeated unless previous experience of the nominated moisture and density in some of their
Licensed Copy: Giorgio Cavalieri, none, 17-Nov-00, Uncontrolled Copy. © BSI
materials under test shows that the results are tests). The results on one test portion from another
consistent with what would be expected. laboratory were rejected, because the range between
b) If the mean heave of the three specimens is less the frost-heave specimens from that test portion
than 18.0 mm, calculate the range was an outlier.
(i.e. highest- lowest) of the heaves of the three 12.3 Definitions of r1, R1, and R2 are given in
specimens. If the range exceeds 6.0 mm repeat clause 2 of BS 812-101:1984. The variabilities which
the test before reporting any result. arise in the sampling and sample reduction
c) If the mean heave of the three specimens operations are apportioned to Vr1 and VS according
is 18.0 mm or greater no further testing is to the definitions of sampling error and sample
required. reduction error given in clause 2 of Part 101:1984.
11.3 When any repeat testing has been completed The variances Vr1, VL and VS are defined by the
calculate the mean heave using the results from all equations given in Table 1 of Part 101:1984. For the
the specimens. frost-heave test, the variance Vr1 contains
contributions from three components:
12 Precision VRuns = variation between runs of the
Table 2 — Precision estimates, frost-heave SRU,
(mm) VTest portions = variation between test portions of
Level Average r1 R1 R2 √Vr1 √VL √VS a laboratory sample;
mm mm mm mm mm mm mm
VSpecimens = variation between frost-heave
specimens, from the same test
Flint gravel 13.5 7.0 8.5 9.0 2.5 1.8 1.0 portion, in the same run.
12.1 The precision data given in Table 2 were A “run” consists of the cycle of operations described
determined from an experiment conducted in clause 10.
in 1984/5 involving 19 laboratories. The experiment
When the frost-heave test is carried out as
was designed, and the data analysed following the
suggested in 9.1, using three frost-heave specimens
principles set out in BS 5497-1:1979. The material
prepared from one test-portion, the “test result” is
tested consisted of a 20 tonne lot of flint gravel,
the average over three specimens, and
complying with the grading requirements for a
Type 2 road sub-base. The laboratory samples were Vr1 = VRuns + VTest portions + (VSpecimens/3)
taken according to BS 812-102:1984, all by one This equation was used to calculate Vr1 in Table 2
sampler. Two randomly selected laboratory samples above. Consequently, the precision estimates r1, R1
were sent to each laboratory. The laboratories and R2 may be compared with differences between
produced two test portions (each sufficient for three two test results when the two test results are
frost-heave specimens) from each laboratory sample obtained from different test portions and from
by following the procedure given in 6.4 of different runs, and as averages over three
BS 812-102:1984. All the frost-heave specimens specimens. The following values were obtained in
which were used to obtain the above precision data the experiment:
were prepared at a moisture content and a density
which had been nominated in advance (see note). VRuns = 1.8 mm
VTest Portions = 1.3 mm
VSpecimens = 1.9 mm
© BSI 02-1999 19
BS 812-124:1989
13 Test report
The test report shall affirm that the frost-heave was
determined in accordance with this Part of BS 812
and whether or not a certificate of sampling is
available. if available, a copy of the certificate of
sampling shall be provided. The test report shall
contain the following information.
20 © BSI 02-1999
BS 812-124:1989
© BSI 02-1999 21
BS 812-124:1989
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Table 4 — SRU tuning, temperature parameter summary chart © BSI 02-1999
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BS 812-124:1989
Publications referred to
© BSI 02-1999
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