2 RESPONSIBILITIES
2.1 The Quality Director or designee: 2.1.1 Issues stamps to certified employees 2.1.2 Verifies and audits the process per MTI procedure. 2.1.3 Ensures that the required testing is performed in compliance with this procedure. 2.2 The PM: 2.2.1 Oversees employee training and certification. 2.2.2 Ensures all calibrations and surveys are current. 2.2.3 Reviews heat-treat records and charts for conformance to customer requirements and maintains the records for a period of seven years. 2.3 The Engineer: 2.3.1 Specifies on the router the correct time and temperature range to which the parts are to be heated. 2.4 The Operator: 2.4.1 Maintains his/her personal safety equipment and ensures personal safety. 2.4.2 Maintains the temperature control instrumentation. 2.4.3 Maintains and archives the temperature recording charts. 2.4.4 Ensures traceability of the temperature/time recorder charts on the shop router. 2.4.5 Ensures all calibrations and surveys are current.
3.3
3.4
3.5
3 PROCEDURE
3.1 For alloys not specified in this document, refer to the customer specifications. The engineer must specify all parameters on the part routing. 3.2 Applicable Documents Heat Treat of Titanium Alloys MQ-04-14-00-00 rev 02 3.6
Date Printed
Apr 3, 2008
3.6.1 The maximum time for heating equipment to recover to a minimum of the temperature tolerance range tolerance should be as follows: 3.6.1.1 Thermal treatment over 1500 F in air 35 minutes. 3.6.1.2 Aging, stress relieving or forming of STA material 2 hours. 3.6.1.3 Annealing, stress relieving, or forming below 1500 F of MA and RA materials 10 hours. 3.7 Fixtures 3.7.1 Fixtures may be used during age or stress relief to minimize distortion. They are not allowed for solution annealing without prior approval from engineering. 3.8 Cleaning 3.8.1 Wear white cotton gloves when handling titanium parts. 3.8.2 Cleaning prior to thermal processing. 3.8.2.1 All parts shall be cleaned and free of fingerprints, dirt, oil, water, and other foreign materials, except scale inhibiting compound. Clean parts per Cleaning and Etching of Titanium Alloys, MQ-04-28-00-00. When multiple thermal processing is used, the pretreat need not be removed between processes. However, the pretreat must be evaluated and touched up if required. 3.8.2.2 All parts cleaned and protected with pretreat must be handled in such a manner as to prevent contamination by oil, grease, or fingerprints. 3.8.2.3 All fixtures that will contact the part shall also be cleaned to ensure that the titanium is not contaminated during treatment. Loose scale, dirt, oil, water, and other foreign material shall be removed. 3.8.3 Cleaning After Thermal Processing 3.8.3.1 All parts shall be descaled and etched per Cleaning and Etching of Titanium Alloys, MQ-04-28-00-00. 3.9 General 3.9.1 Loading parts for the thermal processing shall not damage pretreat coating. 3.9.2 During annealing and stress relieving, flat or nested parts may be stacked to a thickness greater than one inch provided that the thermocouples are attached in the area of the greatest thickness or in the area of the slowest heat up.
3.9.3 Total thickness of the stack rather than part thickness shall be used in Table 3, Tables for Heat Treat of Titanium Alloys, MQ-04-1400-01. 3.10 Stress Relieving 3.10.1 Time-temperature requirements for stress relieving shall be in accordance with Table 3, Tables for Heat Treat of Titanium Alloys, , MQ-04-14-00-01, unless parts are being formed or flattened during stress relief cycle, then Table 1, Tables for Heat Treat of Titanium Alloys, , MQ-04-14-00-01, will be used. 3.10.2 Stress relieving is required on parts that are hot brake formed unless noted on the shop router. 3.11 Metal removal after heat treatment is performed in accordance with Cleaning and Etching of Titanium Alloys, MQ-04-28-00-01 Table 1. 3.12 Hydrogen pick-up testing is not required for MTI processes because furnace temperature ranges and/or furnace types meet or exceed customer specified requirements.
Approvals
3 Apr 2008 Date
Document Custodian
Quality Director
Date Printed
Apr 3, 2008